RESUMO
Permittivity of materials is of utmost importance for microwave applicators' design and to predict high-frequency dielectric heating of materials. In the case of aromatic plant biomass, however, there are few data that help researchers design microwave applicators for microwave-assisted extraction. In this work, the permittivity of cypress and rockrose biomass samples were measured versus temperature, density, and moisture content. A resonant technique based on a coaxial bi-reentrant microwave cavity was employed to obtain the complex permittivity of biomass samples as a function of those magnitudes around the 2.45 GHz ISM frequency. The obtained measurements show that large variations for permittivity values can be found with moisture content and density changes for both cypress and rockrose biomass. Temperature also has effects in a lesser degree, although it has an important influence on the cypress biomass loss factor. Polynomial expressions fitting the experimental data were provided in order to facilitate the estimation of intermediate values, which were not explicitly arranged in this work. As a general trend, the permittivity of cypress and rockrose biomass increases with increasing values of moisture content and density, whereas the biomass loss factor increases when temperature rises.
Assuntos
Cupressus , Biomassa , Micro-Ondas , TemperaturaRESUMO
BACKGROUND: The heating of a green smoothie during an innovative semi-continuous microwave treatment (MW; 9 kW for 15 s) was modelled. Thermal and dielectric properties of the samples were previously determined. Furthermore, the heating effect on the main chemopreventive compounds of the smoothie and during its subsequent storage up to 30 days at 5 or 15 °C were studied. Such results were compared to conventional pasteurisation (CP; 90 °C for 45 s) while unheated fresh blended samples were used as the control. RESULTS: A procedure was developed to predict the temperature distribution in samples inside the MW oven with the help of numerical tools. MW-treated samples showed the highest sulforaphane formation after 20 days, regardless of the storage temperature, while its content was two-fold reduced in CP samples. Storage of the smoothie at 5 °C is crucial for maximising the levels of the bioactive compound S-methyl cysteine sulfoxide. CONCLUSION: The proposed MW treatment can be used by the food industry to obtain an excellent homogeneous heating of a green smoothie product retaining high levels of bioactive compounds during subsequent retail/domestic storage up to 1 month at 5 °C. © 2017 Society of Chemical Industry.
Assuntos
Cisteína/análogos & derivados , Manipulação de Alimentos/métodos , Sucos de Frutas e Vegetais/análise , Sucos de Frutas e Vegetais/efeitos da radiação , Frutas/química , Glucosinolatos/química , Imidoésteres/química , Isotiocianatos/química , Verduras/química , Cor , Cisteína/química , Armazenamento de Alimentos , Temperatura Alta , Micro-Ondas , Oximas , SulfóxidosRESUMO
Fabric permittivity is critical for the manufacturing of wearable sensors and antennas as well as predicting how fabrics interact with electromagnetic fields. Engineers should also understand how permittivity changes under different temperatures, densities, and moisture content values, or when several fabrics are mixed in aggregates, when designing future applications such as microwave dryers. The permittivity of cotton, polyester, and polyamide fabric aggregates is investigated in this paper for a wide range of compositions, moisture content levels, density values, and temperature conditions around the 2.45 GHz ISM band using a bi-reentrant resonant cavity. The obtained results show extremely comparable responses for all characteristics investigated for single and binary fabric aggregates. Permittivity always increases as temperature, density, or moisture content levels rise. Moisture content is the most influential characteristic, causing enormous variations in the permittivity of aggregates. Fitting equations are supplied for all data, with exponential functions used to accurately model variation in temperature and polynomial functions employed to precisely model density and moisture content variations with low error levels. The temperature permittivity dependence of single fabrics without the influence of air gaps is also extracted from fabric and air aggregates by using complex refractive index equations for two-phase mixtures.