Novel treatment of in-office tooth bleaching sensitivity: A randomized, placebo-controlled clinical study.

OBJECTIVES: Aim of this clinical trial was to investigate the effect of a calcium phosphate based desensitizer paste applied prior to in-office tooth whitening on bleaching sensitivity (BS). METHODS: This crossover study was designed as randomized double-blinded, placebo-controlled trial. The desensitizer paste Teethmate AP (TAP) contains tetracalcium phosphate and dicalcium phosphate anhydrous in glycerol and polyethylene glycol, whereas placebo (PLA) is a calcium phosphate free analog. Fifty patients with sound maxillary incisors and canines were enrolled. Tooth shades were determined with a Vitapan Classic Shade guide. Randomly, TAP and PLA were applied to the left or to the right anterior teeth. After rinsing and air-drying the bleaching gel (Opalescence Boost PF 40%) was applied and left on the labial surfaces for 15 minutes. Sensitivity was recorded using a 10 cm visual analog scale (VAS) before, at 5, 10, and 15 minutes during, and at 1 hour, 1, 2, and 7 days after bleaching. Tooth whitening was determined with the shade guide after 1 day and 1 week. RESULTS: Prebleaching desensitization with TAP reduced BS significantly when compared with PLA. Between 1 and 7 days the average sensitivity scores were close to zero, whereas the average scores for PLA were significantly higher during this time interval. Independent from the desensitizing treatment after 1 and 7 days the medians of the shades were between 5 and 3.5 units brighter. CONCLUSIONS: Prebleaching desensitization with TAP was effective in reducing BS during and after tooth whitening treatment and had no adverse effect on the bleaching result. CLINICAL SIGNIFICANCE: Prebleaching topical application of a calcium phosphate containing compound reduced significantly bleaching sensitivity during a single 15 minutes treatment and up to one week with a 40% hydrogen peroxide containing gel without compromising tooth whitening.

In vitro and in vivo evaluation of the effectiveness of three dentin desensitizing treatment regimens.

PURPOSE: To evaluate the in vitro and in vivo effects of three treatment regimens on dentin permeability and reduction of dentin hypersensitivity (DH). METHODS: The desensitization treatments were: Gluma Desensitizer PowerGel (GLU), MS Coat One (MSC), and dentin burnishing with fiber-resin burs (STB). A split-chamber device was used to determine the permeability of dentin slices cut from human molars in vitro. Fluid flow through dentin was recorded with a photochemical method after EDTA cleaning, albumin soaking and desensitization treatment (n = 10). 61 study participants with three severely hypersensitive teeth each were enrolled. Sensitivity was determined with an air stimulus before, immediately after treatment, and after 1, 3 and 6 months, using a verbal rating scale. RESULTS: From the 61 study participants enrolled, 52 completed the trial. Permeability at baseline and after albumin soaking was not significantly different. All treatments produced reduced fluid flow through dentin (P > 0.05). All treatments reduced DH significantly (no or moderate sensitivity). Statistical results revealed significant differences among the treatments (P = 0.03). Mann-Whitney comparisons showed GLU, STB < MSC.

Randomized controlled clinical trial on the efficacy of dentin desensitizing agents.

OBJECTIVE: To investigate the effects of four dentin desensitizers on pain reduction in hypersensitive cervical dentin lesions. MATERIALS AND METHODS: The trial was designed as a randomized, controlled, four-arm, single-masked study. Fifty subjects with at least one hypersensitive lesion in each of the four quadrants were allocated. The requested pre-operative pain, determined as a response to 2-s air-blast (AB) and probe scratching (PS), was ≥5 on a VAS scale, 0 = no through to 10 = worst pain. Randomly each subject received each of the four treatments: MS Coat One F (MSC, Sun Medical, Japan), Nanoseal (NAN, Nishin, Japan), Teethmate Desensitizer (TMD, Kuraray Noritake, Japan) and Gluma Desensitizer PowerGel (GLU, HeraeusKulzer, Germany). The investigator assessed blindly the pain response using the two stimuli and recorded the patients' VAS scores before and immediately after application, after 1 week and after 1, 3 and 6 months. STATISTICAL DATA TREATMENT: ANOVA and post-hoc testing (p ≤ 0.05). RESULTS: Forty-nine subjects completed the trial. Pre-operative dentin hypersensitivity (DH) for the groups was not significantly different. All desensitizers reduced DH significantly throughout the 6-months observation. ANOVA revealed significant differences among VAS scores, obtained with the desensitizing agents (p < 0.001). Ranking by post-hoc testing was: MSC > NAN > TMD > GLU (p < 0.05). Upon PS NAN and TMD showed slight but significant regain of sensitivity after 6 months. For GLU PS scores immediately after application and after 6 months were not significantly different, whereas recalls after 1 week, 1 month and 3 months revealed significantly lower scores. CONCLUSION: The calcium phosphate-based TMD and GLU proved highly effective in reducing sensitivity.

Texture of composite resins exposed to two- and three-body wear in vitro.

PURPOSE: To analyze on scanning electron microscopy (SEM) pictures from eight composite resins, taken in the centers of the initial, the middle and the terminal thirds of in vitro produced wear tracks morphological features to explain causative mechanisms for the material wear observed under two- and three-body wear. MATERIALS AND METHODS: In vitro wear behavior of eight composite resins, three conventional and five nanofiller containing marketed products was evaluated using a custom-made Zr-ball-on-disk sliding device. The composite specimens were subjected to 50,000 one-way sliding cycles (1.2 Hz, 50 N load), either simulating two-body wear with water as the intermediate medium or three-body wear using aqueous suspensions of polymethyl methacrylate (PMMA) beads and poppy seeds, respectively. Volume loss of the materials was determined in previous study. Representative specimens were selected for inspection by scanning electron microscopy at 500-fold magnification. From each of the 24 wear tracks microphotographs were taken in the central deepest parts of the initial, middle and terminal thirds of the tracks. RESULTS: For most materials morphological differences were detected depending on the location within the wear track. As a rule, the surface deterioration found increased toward the final part of the wear scar. According to common classification in tribology abrasive wear and fatigue wear, or a combination of both mechanisms were found for all materials tested. Wear was dependent both on the testing mode and on the composition of the individual composite resin material. CONCLUSION: The morphological assessment of wear tracks refects the nature of the abrasive and reveals insight into the mechanism generating wear patterns. Morphological details confirmed abrasive and fatigue-related wear as main failure mechanisms. Selection of food-like slurries as third-body media, such as poppy seed suspension is mandatory to simulate wear of composite restorations in occlusal cavities where three-body wear is the dominating determinant of loss of substance and surface deterioration.

Clinical trial of tooth desensitization prior to in-office bleaching.

The aim of this clinical trial was to compare tooth sensitivity during and after bleaching with hydrogen peroxide gel following application of GLUMA Desensitizer PowerGel or placebo. Forty-six subjects with sound maxillary incisors and canines were enrolled. Tooth shades were determined by comparison with a Vitapan Classic Shade guide. GLUMA Desensitizer PowerGel and placebo were randomly applied to the labial surfaces of the left or right anterior teeth for 1 min, which were then rinsed and dried. Then, Opalescence Boost PF 40% gel was applied onto labial enamel for 15 min. Sensitivity scores [recorded on a 10-point visual-analog scale (VAS)] were determined before, at 5, 10, and 15 min during, and 1, 24, 48 h and 1 wk after, the bleaching treatment. Shades were determined postbleaching and after 1 wk. Prebleaching application of GLUMA Desensitizer PowerGel significantly reduced tooth sensitivity during and after bleaching when compared with treatment with placebo. The whitening effects immediately and 1 wk after bleaching were significant when compared with the prebleaching shades. In conclusion, tooth pretreatment with GLUMA Desensitizer PowerGel for 1 min prior to 15 min of in-office bleaching with 40% hydrogen peroxide gel was highly effective in reducing tooth sensitivity during and after bleaching.

Effects of toothbrush hardness on in vitro wear and roughness of composite resins.

AIM: To investigate and compare the effects of toothbrushes with different hardness on abrasion and surface roughness of composite resins. MATERIALS AND METHODS: Toothbrushes (DENT. EX Slimhead II 33, Lion Dental Products Co. Ltd., Tokyo, Japan) marked as soft, medium and hard, were used to brush 10 beam-shaped specimens of each of three composites resins (Venus [VEN], Venus Diamond [VED] and Venus Pearl [VEP]; HeraeusKulzer) with standardized calcium carbonate slurry in a multistation testing machine (2N load, 60 Hz). After each of five cycles with 10k brushing strokes the wear depth and surface roughness of the specimens were determined. After completion of 50k strokes representative samples were inspected by SEM. Data were treated with ANOVA and regression analyses (p < 0.05). RESULTS: Abrasion of the composite resins increased linearly with increasing number of brushing cycles (r² > 0.9). Highest wear was recorded for VEN, lowest for VED. Hard brushes produced significantly higher wear on VEN and VEP, whereas no difference in wear by toothbrush type was detected for VED. Significantly highest surface roughness was found on VED specimens (Ra > 1.5 µm), the lowest one on VEN (Ra < 0.3 µm). VEN specimens showed increased numbers of pinhole defects when brushed with hard toothbrushes, surfaces of VEP were uniformly abraded without level differences between the prepolymerized fillers and the glass filler-loaded matrix, VED showed large glass fillers protruding over the main filler-loaded matrix portion under each condition. CONCLUSION: Abrasion and surface roughness of composite resins produced by toothbrushing with dentifrice depend mainly on the type of restorative resin. Hardness grades of toothbrushes have minor effects only on abrasion and surface roughness of composite resins. No relationship was found between abrasion and surface roughness. CLINICAL SIGNIFICANCE: The grade of the toothbrush used has minor effect on wear, texture and roughness of the composite resin.

Effects of two topical desensitizing agents and placebo on dentin hypersensitivity.

PURPOSE: To evaluate the efficacy of two commercial desensitizing agents in subjects with moderate to severe dentin hypersensitivity for a period of 6 months and to compare the results with topical application of water as negative control. METHODS: BisBlock (BIS; oxalate) and Gluma Desensitizer PowerGel (GLU; glutaraldehyde/HEMA) were tested. 50 subjects, average age 32.4 years, with at least one cervical hypersensitive incisor, canine or premolar tooth area and pre-operative pain score > or = 6 on VAS from 0 to 10 in each of three quadrants were included. Prior to application of the desensitizing agents or placebo (PLA; water) the sensitive areas were cleaned with prophy paste. Desensitizers were applied according to manufacturers' instructions, the placebo was left for 60 seconds dwell, rinsed off and dried. Pain scores were determined using both evaporative and tactile stimuli immediately after treatment, after 1 day, 1 week, 1, 3 and 6 months. Statistical analyses of the findings were performed using ANOVA and pot-hoc tests with a significance set at P < or = 0.05. RESULTS: All subjects completed the trial. Both the two desensitizing agents and placebo showed significant reduction in sensitivity at baseline and throughout the 6-month evaluation. The effects of the three treatments were significantly different. Pain reduction with GLU was consistently highest, followed by PLA that was significantly greater than BIS. VAS scores for the evaporative stimulus were moderately, but significantly lower than for tactile stimulation.

Comparative evaluation of mechanical characteristics of nanofiller containing resin composites.

PURPOSE: To determine basic mechanical characteristics of six commercially available nanofiller containing resin composites compared to a microhybrid and a microfilled reference material. The tested hypothesis was that there are no differences in mechanical properties between the materials. METHODS: Durafill VS (DUR) and Filtek Z250 (Z250) were used as microfilled and microhybrid references. The nanofiller containing products were: Filtek Supreme XT (FIL), Grandio (GRA), Kalore (KAL), MI Flow (MIF), Tetric EvoCeram (TET), and Venus Diamond (VED). The following material characteristics were determined after 24 hours water storage (n = 6): Flexural strength and modulus (FM), yield stress (0.02%), tensile strength and modulus (TM), diametral tensile strength, Knoop hardness (KHN), and fracture toughness (KIC). RESULTS: The microfilled composite DUR consistently showed the lowest values for each property investigated. The group of nanofiller containing products could be subdivided into two groups: the nanohybrid products GRA and VED and the nanofilled FIL with higher values, on the one hand, and the flowable MIF, and the prepolymer containing composites KAL and TET, on the other. The mechanical performance of the microhybrid reference material Z250 was overall slightly better or in line with the nanohybrid and nanofilled materials. Stringent linear relationships were found between KHN and the moduli FM and TM, respectively (r > 0.95). Linear relations between the other materialvalues investigated were moderate to high.

Effect of spherical silica additions on marginal gaps and compressive strength of experimental glass-ionomer cements.

PURPOSE: To clarify the effects of the addition of silanized (S) and unsilanized (U) spherical silica filler to resin-modified glass-ionomer cement and of powder-liquid ratio on (1) the early marginal gap-width of restorations in both tooth cavities and Teflon molds, (2) the gap-formation of restorations in Class V cavities, and (3) the compressive strength of the cement. METHODS: Resin-modified glass-ionomer powder (Fuji II LC EM, GC) was modified by adding 5 and 10 wt% of powder respectively, of S and U, and then the powder-liquid ratio was increased up to 4.8. Human premolars, extracted for orthodontic reasons, were used for this study. Cylindrical cavities (1.5 mm deep, 3.5 mm in diameter; one cavity was prepared in each tooth in the coronal region and medial surface) were prepared in extracted human premolar teeth and restored with resin-modified glass-ionomer cements. Each restoration margin was inspected immediately after curing and polishing (as the immediate condition was the most severe), the maximum gap-width and the opposing width (if any) were determined microscopically (n = 10). An additional test was conducted in model Class V cavities. After finishing of restorations in model Class V cavities, each tooth was sectioned in a bucco-lingual direction through the center of the restoration, and the presence or absence of gaps along the cavity interface was evaluated (n = 10). Additionally, the maximum marginal gap-width and the opposing-width along margins of restorations in cylindrical Teflon molds were measured (n= 10). The compressive strengths of the restorative materials were determined immediately after light-activation (n = 10). RESULTS: Marginal gap (tooth cavity: 0.32 to 0.25-0.20%, P < 0.05; Teflon cavity: 0.94 to 0.6-0.8%, P < 0.05) and cavity adaptation (no gap in the Class V: 22 to 40-50%, P < 0.05) of the restorations improved with increasing powder-liquid ratio (3.0 to 4.4-4.8) and compressive strength increased (111 to 150-170 MPa, P < 0.05). Highly significant correlation coefficients were found for the relationships between powder-liquid ratio and (1) percentage of marginal gap width in the tooth cavity (r = -0.96, P = 0.002, n = 6), (2) gap-free tooth/cement interfaces (r = 0.90, P = 0.015, n = 6), (3) percentage of marginal gap widths in the Teflon mold (r = 0.98, P = 0.0004, n = 6) and (4) compressive strengths of the cements (r = 0.95, P = 0.004, n = 6).

Surface texture and roughness of polished nanofill and nanohybrid resin composites.

Nanofiller-containing resin composites have gained appreciable market share in dentistry due to their claims of high mechanical strength and low polymerization contraction. In this study, the polishability of one nanofill (Filtek Supreme XT/FIL) and three nanohybrid materials (Grandio/GRA, Tetric EvoCeram/TET, Venus Diamond/VED) was investigated using surface profilometry and SEM. After the specimens were cured under a Mylar strip or pre-ground with 600-grit SiC paper, three polishing systems were applied and their polishing effects compared: diamond polishing points, a diamond paste, and urethane-backed aluminum oxide disks. Except for the profilometry results obtained by glass filler-containing GRA and VED with one polishing system that comprised the consecutive application of diamond particles and a diamond polishing paste, the final roughness (Ra) of all other specimens were lower than the clinically acceptable 0.2 microm threshold. The surface textures of the polished nanofill FIL and nanohybrid TET were uniformly smooth, whereas relief polishing effects and filler extrusion of varying extents were seen on the nanohybrid composites GRA and VED.

Effect of desensitizing agents on dentin permeability.

PURPOSE: To investigate the in vitro efficacy of two dentin desensitizing products at reducing liquid permeability through human dentin discs. The tested hypothesis was that the products, in spite of different chemical mechanisms were not different at reducing or eliminating flow through dentin discs. METHODS: Dentin slices (1 mm thick) were prepared from 16 extracted human third molars and their permeability was indirectly recorded in a split chamber model, using a chemiluminescence technique, after EDTA treatment (control), after soaking with albumin, and after desensitizer application. Two products were studied: MS Coat, a self-curing resin-containing oxalate product, and Gluma Desensitizer, a glutaraldehyde/HEMA-based agent without initiator. The dentin slices were mounted between an upper chamber, filled with an aqueous solution of 1% potassium ferricyanide and 0.3% hydrogen peroxide, and a lower chamber filled with 1% sodium hydroxide solution and 0.02% luminol. The upper solution was pressurized, and upon contact with the luminol solution a photochemical signal was generated and recorded as a measure of permeability throughout two consecutive pressurizing cycles at 2.5 and 13 kPa (26 and 133 cm H2O), respectively. RESULTS: The permeability of the control and albumin-soaked samples was similarly high. After application of the desensitizing agents, dentin permeability was reduced to virtually zero at both pressure levels (P < 0.001).

Effects of opacity and oxygen inhibition of coating resin composites on bond strength to enamel.

The purpose of this in vitro investigation was to study the effects on bond strength to primed human enamel stemming from opacity and polymerization inhibition by oxygen due to two coating resins. The coating resins and primers used were White Coat and an experimental material, SIR. The bond strengths on fine-ground enamel were evaluated for three shades of each of these coating resins after 24-hour storage in water. In addition, their degrees of opacity and oxygen inhibition depths were measured. The mild self-etch primer solutions produced very shallow but distinct etching patterns for micromechanical retention of the coating resin. Significant linear relationships between bond strength on the one hand and opacity and oxygen inhibition depth on the other were found for the three shades of each coating resin. Generally, the bond strength mediated on enamel is sufficiently high when these resins are combined with their proprietary adhesives. Therefore, the decrease in bond strength with increasing opacity of the coating resin shades has to be taken into account during application and light-curing.

Discoloration of coating resins exposed to staining solutions in vitro.

The purpose of this in vitro investigation was to study the effects of coffee and tea immersion on surface discoloration of one commercial temporary resin coating material, White Coat (WHC; Kuraray Medical Inc., Tokyo, Japan), and an experimental one, SI-R20209 (SIR; Shofu Inc., Kyoto, Japan). Disk-shaped specimens were prepared, their colors were determined at baseline, and after immersion in water (control), tea and coffee solutions for 24, 48, and 72 hours. Very little discoloration was found with the water-stored specimens. Staining response was most pronounced after coffee immersion for White Coat and after tea immersion for the experimental material, exceeding the clinically acceptable discoloration threshold value of deltaE=3.3. However, most of the resin shades tested are likely to be sufficiently safe against heavy discoloration when used for short-term restoration only.

Resistance of nanofill and nanohybrid resin composites to toothbrush abrasion with calcium carbonate slurry.

The aim of this study was to investigate the wear of four nanofilled resin composites using simulated toothbrushing for 50,000 cycles with calcium carbonate slurry. The depth of abrasion and roughness (Ra) were measured after each 10,000 brushing cycle. The surface texture of the worn samples was examined by SEM.The wear depths of the nanofill Filtek Supreme XT (FIL), the nanohybrides Grandio (GRA), Tetric EvoCeram (TET), and Venus Diamond (VED) increased linearly with numbers of brushing cycles or approximately 80, 12, 600, and 60 mum, respectively after 50,000 strokes. Surface roughness showed virtually no change between 10,000 and 50,000 brushing cycles; the ranking order was TET < FIL < GRA < VED. FIL showed rather uniform abrasion with nanoclusters protruding from the surface. TET was very smoothly abraded without signs of debonding of the prepolymerized particles, whereas GRA and VED showed pronounced wear of the matrix polymer surrounding larger glass filler particles.

Removal of Invisalign retention attachments: a new minimally invasive method.

Removal of Invisalign resin retention buttons without damaging underlying enamel is a major challenge. To date, the use of tungsten carbide burs is the most common and fastest--yet a risky-ablation method. Stainbuster, a fiber-reinforced resin bur, has been introduced for removal of surface stains and resin remnants from tooth surfaces. This comparative in vitro and in vivo study proved that a combined technique, using multifluted tungsten carbide burs for fast removal of the bulk of resin followed by Stainbuster grinding for gentle removal of the final resin layer, is a safe and minimally invasive procedure for removing composite buttons from enamel.

Effect of artificial saliva on permeability of dentin treated with phosphate containing desensitizer measured by digital flow meter.

The aim of this study was to investigate the effects of artificial saliva on permeability measured using a highly sensitive digital flow meter of dentin discs treated with a phosphate containing desensitizer compound (Teethmate desensitizer; TD). Four random groups (n=10) were treated either with TD or distilled water (DW), then stored in artificial saliva (AS) or DW for 1 day, 1 week and 1 month. Flow rates under 2 kPa pressure were calculated as percentage reduction (PR%) from the baseline. The PR% of TD/AS group was significantly lower after 1 day and 1 week, but the PR%s of 1 month groups among TD/AS, TD/DW and DW/AS were not significantly different. The SEM photograph of TD/AS group displayed that the dentin surface was densely covered with mineral deposits. Ca and phosphate ions from the artificial saliva could penetrate into the tubules and precipitate as hydroxyapatite, resulting in the reduction in permeability.

Sulcus reproduction with elastomeric impression materials: a new in vitro testing method.

OBJECTIVES: Aim of this study was to investigate the depth reproduction of differently wide sulci with elastomeric impression materials by single- and double-mix techniques using a tooth and sulcus model, simulating clinical conditions. METHODS: Impressions with one vinyl polysiloxane (VPS; FLE), two polyethers (PE; IMP and P2), and one hybrid VPS/PE elastomer (FUS) were taken from a truncated steel cone with a circumferential 2 mm deep sulcus, 50, 100 or 200 microm wide. The "root surface" was in steel and the "periodontal tissue" in reversible hydrocolloid. Single-mix impressions were taken with light-body (L) or monophase (M) pastes, double-mix impressions with L as syringe and M or heavy-body (H) as tray materials (n=8). Sulcus reproduction was determined by 3D laser topography of impressions at eight locations, 45 degrees apart. Statistical data analysis by ANOVA and multiple comparison tests (p<0.05). RESULTS: For 200 microm wide sulci, significant differences were found between impression materials only: FLE=IMP>FUS=P2. At 50 and 100 microm width, significant differences were found between materials (IMP>FUS=FLE>P2) and techniques (L+H=L+M>M>L). SIGNIFICANCE: The sulcus model is considered useful for screening evaluation of elastomeric impression materials ability to reproduce narrow sulci. All tested materials and techniques reproduced 200 microm wide sulci to almost nominal depth. Irrespective of the impression technique used, IMP showed the best penetration ability in 50 and 100 microm sulci. Double-mix techniques are more suitable to reproduce narrow sulci than single-mix techniques.

All-in-one self-etch model adhesives: HEMA-free and without phase separation.

OBJECTIVE: Aim of this study was to design HEMA-free all-in-one self-etch model adhesives without phase separation, and to investigate their efficiency on extracted human teeth. MATERIALS AND METHODS: Compositions of adhesives in mass% (1): UDMA (25), 4-META (20), H(2)O (0, 1, 2, 5, 10, 20, 35, and 45), balance of acetone or ethanol. (2): UDMA (35), 4-META or 4-MET (28), H(2)O (0, 2, 4, 5, 6, and 8), balance of acetone. Phase separation was evaluated on samples exposed to ambient atmosphere. Conventional shear bond strengths (SBS, n=8) were determined on human enamel and dentin. Marginal adaptation (MGW, n=8) was assessed in cylindrical butt-joint dentin cavities. RESULTS: Solutions (1) and (2) with 5 and 8% or less water content, respectively, showed no phase separation. SBSs on enamel were not different within the acetone- or ethanol-group and between the adhesive groups (1). Water content of adhesives (2) was a significant determinant of enamel SBSs, groups with 4-META or 4-MET were not different (p>0.05). Dentin SBSs with adhesives (1) were not different (p>0.05) within solvent groups, yet higher for acetone-dissolved adhesives (p<0.05). Dentin SBSs with adhesives (2) were different by water content and functional monomer (p<0.05). MGW for solutions (1) were smaller with acetone-dissolved than with ethanol-dissolved adhesives (p<0.001). Acetone solutions between 2 and 45% water content produced almost perfect marginal adaptation. Marginal adaptation of adhesives (2) was almost perfect at 5 through 8% water content. CONCLUSIONS: Simplified HEMA-free self-etch adhesives without phase separation were prepared without compromises on bonding efficiency to enamel and dentin.

Shark fin test and impression quality: a correlation analysis.

OBJECTIVES: To evaluate the correlation between the shark fin test and the dimensional accuracy of impressions, surface detail reproduction of impressions and rheological properties of impression materials within the manufacturer's recommended working time. METHODS: Four chemically different types of impression material (Flexitime: VPS; Fusion: Polyether/VPS blend; Impregum: classical Polyether; P2: new Polyether) were subjected to the shark fin test as well as three other test regimes. Dimensional accuracy was determined as being the discrepancy in diameter between a steel master cone and stone dies poured from impressions taken from the steel master cone at defined 30s intervals after mixing within the manufacturer's recommended working time. Surface detail reproduction was calculated as being the difference in average arithmetic roughness (Ra) between a ground dentin surface and the corresponding area of the impressions, taken at the same 30s intervals. Phase angle and storage modulus were measured using a rotational rheometer. Spearman's Rho was used for correlation analysis. RESULTS: With respect to the majority of impression materials used, significant correlations mainly exist between shark fin test data, phase angle and storage modulus. No correlation was found between the results of the shark fin test versus dimensional accuracy, respectively, surface detail reproduction. CONCLUSIONS: Results obtained from the shark fin test within the manufacturer's recommended working time do not allow predictions regarding the dimensional accuracy or surface detail reproduction of impressions as clinically relevant material characteristics.

Interactions of self-etch adhesives with resin composites.

OBJECTIVE: Aim of this in vitro study was to investigate the correlation of shear bond strength and marginal cavity adaptation, together with polymerization shrinkage and contraction stress, using the combination of four self-etch adhesives and three resin composites. MATERIALS AND METHODS: Interactions were studied between one two-step and three one-step adhesives, and the hybrid-type resin composites, Beautifil (BEU, Shofu) and Venus (VEN, Heraeus), and an experimental nano-hybrid resin composite NEUN (NEU, Heraeus). For all 12 combinations shear bond strengths (SBS) were determined on human dentin. Marginal adaptation (MGW) was assessed in cylindrical butt-joint dentin cavities. Further, polymerization contraction and contraction stress of the resin restoratives were measured. RESULTS: Significant determinants of SBSs on dentin were time of testing (10min or 24h) and adhesives (p<0.001). Marginal adaptation was best for NEU, followed by VEN and BEU. Only the resin composite used was a highly significant determinant of cavity adaptation. Polymerization shrinkage after 5min was 2.58, 2.74, and 1.53% for BEU, VEN, and NEU, respectively. Polymerization contraction stresses were largest for BEU, less for VEN, and smallest for NEU (p<0.05). CONCLUSIONS: No correlation was found between bond strength and marginal cavity adaptation. In contrast, reduced shrinkage and low polymerization contraction stress of resin composites were identified as important determinants of marginal cavity adaptation.