Bending properties and damage evolution of fiber-reinforced aeolian sand backfill materials.

Backfilling is a promising measure for controlling surface subsidence in mined-out areas and disposing solid wastes from the mineral processing, there are increasing demands of enhanced toughness and anti-cracking properties of backfill materials to prolong the service life under the complex loads. In this study, polypropylene (PP) fibers were employed to improve performance of backfills, four-point bending and uniaxial compression tests were conducted to investigate the failure process and damage evolution of fiber-reinforced aeolian-sand backfill materials (FABs) using Digital Image Correlation (DIC) and Acoustic Emission (AE) techniques. The results show that the compressive strength tends to decrease with the increasing fiber volume fractions, while the four-point bending strength shows a tendency to increase initially and then decrease, and the optimum volume fraction of PP fiber is 0.6%. At the optimal fiber volume fraction, PP fibers with lengths of 3 mm and 9 mm resulted in a 65.25% and 81.62% increase in the four-point bending strength of FABs, respectively. As indicated by DIC measurements, PP fibers with a length of 9 mm were more effective in controlling the horizontal and vertical displacements of FABs under four-point bending loads than that of 3 mm, and the cracks developed more slowly at the same deflection. In addition, PP fibers with a length of 9 mm have stronger crack extension delay characteristics due to longer effective anchorage distance, as evidenced by more frequent acoustic emission ringing counts and higher cumulative ringing counts. The results of the study may provide a theoretical basis for the application of FABs materials in backfilling.

Mechanical Properties and Microstructural Features of Biomass Fly Ash-Modified Self-Compacting Coal Gangue-Filled Backfill.

To achieve sustainable utilization of a large amount of mine solid waste, this study investigated the performance of self-compacting coal gangue-filled backfill (SCFB) containing biomass fly ash (BFA) generated from biomass power plants as a supplementary cementitious material (SCM). The correlations between the physical structure and compressive strength of SCFB samples were obtained by ultrasonic pulse velocity (UPV). The failure process of the SCFB samples was monitored by the digital image correlation (DIC) technique, and the stress-strain relationship and failure pattern were also analyzed. The micro-morphological structure and hydration products of SCFB samples were evaluated by X-ray diffraction (XRD), scanning electron microscopy (SEM), and backscattered electron imaging (SEM-BSE). The results show that the usage of 30~40% BFA in SCFB improves the physical structure and strength of the samples. The compressive strength and UPV value of SCFB samples with different water-to-cement (w/c) ratios showed a similar trend of increasing and then gradually decreasing as the proportion of ordinary Portland cement (OPC) replaced by BFA increased. BFA exhibits better reactivity and filling effect in SCFB samples with a high w/c ratio. The peak stress of SCFB samples gradually decreases, and resistance to deformation gradually weakens with the increase in w/c ratios, while the DIC results further verify the mechanical experimental results. Microstructural analysis revealed that reducing the w/c ratio and incorporating specific ratios of BFA can reduce the thickness of the interface transition zone (ITZ) and porosity. The results of the study will provide theoretical guidance for the modification, stability monitoring, and strengthening of SCFB.

The Role of Rheological Additives on Fresh and Hardened Properties of Cemented Paste Backfill.

Cemented paste backfill (CPB) has become a significant structural material in most mines across the world. In this study, the effects of chemical rheological additives including viscosity modifying agent (i.e., polyacrylamide) and polycarboxylate superplasticizer (PCE) on fresh and hardened properties of CPB with different water-to-solid (W/S) ratios and water-to-cement (W/C) ratios were investigated. The microstructure of CPB specimens was also characterized by X-ray diffraction (XRD), thermogravimetric analysis (TGA), scanning electron microscopy (SEM), and backscattered electron image (SEM-BSE). The obtained results indicate that PAM (polyacrylamide) dosage and W/S are the most significant parameters influencing the workability of fresh CPB mixtures. For the hardened CPB specimens, the decreasing W/S ratio leads to higher flexural and compressive strength values and lower dry shrinkage strains. The interfacial transition zone (ITZ) between the cement matrix and the tailings sand was also observed to be narrower, with fewer micro cracks and capillary pores. Meanwhile, the existence of PAM decreased the number of hydration products and retarded the hydration reaction. Overall, the CPBs with high W/C ratios (i.e., 1.0 and 1.2), low W/S ratios (i.e., 0.3), and moderate amounts of rheological additives (i.e., 0.05% PAM and 1.0% PCE) have excellent fresh and hardened properties. The findings of this study contribute to better optimization of CPB mixtures in backfill construction, bringing benefits of low costs and low environmental impacts.

Factors Influencing the Properties of Extrusion-Based 3D-Printed Alkali-Activated Fly Ash-Slag Mortar.

The mix proportioning of extrusion-based 3D-printed cementitious material should balance printability and hardened properties. This paper investigated the effects of three key mix proportion parameters of 3D-printed alkali-activated fly ash/slag (3D-AAFS) mortar, i.e., the sand to binder (s/b) ratio, fly ash/ground granulated blast-furnace slag (FA/GGBS) ratio, and silicate modulus (Ms) of the activator, on extrudability, buildability, interlayer strength, and drying shrinkage. The results showed that the loss of extrudability and the development of buildability were accelerated by increasing the s/b ratio, decreasing the FA/GGBS ratio, or using a lower Ms activator. A rise in the s/b ratio improved the interlayer strength and reduces the drying shrinkage. Although increasing the FA/GGBS mass ratio from 1 to 3 led to a reduction of 35% in the interlayer bond strength, it decreased the shrinkage strain by half. A larger silicate modulus was beneficial to the interlayer bond strength, but it made shrinkage more serious. Moreover, a simple centroid design method was developed for optimizing the mix proportion of 3D-AAFS mortar to simultaneously meet the requirements of printability and hardened properties.