Infill Density Influence on Mechanical and Thermal Properties of Short Carbon Fiber-Reinforced Polyamide Composites Manufactured by FFF Process.

In three-dimensional (3D) printing, one of the main parameters influencing the properties of 3D-printed materials is the infill density (ID). This paper presents the influence of ID on the microstructure, mechanical, and thermal properties of carbon fiber-reinforced composites, commercially available, manufactured by the Fused Filament Fabrication (FFF) process. The samples were manufactured using FFF by varying the infill density (25%, 50%, 75%, and 100%) and were subjected to tensile tests, three-point bending, and thermal analyses by Differential Scanning Calorimetry (DSC) and Thermogravimetric Analysis (TGA). It was shown that the samples with 100% ID had the highest values of both tensile, 90.8 MPa, and flexural strengths, 114 MPa, while those with 25% ID had the lowest values of 56.4 MPa and 62.2 MPa, respectively. For samples with infill densities of 25% and 50%, the differences between the maximum tensile and flexural strengths were small; therefore, if the operating conditions of the components allow, a 25% infill density could be used instead of 50%. After DSC analysis, it was found that the variation in the ID percentage determined the change in the glass transition temperature from 49.6 °C, for the samples with 25% ID, to 32.9 °C, for those with 100% ID. TGA results showed that the samples with IDs of 75% and 100% recorded lower temperatures of onset degradation (approximately 344.75 °C) than those with infill densities of 25% and 50% (348.5 °C, and 349.6 °C, respectively).

Fused Filament Fabrication of Short Glass Fiber-Reinforced Polylactic Acid Composites: Infill Density Influence on Mechanical and Thermal Properties.

Fused Filament Fabrication (FFF) is one of the frequently used material extrusion (MEX) additive manufacturing processes due to its ability to manufacture functional components with complex geometry, but their properties depend on the process parameters. This paper focuses on studying the effects of process parameters, namely infill density (25%, 50%, 75%, and 100%), on the mechanical and thermal response of the samples made of poly(lactic acid) (PLA) reinforced with short glass fibers (GF) produced using FFF process. To perform a comprehensive analysis, tensile, flexural, compression, differential scanning calorimetry (DSC), and thermal gravimetric analysis (TGA) tests were used. The paper also aims to manufacture by FFF process of composite structures of the fuselage section type, as structural elements of an unmanned aerial vehicle (UAV), and their testing to compression loads. The results showed that the tensile, flexural and compression strength of the additive manufactured (AMed) samples increased with the increase of infill density and therefore, the samples with 100% infill density provides the highest mechanical characteristics. The AMed samples with 50% and 75% infill density exhibited a higher toughness than samples with 100% infill. DSC analyses revealed that the glass transition (Tg), and melting (Tm) temperature increases slightly as the infill density increases. Thermogravimetric analyses (TGA) show that PLA-GF filament loses its thermal stability at a temperature of about 311 °C and the increase in fill density leads to a slight increase in thermal stability and the complete degradation temperature of the AMed material. The compression tests of the fuselage sections manufactured by FFF made of PLA-GF composite showed that their stiffening with stringers oriented at an angle of ±45° ensures a higher compression strength than the stiffening with longitudinal stringers.

Compression and Bending Properties of Short Carbon Fiber Reinforced Polymers Sandwich Structures Produced via Fused Filament Fabrication Process.

Additive manufacturing, through the process of thermoplastic extrusion of filament, allows the manufacture of complex composite sandwich structures in a short time with low costs. This paper presents the design and fabrication by Fused Filament Fabrication (FFF) of composite sandwich structures with short fibers, having three core types C, Z, and H, followed by mechanical performance testing of the structures for compression and bending in three points. Flatwise compression tests and three-point bending have clearly indicated the superior performance of H-core sandwich structures due to dense core structures. The main modes of failure of composite sandwich structures were analyzed microscopically, highlighting core shear buckling in compression tests and face indentation in three-point bending tests. The strength-mass ratio allowed the identification of the structures with the best performances considering the desire to reduce the mass, so: the H-core sandwich structures showed the best results in compression tests and the C-core sandwich structures in three-point bending tests. The feasibility of the FFF process and the three-point bending test of composite wing sections, which will be used on an unmanned aircraft, have also been demonstrated. The finite element analysis showed the distribution of equivalent stresses and reaction forces for the composite wing sections tested for bending, proving to validate the experimental results.