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Palladium-Catalyzed Synthesis of Nitrones Via Redox Cross-Coupling of Nitro Compounds and Alcohols.
Xing, Jian; Tang, Hong-Yu; Chen, Jing-Lin; Huang, Zheng; Liang, Jun-Jie; Quan, Yao-Sheng; Mao, Jian-Gang.
Afiliação
  • Xing J; School of Chemistry and Chemical Engineering, Jiangxi Province Key Laboratory of Functional Crystalline Materials Chemistry, Jiangxi University of Science and Technology, 156 Kejia Avenue, Ganzhou 341000, P. R. China.
  • Tang HY; School of Chemistry and Chemical Engineering, Jiangxi Province Key Laboratory of Functional Crystalline Materials Chemistry, Jiangxi University of Science and Technology, 156 Kejia Avenue, Ganzhou 341000, P. R. China.
  • Chen JL; School of Chemistry and Chemical Engineering, Jiangxi Province Key Laboratory of Functional Crystalline Materials Chemistry, Jiangxi University of Science and Technology, 156 Kejia Avenue, Ganzhou 341000, P. R. China.
  • Huang Z; School of Chemistry and Chemical Engineering, Jiangxi Province Key Laboratory of Functional Crystalline Materials Chemistry, Jiangxi University of Science and Technology, 156 Kejia Avenue, Ganzhou 341000, P. R. China.
  • Liang JJ; School of Chemistry and Chemical Engineering, Jiangxi Province Key Laboratory of Functional Crystalline Materials Chemistry, Jiangxi University of Science and Technology, 156 Kejia Avenue, Ganzhou 341000, P. R. China.
  • Quan YS; School of Chemistry and Chemical Engineering, Jiangxi Province Key Laboratory of Functional Crystalline Materials Chemistry, Jiangxi University of Science and Technology, 156 Kejia Avenue, Ganzhou 341000, P. R. China.
  • Mao JG; School of Chemistry and Chemical Engineering, Jiangxi Province Key Laboratory of Functional Crystalline Materials Chemistry, Jiangxi University of Science and Technology, 156 Kejia Avenue, Ganzhou 341000, P. R. China.
J Org Chem ; 89(14): 9841-9852, 2024 Jul 19.
Article em En | MEDLINE | ID: mdl-38917372
ABSTRACT
A novel methodology for the synthesis of nitrones via palladium-catalyzed redox cross-coupling of nitro compounds and alcohols is established. The protocol is a mild, convenient, ligand-free, and scalable synthesis method that can be compatible with various nitro compounds and alcohols. Nitrone is a significant multifunctional platform synthon which can be synthesized directly and efficiently via this tactic from commercially available and cheap raw materials.
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2024 Tipo de documento: Article
Texto completo
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Texto completo: 1 Base de dados: MEDLINE Idioma: En Ano de publicação: 2024 Tipo de documento: Article