Temperature Rise of an Adhesive Particle-Reinforced Polymer during Fatigue Testing.

Construction adhesives are usually polymers that have been modified to achieve specific properties so that they can be used under various loading conditions. An attempt was made to estimate the effect of fatigue loading on the temperature of an adhesive material by further physically modifying the basic adhesive composition used in the research. The temperature of the materials during the tests was recorded using a thermal imaging camera and a thermoelectric thermometer. For most materials tested at 20 Hz, an increase in the number of load cycles corresponded to an increase in the temperature of the samples. For a frequency of 30 Hz, after the temperature increased by a certain value, the temperature of the modified samples recorded with the thermal imaging camera decreased. Fatigue loading caused an increase of the temperature of all tested polymeric materials. Observation of the sample during testing with a thermal imaging camera allows a simple identification of the areas with the highest temperature and can be much more useful in practice than recording temperatures with a thermocouple thermometer, as thermocouples need to be properly positioned before testing.

The Influence of Low-Energy Impact Loads on the Properties of the Sandwich Composite with a Foam Core.

Composite materials are widely used in the construction of means of transport. Due to their low density and high stiffness, sandwich composites generate significant interest. The authors conducted static and dynamic tests in order to determine the effect of density and core thickness on the mechanical properties of a sandwich composite. Particular attention was paid to the impact properties of such composites. Herex and Airex polymer foams of different densities were used as cores, whereas the faces were made up of two layers of fabrics: glass and carbon. The matrix base of the tested materials was made of epoxy resin cured with a dedicated hardener. As a result of the study, a significant influence of the core on the strength parameters of the tested spacer materials was found. The examined polymer foams were found to have different adhesive properties, which affected their residual strength after an impact and the nature of destruction of the studied composites. It was observed that sandwich composites with a thicker core of higher density have higher impact strength and resistance to puncture. In the sandwich composites, low-energy impact loads result in damage only to the layer to which the load has been applied and has a core, so repairing such an element is much easier than in classic layered composites without a core. What is very important is that, in contrast to classic laminates, the bottom cover of the composite is not destroyed at low-impact energy values.

Mechanical Properties of Bio-Composites Based on Epoxy Resin and Nanocellulose Fibres.

The aim of our research was to investigate the effect of a small nanocellulose (NC) addition on an improvement of the mechanical properties of epoxy composites. A procedure of chemical extraction from pressed lignin was used to obtain nanocellulose fibers. The presence of nanoparticles in the cellulose pulp was confirmed by FTIR/ATR spectra as well as measurement of nanocellulose particle size using a Zetasizer analyzer. Epoxy composites with NC contents from 0.5% to 1.5% w/w were prepared. The obtained composites were subjected to strength tests, such as impact strength (IS) and resistance to three-point bending with a determination of critical stress intensity factor (Kc). The impact strength of nanocellulose composites doubled in comparison to the unmodified epoxy resin (EP 0). Moreover, Kc was increased by approximately 50% and 70% for the 1.5 and 0.5% w/w NC, respectively. The maximum value of stress at break was achieved at 1% NC concentration in EP and it was 15% higher than that for unmodified epoxy resin. The highest value of destruction energy was characterized by the composition with 0.5% NC and corresponds to the increase of 102% in comparison with EP 0. Based on the analysis of the results it was noted that satisfactory improvement of the mechanical properties of the composite was achieved with a very small addition of nanofiller while other research indicates the need to add much more nanocellulose. It is also expected that this kind of use of raw materials will allow increasing the economic efficiency of the nanocomposite preparation process. Moreover, nanocomposites obtained in this way can be applied as elements of machines or as a modified epoxy matrix for sandwich composites, enabling production of the structure material with reduced weight but improved mechanical properties.