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Spectrochim Acta A Mol Biomol Spectrosc ; 251: 119426, 2021 Apr 15.
Artigo em Inglês | MEDLINE | ID: mdl-33485242

RESUMO

A method is described using rapid and sensitive Fourier transform near-infrared spectroscopy combined with Gas Chromatograpy internal standard method detection for the simultaneous identification and determination of three bioactive compounds in Amomum villosum samples. Partial least squares regression is selected as the analysis type and multiplicative scatter correction, second derivative, and SNV were adopted for the spectral pretreatment. The correlation coefficients (R) of the calibration models were above 0.95 and the root mean square error of predictions were under 0.8. The developed models were applied to unknown samples with satisfantory results. The established method was validated and can be applied to the intrinsic quality control of Amomum villosum.


Assuntos
Amomum , Calibragem , Análise de Fourier , Análise dos Mínimos Quadrados , Espectroscopia de Infravermelho com Transformada de Fourier , Espectroscopia de Luz Próxima ao Infravermelho
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