Alignment-free twisted-split-ring metasurface on single substrate with 2π phase range for linearly polarized sub-terahertz wave.

To achieve high-speed, large-capacity communication, next-generation mobile communication systems will require manipulation of the propagation of sub-terahertz waves in the propagation channel. In this paper, we propose the use of a novel split-ring resonator (SRR) structure as a metasurface unit cell for manipulating the linearly polarized incident and transmission waves used in mobile communication systems. In this SRR structure, the gap is twisted by 90° to efficiently use cross-polarized scattered waves. By changing the twist direction and gap size of the unit cell, 2π phase designability can be achieved, which enables linear polarization conversion efficiencies of -2 dB with a backside polarizer and -0.2 dB with two polarizers. In addition, a complementary pattern of the unit cell was fabricated, and a measured conversion efficiency of more than -1 dB at the peak with only the backside polarizer on a single substrate was verified. In the proposed structure, the 2π phase designability and efficiency gain are obtained independently by the unit cell and polarizer, respectively, thus enabling alignment-free characteristics, which are highly advantageous from an industrial viewpoint. Metasurface lenses with binary phase profiles of 0 and π were fabricated using the proposed structure with a backside polarizer on a single substrate. The lenses' focusing, deflection, and collimation operations were experimentally verified with a lens gain of 20.8 dB, which agreed well with our calculated results. Our metasurface lens has the great advantages of easy fabrication and implementation, and it has the potential to enable dynamic control by combining it with active devices because of the simple design methodology, which entails only changing the twist direction and the gap's capacitance component.

Analysis of Asymmetry in Active Split-Ring Resonators to Design Circulating-Current Eigenmode: Demonstration of Beamsteering and Focal-Length Control toward Reconfigurable Intelligent Surface.

In this work, toward an intelligent radio environment for 5G/6G, design methodologies of active split-ring resonators (SRRs) for more efficient dynamic control of metasurfaces are investigated. The relationship between the excitation of circulating-current eigenmode and the asymmetric structure of SRRs is numerically analyzed, and it is clarified that the excitation of the circulating-current mode is difficult when the level of asymmetry of the current path is decreased by the addition of large capacitance such as from semiconductor-based devices. To avoid change in the asymmetry, we incorporated an additional gap (slit) in the SRRs, which enabled us to excite the circulating-current mode even when a large capacitance was implemented. Prototype devices were fabricated according to this design methodology, and by the control of the intensity/phase distribution, the variable focal-length and beamsteering capabilities of the transmitted waves were demonstrated, indicating the high effectiveness of the design. The presented design methodology can be applied not only to the demonstrated case of discrete varactors, but also to various other active metamaterials, such as semiconductor-integrated types for operating in the millimeter and submillimeter frequency bands as potential candidates for future 6G systems.

Shape-dependent infrared reflectance properties of CNT forest metamaterial arrays.

In this work, shape-dependent mid-infrared properties of novel split ring resonator (SRR) metamaterials composed of single-walled carbon nanotube (CNT) forest are investigated. The introduction of the gap and dip shape to the closed ring geometry reduced the total reflectance by 15%, due to the generation of circular currents and LC resonances in SRRs. The increase of the SRR height reduced the total IR reflectance by 25%. Unique one-dimensional anisotropic electric and photonic properties of CNTs, combined with an artificial refractive index induced in SRR circuits, will stimulate the development of new optoelectronics applications.

Fabrication of Self-Assembling Carbon Nanotube Forest Fishnet Metamaterials.

The investigation of the preparation of polystyrene (PS) nanosphere monolayers for the fabrication of carbon nanotube (CNT) forest fishnet metamaterial structures is studied in this paper, as a cheap alternative for top-down patterning methods. The precise control of dry etching conditions resulted in a highly controlled diameter of PS nanobeads, which were then used as a shadow mask for CNT fishnet preparation. The change of the size of the holes from 370 nm to 665 nm resulted in a gradual change of the CNT morphology from multi-walled to single-walled CNTs. The ultraviolet-visible (UV-Vis) reflectance spectra showed that the variation of the hole diameter resulted in the nonlinear light absorption in CNT fishnets that caused the change of the resonance frequency. The change of the fishnet wire width (inductance) and the hole size (capacitance) resulted in the blueshift of the broadband resonance frequency peak. The presented work has a significant potential to allow for the large-scale fabrication of CNT-based fishnet metamaterial structures for applications in energy harvesting, energy storage, solar cells, or optoelectronic devices, such as neuromorphic networks.

FIB Secondary Etching Method for Fabrication of Fine CNT Forest Metamaterials.

Anisotropic materials, like carbon nanotubes (CNTs), are the perfect substitutes to overcome the limitations of conventional metamaterials; however, the successful fabrication of CNT forest metamaterial structures is still very challenging. In this study, a new method utilizing a focused ion beam (FIB) with additional secondary etching is presented, which can obtain uniform and fine patterning of CNT forest nanostructures for metamaterials and ranging in sizes from hundreds of nanometers to several micrometers. The influence of the FIB processing parameters on the morphology of the catalyst surface and the growth of the CNT forest was investigated, including the removal of redeposited material, decreasing the average surface roughness (from 0.45 to 0.15 nm), and a decrease in the thickness of the Fe catalyst. The results showed that the combination of FIB patterning and secondary etching enabled the growth of highly aligned, high-density CNT forest metamaterials. The improvement in the quality of single-walled CNTs (SWNTs), defined by the very high G/D peak ratio intensity of 10.47, demonstrated successful fine patterning of CNT forest for the first time. With a FIB patterning depth of 10 nm and a secondary etching of 0.5 nm, a minimum size of 150 nm of CNT forest metamaterials was achieved. The development of the FIB secondary etching method enabled for the first time, the fabrication of SWNT forest metamaterials for the optical and infrared regime, for future applications, e.g., in superlenses, antennas, or thermal metamaterials.