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1.
Small ; : e2308491, 2023 Dec 06.
Artigo em Inglês | MEDLINE | ID: mdl-38054766

RESUMO

Developing desirable sensors is crucial for underwater perceptions and operations. The perceiving organs of marine creatures have greatly evolved to react accurately and promptly underwater. Inspired by the fish lateral line, this study proposes a triboelectric dynamic pressure sensor for underwater perception. The biomimetic lateral line sensor (BLLS) has high sensitivity to the disturbance amplitude/frequency, good adaptability to underwater environments and (relative) low cost. The sensors are deployed at the bottom of the test basin to perceive various moving objects, such as a robotic fish, robotic seal, etc. By analyzing the electrical signal of the sensor, the motion parameters of the objects passed over can be obtained. By monitoring signal variations across multiple sensors, the ability to sense different disturbance movement trajectories, including linear and angular trajectories, is achievable. The study will prove significant in forming an unconventional underwater perceiving method, which can back-up the sonic/optical sensors when are impaired in complex underwater environments.

2.
J Appl Biomech ; 39(2): 90-98, 2023 Apr 01.
Artigo em Inglês | MEDLINE | ID: mdl-36848903

RESUMO

This study aims to investigate the difference in hand acceleration induced by rapid changes in hand movement directions and propulsion between fast and slow groups of swimmers during front crawl swimming. Twenty-two participants, consisting of 11 fast and 11 slow swimmers, performed front crawl swimming at their maximal effort. Hand acceleration and velocity and the angle of attack were measured using a motion capture system. The dynamic pressure approach was used to estimate hand propulsion. In the insweep phase, the fast group attained significantly higher hand acceleration than the slow group in the lateral and vertical directions (15.31 [3.44] m·s-2 vs 12.23 [2.60] m·s-2 and 14.37 [1.70] m·s-2 vs 12.15 [1.21] m·s-2), and the fast group exerted significantly larger hand propulsion than the slow group (53 [5] N vs 44 [7] N). Although the fast group attained large hand acceleration and propulsion during the insweep phase, the hand velocity and the angle of attack were not significantly different in the 2 groups. The rapid change in hand movement direction could be considered in the technique of underwater arm stroke, particularly in the vertical direction, to increase hand propulsion during front crawl swimming.


Assuntos
Mãos , Natação , Humanos , Fenômenos Biomecânicos , Extremidade Superior , Movimento
3.
Sensors (Basel) ; 22(15)2022 Jul 27.
Artigo em Inglês | MEDLINE | ID: mdl-35957179

RESUMO

In order to study the characteristics of pressure fluctuation during unstable combustion, experimental studies had been conducted on the mechanism model of the swirl combustor and the industrial swirl combustor. The signal of dynamic pressure, heat release rate, and the high-speed flame image in the two combustors were synchronously collected by using dynamic pressure sensors, a photoelectric sensor, and a high-speed camera under normal temperature and pressure. After empirical mode decomposition of the dynamic pressure signal, several intrinsic mode functions were obtained. It was found that the pressure pulsation energy is concentrated in the first three order intrinsic mode function. Through fast Fourier transform spectrum calculation, it was found that the first three order intrinsic mode function pulsation can characterize the changes of heat release rate and air flow pulsation under cold state and flame instability. It showed that the decomposition of the dynamic pressure in the combustor by this method can obtain the main physical processes in its connotation, and provide data processing methods for the induction mechanism of oscillating combustion and combustion diagnosis in an industrial combustor test.

4.
Sensors (Basel) ; 22(22)2022 Nov 10.
Artigo em Inglês | MEDLINE | ID: mdl-36433271

RESUMO

To control the problem of coal wall spalling in large mining height working faces subject to mining, considering the Duanwang Mine 150505 fully mechanized working face, the mechanism of coal wall spalling in working faces was investigated by theoretical analysis, numerical simulation and field experiment. Based on analysis of coal wall spalling in the working face, a new grouting material was developed. The stress and plastic zone changes affecting the coal wall, before and after grouting in the working face, were analyzed using numerical simulation and surrounding rock grouting reinforcement technology was proposed for application around the new grouting material. The results showed that: (1) serious spalling of the 150505 working face was caused by the large mining height, fault influence and low roof strength, and (2) the new nano-composite low temperature polymer materials used have characteristics of rapid reaction, low polymerization temperature, adjustable setting time, high strength and environmental protection. Based on analysis of the working face coal wall spalling problem, grouting reinforcement technology based on new materials was proposed. Industrial tests were carried out on the working face. Field monitoring showed that the stability of the working face coal wall was significantly enhanced and that rib spalling was significantly improved after comprehensive anti-rib-spalling grouting measures were adopted. These results provide a basis for rib spalling control of working faces under similar conditions.


Assuntos
Minas de Carvão , Carvão Mineral , Tecnologia , Simulação por Computador
5.
Sensors (Basel) ; 21(13)2021 Jun 29.
Artigo em Inglês | MEDLINE | ID: mdl-34210071

RESUMO

Accurate dynamic pressure measurements are increasingly important. While traceability is lacking, several National Metrology Institutes (NMIs) and calibration laboratories are currently establishing calibration capacities. Shock tubes generating pressure steps with rise times below 1 µs are highly suitable as standards for dynamic pressures in gas. In this work, we present the results from applying a fast-opening valve (FOV) to a shock tube designed for dynamic pressure measurements. We compare the performance of the shock tube when operated with conventional single and double diaphragms and when operated using an FOV. Different aspects are addressed: shock-wave formation, repeatability in amplitude of the realized pressure steps, the assessment of the required driver pressure for realizing nominal pressure steps, and economy. The results show that using the FOV has many advantages compared to the diaphragm: better repeatability, eight times faster to operate, and enables automation of the test sequences.

6.
Sensors (Basel) ; 21(14)2021 Jul 14.
Artigo em Inglês | MEDLINE | ID: mdl-34300539

RESUMO

In various domains of material processing, such as surface cleaning and surface treatment, cavitation phenomenon may become an alternative to traditional methods if this phenomenon is well understood. Due to experimental and mathematical difficulties in theoretical models, it is still a challenge to accurately measure the physical mechanism of the fluid/structure interactions. In this study, we verified the feasibility of using polyvinylidene fluoride (PVDF) sensors to quantitatively measure the under-water pressure wave generated by the collapse of a single cavitation bubble. The electrical signal obtained by PVDF can be converted into pressure information only by using the sensor material parameters provided by the supplier. During the conversion process, only the capacitance of the acquisition chain needs to be additionally measured. At the same time, a high-speed video recording system was used to visualize the evolution of the cavitation bubble. The Gilmore analytical model and an associated wave propagation model were used to simulate the pressure peak of the first collapse of the cavitation bubble. This theoretical pressure was compared with the experimental results. The result showed that, for bubbles with a normalized standoff distance γ larger than 5, the PVDF sensor had the ability to quantitatively measure the pressure wave generated by a single cavitation bubble.

7.
Entropy (Basel) ; 24(1)2021 Dec 27.
Artigo em Inglês | MEDLINE | ID: mdl-35052071

RESUMO

Hydrodynamic pressure exerted on a plunge pool slab by jet impingement is of high interest in high dam projects. The present study experimentally investigated the characteristics of pressure induced by a jet through a constant width flip bucket (CFB) and a slit flip bucket (SFB). A pressurized plane pipe was employed in the flume experiments to control the inlet velocities in the flip buckets. A concise method is proposed to predict the mean dynamic pressure field. Its implementation is summarized as follows: First, the position of the pressure field is determined by the trajectories of free jets, and to calculate its trajectories, an equation based on parabolic trajectory theory is used; second, the maximum mean dynamic pressure is obtained through dimensional analysis, and then the pressure field is established by applying the law of Gaussian distribution. Those steps are integrated into a concise computing procedure by using some easy-to-obtain parameters. Some key parameters, such as takeoff velocity coefficient, takeoff angle coefficient, and the parameter k2, are also investigated in this paper. The formulas of these coefficients are obtained by fitting the experimental data. Using the proposed method, the easy-to-obtain geometric parameters and initial hydraulic conditions can be used to calculate the maximum mean dynamic pressure on the slab. A comparison between experimental data and calculated results confirmed the practicability of this model. These research results provide a reference for hydraulic applications.

8.
Sensors (Basel) ; 19(6)2019 Mar 21.
Artigo em Inglês | MEDLINE | ID: mdl-30901968

RESUMO

Tip clearance flow in axial flow compressor is unavoidable and responsible for pressure losses and noise generation and influences the stability of the compressor. However, necessary flow measurement in the blade tip region is a great challenge due to the small gap width as well as the structure limitation. In this paper, a polyvinylidene fluoride (PVDF) piezoelectric-film sensor array is developed to capture the dynamic pressure field over the blade tip in an axial flow compressor. The PVDF sensor array with 40 evenly distributed sensing points is fabricated directly on a 30 µm thick aluminum-metalized polarized PVDF film through photolithography. Dynamic calibration of the sensor is accomplished using acoustic source as excitation and a microphone as a reference. The test pressure range is up to 3.5 kPa and the sampling frequency is 20 kHz. The sensor presents a high signal-to-noise ratio and good consistency with the reference microphone. Sensitivity, frequency response, linearity, hysteresis, repeatability as well as the influence of temperature are also investigated through the calibration apparatus. The calibration gives credence to the relevance and reliability of this sensor for the application in dynamic pressure field measurement. The sensor is then applied to an actual measurement in a compressor. The output of the PVDF sensor array is also compared with the results of common pressure transducers, and the features of the dynamic pressure filed are discussed. The results indicate that the PVDF sensor array is capable of the dynamic pressure field measurement over the blade tip, and superior to the conventional approaches in installation, spatial resolution, frequency response, and cost. These advantages indicate its potential broad application in pressure measurement, especially for the complex spatial surface or thin-walled structure, such as the blade surface and the thin casing wall of the compressor.

9.
Sensors (Basel) ; 19(9)2019 Apr 30.
Artigo em Inglês | MEDLINE | ID: mdl-31052216

RESUMO

This study presents a procedure to reduce the uncertainty of wind power density estimations, which is useful to improve the energy production predictions of wind farms. Power density is usually determined from the wind speed measured by a cup anemometer and the air density value (conventional procedure). An alternative procedure based on wind speed and dynamic pressure estimations provided by a cup anemometer is proposed. The dynamic pressure is obtained by means of a calibration curve that relates the anemometer rotation frequency and the dynamic pressure measured by a Pitot tube. The quadratic regression, used to define the calibration curve, and its uncertainty are both detailed. A comparison between the alternative procedure and the conventional one points out the advantage of the proposed alternative since results show a high reduction of the indirect measurement uncertainty of wind power density.

10.
Cephalalgia ; 38(7): 1257-1266, 2018 06.
Artigo em Inglês | MEDLINE | ID: mdl-28856912

RESUMO

Objectives To explore the validity of the roller pressure algometer as a new tool for evaluating dynamic pressure sensitivity by assessing its association with pain features and widespread pressure pain sensitivity in migraine women, and also to determine whether dynamic pressure algometry differentiates between episodic and chronic migraine. Methods One hundred and twenty women with migraine (42% chronic, 58% episodic) participated. Dynamic pressure sensitivity was assessed with a set of roller pressure algometers (Aalborg University, Denmark®) consisting of 11 rollers with fixed pressure levels from 500 to 5300 g. Each roller was moved at a speed of 0.5 cm/sec over a 60 mm horizontal line covering the temporalis muscle. The dynamic pain threshold (the pressure level of the first painful roller) and pain elicited during the pain threshold (roller evoked pain) were determined. Static pressure pain thresholds were assessed over the temporalis muscle, C5/C6 joint, second metacarpal, and tibialis anterior. Results Side-to-side consistency between dynamic pain threshold (rs = 0.769, p < 0.001) and roller evoked pain (rs = 0.597; p < 0.001) were found. Women with chronic migraine exhibited bilateral lower dynamic pain thresholds ( p < 0.01), but similar widespread pressure pain thresholds (all, p > 0.284) than those with episodic migraine. Dynamic pain threshold was moderately positively associated with widespread pressure pain thresholds (0.358 > rs > 0.700, all p < 0.001). This association was slightly stronger in chronic migraine. Pain during dynamic pain threshold was negatively associated with widespread pressure pain thresholds (-0.336 < rs < -0.235, all p < 0.01). Conclusions Roller pressure algometry was valid for assessing dynamic pressure sensitivity in migraine in the trigeminal area and is consistent with widespread static pressure pain sensitivity. Roller, but not static, pressure algometry differentiated between episodic and chronic migraine. Assessing static and dynamic deep somatic tissue sensitivity may provide new opportunities for evaluating treatment outcomes.


Assuntos
Transtornos de Enxaqueca/diagnóstico , Medição da Dor/instrumentação , Limiar da Dor/fisiologia , Estimulação Física/instrumentação , Adulto , Feminino , Humanos , Pessoa de Meia-Idade , Pressão
11.
Philos Trans A Math Phys Eng Sci ; 376(2111)2018 Jan 28.
Artigo em Inglês | MEDLINE | ID: mdl-29229802

RESUMO

To investigate changes in the instability of Stokes waves prior to wave breaking in shallow water, pressure data were recorded vertically over the entire water depth, except in the near-surface layer (from 0 cm to -3 cm), in a recirculating channel. In addition, we checked the pressure asymmetry under several conditions. The phase-averaged dynamic-pressure values for the wave-current motion appear to increase compared with those for the wave-alone motion; however, they scatter in the experimental range. The measured vertical distributions of the dynamic pressure were plotted over one wave cycle and compared to the corresponding predictions on the basis of third-order Stokes wave theory. The dynamic-pressure pattern was not the same during the acceleration and deceleration periods. Spatially, the dynamic pressure varies according to the faces of the wave, i.e. the pressure on the front face is lower than that on the rear face. The direction of wave propagation with respect to the current directly influences the essential features of the resulting dynamic pressure. The results demonstrate that interactions between travelling waves and a current lead more quickly to asymmetry.This article is part of the theme issue 'Nonlinear water waves'.

12.
Klin Lab Diagn ; 60(7): 14-27, 2015.
Artigo em Russo | MEDLINE | ID: mdl-31561669

RESUMO

In phylogenesis, regulation of metabolism formed autocrine separately in paracrin regulated cells cenosises and on the level of organism. Under essential (metabolic) arterial hypertension organs-targets are involved into pathological process for the second time; realization of biological functions of homeostasis, trophology, endoecology and adaptation are disturbed for the second time too. Every organ-target regulates in vivo function of local hydro-dynamic systems: kidneys - pool of primary urine; brain - pool of cerebrospinal fluid; lungs - blood of pulmonary circulation. The arterial pressure is increased not by kidneys but by vasomotor center on the basis of afferent information from chemoreceptors about disorder of metabolism and micro-circulation n and hence initiates efferent stimulation of heart, increase of arterial pressure in proximal and hydro-dynamic pressure in distal section of arterial flow. The increasing of arterial pressure in afferent arteriole of glomeruli can increase filtration more than proximal tubules can reabsorb primary urine. The angiotensin is called to decrease arterial pressure over basal membrane because together with aldosterone they preserve parameters of intercellular medium in vivo. Under metabolic arterial pressure, the purpose of vasomotor center is to ameliorate realization of biological function of endoecology; to decrease amount of biological "garbage" of small sizes and "uremic toxins" in intercellular medium; to decrease afferent, parasympathetic signalization from chemoreceptors; to decrease sympathetic stimulation of heart. The formation of three stages of relative "biological perfection" in phylogenesis and non-eliminated "regulatory inconsistencies" on autocrine level, both in paracrin regulated cells cenosises and on level of organism, constitute pathogenic foundation, united algorithm of pathogenesis of all metabolic pandemic - "civilization diseases", including metabolic syndrome, metabolic arterial pressure, atherosclerosis, insulin resistance and obesity. The aphysiologic impacts of environment are most often the etiological factor of metabolic epidemic.

13.
Food Chem ; 464(Pt 2): 141723, 2024 Oct 23.
Artigo em Inglês | MEDLINE | ID: mdl-39476577

RESUMO

Pressure promotes the formation of starch-polyphenol complexes, but their classification and properties are still unclear. This study aimed to elucidate the effects of dynamic high-pressure homogenization (10-50 MPa) and static hydrostatic pressure (100-500 MPa) on the copolymerization behavior and properties of lotus seed starch (LS)-endogenous polyphenol chlorogenic acid (CA) complexes. The results showed that both pressures induced LS-CA to form stable inclusion-type complexes and easily destructible noninclusion-type complexes. Increased pressure promoted the formation of inclusion-type complexes, with dynamic pressure having a particularly strong effect. However, noninclusion-type complexes began breaking down at 20 MPa under dynamic pressure and 300 MPa under static pressure. Inclusion-type complexes primarily improve starch ordering, and noninclusion-type complexes enhance water holding capacity, but excessive proportions of either type affect pasting performance. These findings offer insights into transforming specific starch structures through small molecular components and provide a theoretical basis for controlling functional starch product processing.

14.
J Colloid Interface Sci ; 608(Pt 3): 2414-2420, 2022 Feb 15.
Artigo em Inglês | MEDLINE | ID: mdl-34753623

RESUMO

HYPOTHESIS: Droplet spreading on surfaces is a ubiquitous phenomenon in nature and is relevant with a wide range of applications. In practical scenarios, surfaces are usually associated with certain levels of vibration. Although vertical or horizontal modes of vibration have been used to promote droplet dewetting, bouncing from immiscible medium, directional transport, etc., a quantitative understanding of how external vibration mediates the droplet behaviors remains to be revealed. METHODS: We studied droplets impacting on stationary and vibratory surfaces, respectively. In analogy to the Weber number We=ρUi2D0/γ, we define the vibration Weber number We*=ρUv2D0/γ to quantitively analyze the vibration-induced dynamic pressure on droplet behaviors on vibratory surfaces, where ρ,γ,D0,UiandUv are liquid density, surface tension, initial droplet diameter, impact velocity of the droplet, and velocity amplitude of vibration, respectively. FINDINGS: We demonstrate that the effect of vibration on promoting droplet spreading can be captured by a new scaling number expressed as We*/[We1\2sin(θ/2)], leading to (Dm - Dm0)/Dm0 âˆ We*/[We1\2sin(θ/2)], where θ is the contact angle, and Dm0 and Dm are the maximum diameter of the droplet on stationary and vibratory surfaces, respectively. The scaling number illustrates the relative importance of vibration-induced dynamic pressure compared to inertial force and surface tension. Together with other well-established non-dimensional numbers, this scaling number provides a new dimension and framework for understanding and controlling droplet dynamics. Our findings can also find applications such as improving the power generation efficiency, intensifying the deposition of paint, and enhancing the heat transfer of droplets.

15.
Adv Mater ; 33(39): e2102302, 2021 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-34369023

RESUMO

Bioresorbable electronics that can be absorbed and become part of the organism after their service life are a new trend to avoid secondary invasive surgery. However, the material limitation is a significant challenge. There are fewer biodegradable materials with pressure-sensitive properties. Here, a pressure sensor based on the triboelectric effect between bioabsorbable materials is reported. This effect is available in almost all materials. The bioresorbable triboelectric sensor (BTS) can directly convert ambient pressure changes into electrical signals. This device successfully identifies abnormal vascular occlusion events in large animals (dogs). The service life of the BTS reaches 5 days with a high service efficiency (5.95%). The BTS offers excellent sensitivity (11 mV mmHg-1 ), linearity (R2  = 0.993), and good durability (450 000 cycles). The antibacterial bioresorbable materials (poly(lactic acid)-(chitosan 4%)) for the BTS can achieve 99% sterilization. Triboelectric devices are expected to be applied in postoperative care as bioresorbable electronics.


Assuntos
Implantes Absorvíveis , Doenças Cardiovasculares/cirurgia , Monitorização Fisiológica/instrumentação , Animais , Materiais Biocompatíveis/química , Doenças Cardiovasculares/fisiopatologia , Cães , Dispneia/fisiopatologia , Eletrônica , Camundongos , Monitorização Fisiológica/métodos , Poliésteres/química , Cuidados Pós-Operatórios
16.
J Chromatogr A ; 1652: 462358, 2021 Aug 30.
Artigo em Inglês | MEDLINE | ID: mdl-34237483

RESUMO

A baseline correction method is developed for comprehensive two-dimensional (2D) chromatography (GC × GC) with flame-ionization detection (FID) using dynamic pressure gradient modulation (DPGM). The DPGM-GC × GC-FID utilized porous layer open tubular (PLOT) columns in both dimensions to focus on light hydrocarbon separations. Since DPGM is nominally a stop-flow modulation technique, a rhythmic baseline disturbance is observed in the FID signal that cycles with the modulation period (PM). This baseline disturbance needs to be corrected to optimize trace analysis. The baseline correction method has three steps: collection of a background "blank" chromatogram and multiplying it by an optimized normalization factor, subtraction of the normalization-optimized background chromatogram from a sample chromatogram, and application of Savitzky-Golay smoothing. An alkane standard solution, containing pentane, hexane and heptane was used for method development, producing linear calibration curves (r2 > 0.991) over a broad concentration range (7.8 ppm - 4000 ppm). Further, the limit-of-detection (LOD) and limit-of-quantification (LOQ) were determined for pentane (LOD = 2.5 ppm, LOQ = 8.2 ppm), hexane (LOD = 0.9 ppm, LOQ = 3.0 ppm), and heptane (LOD = 1.9 ppm, LOQ = 6.4 ppm). A natural gas sample separation illustrated method applicability, whereby the DPGM produced a signal enhancement (SE) of 30 for isopentane, where SE is defined as the height of the tallest 2D peak in the modulated chromatogram for the analyte divided by the height of the unmodulated 1D peak. The 30-fold SE resulted in about a 10-fold improvement in the signal-to-noise ratio (S/N) for isopentane. Additional versatility of the baseline correction method for more complicated samples was demonstrated for an unleaded gasoline sample, which enabled the detection (and visual appearance) of trace components.


Assuntos
Ionização de Chama/métodos , Alcanos/química , Gasolina/análise , Hidrocarbonetos/isolamento & purificação , Limite de Detecção , Gás Natural/análise , Pentanos/análise
17.
Sensors (Basel) ; 10(2): 1338-54, 2010.
Artigo em Inglês | MEDLINE | ID: mdl-22205871

RESUMO

Pressure measurement in high temperature environments is important in many applications to provide valuable information for performance studies. Information on pressure patterns is highly desirable for improving performance, condition monitoring and accurate prediction of the remaining life of systems that operate in extremely high temperature environments, such as gas turbine engines. A number of technologies have been recently investigated, however these technologies target specific applications and they are limited by the maximum operating temperature. Thick and thin films of SiCN can withstand high temperatures. SiCN is a polymer-derived ceramic with liquid phase polymer as its starting material. This provides the advantage that it can be molded to any shape. CERASET™ also yields itself for photolithography, with the addition of photo initiator 2, 2-Dimethoxy-2-phenyl-acetophenone (DMPA), thereby enabling photolithographical patterning of the pre-ceramic polymer using UV lithography. SiCN fabrication includes thermosetting, crosslinking and pyrolysis. The technology is still under investigation for stability and improved performance. This work presents the preparation of SiCN films to be used as the body of a sensor for pressure measurements in high temperature environments. The sensor employs the phenomenon of drag effect. The pressure sensor consists of a slender sensitive element and a thick blocking element. The dimensions and thickness of the films depend on the intended application of the sensors. Fabrication methods of SiCN ceramics both as thin (about 40-60 µm) and thick (about 2-3 mm) films for high temperature applications are discussed. In addition, the influence of thermosetting and annealing processes on mechanical properties is investigated.


Assuntos
Cerâmica/química , Eletrônica , Temperatura Alta , Pressão , Compostos de Silício/química , Acetofenonas/química , Polímeros/química , Raios Ultravioleta
18.
Acta Neurol Belg ; 120(5): 1265-1270, 2020 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-32710285

RESUMO

We investigated if dynamic pressure pain sensitivity in the symptomatic area is associated with pressure sensitivity in local and distant pain-free areas in cluster headache (CH). A pressure algometry set consisting of 8 rollers with fixed pressure levels ranging from 500 to 5300 g was used to assess dynamic pressure pain sensitivity in men with episodic CH. Each roller was moved from an anterior-to-posterior direction over the temporalis muscle. The load level of the first painful roller was considered the dynamic pain threshold (DPT). Further, pain elicited during DPT (roller evoked pain) was also assessed. We used a pressure algometer to determine pressure pain thresholds (PPTs) over the temporalis muscle, C5/C6 joint, second metacarpal, and tibialis anterior. Patients were assessed in an asymptomatic (remission) phase, at least 6 months after their last cluster period and without taking pharmacological treatment. Forty men with episodic CH (mean age 42 years) were included. Both outcomes, DPTs (r = 0.781, P < 0.001) and roller-evoked pain (r = 0.586; P < 0.001) were bilaterally correlated. Further, DPT, but not roller-evoked pain, was moderately associated with PPTs measured at the symptomatic (temporalis: r = 0.665, P < 0.001) and distant pain-free (C5-C6 joint: r = 0.389, P = 0.013; second metacarpal: r = 0.551, P < 0.001; and, tibialis anterior: r = 0.308, P = 0.035) points. Dynamic pressure sensitivity in the trigeminal area was correlated to pressure pain sensitivity at both symptomatic and distant pain-free areas in men with CH supporting the use of roller pressure algometry. Dynamic pressure algometry may be a new tool for assessing the status of sensitization in primary headaches.


Assuntos
Cefaleia Histamínica/fisiopatologia , Hiperalgesia/diagnóstico , Medição da Dor/instrumentação , Medição da Dor/métodos , Limiar da Dor/fisiologia , Adulto , Humanos , Masculino , Pessoa de Meia-Idade , Estimulação Física/instrumentação , Estimulação Física/métodos
19.
Ultrason Sonochem ; 68: 105225, 2020 Nov.
Artigo em Inglês | MEDLINE | ID: mdl-32615403

RESUMO

When liquids flow in the pipelines, the onset of cavitation can be characterized by a variant of the Euler number known as the cavitation number (CN), which is based on the velocity and denoted by C in this paper. Conventionally, cavitation is considered to be induced when C ~ 1. However, experimental observations and several pipe bursts indicate that the CN may incorrectly predict the onset of cavitation. For example, when leakage occurs in the pipeline or a valve in the pipeline is opened, the resultant pressure loss generates a dynamic pressure wave with a small amplitude, which may lead to bubble formation, even though C ~ 1 is not satisfied. Hence, this paper proposes another CN based on the amplitude of the generated dynamic pressure wave, rather than the velocity, for ascertaining the onset of cavitation. The validity of the proposed CN was verified through experiments and a case study. The results indicated that the proposed CN can be effectively used for cavitation prediction induced by pressure fluctuations and for investigating phenomena such as pressure fluctuation, leakage, and corrosion in liquid pipelines, tanks, and pressure vessels, as well as the safety design of liquefied natural gas tanks and tankers.

20.
J Chromatogr A ; 1620: 460982, 2020 Jun 07.
Artigo em Inglês | MEDLINE | ID: mdl-32098681

RESUMO

Dynamic pressure gradient modulation (DPGM) is investigated for comprehensive two-dimensional gas chromatography (GC × GC) with time-of-flight mass spectrometry (TOFMS) detection. With DPGM, a commercial pneumatic "pulse" valve is opened to introduce a suitably high auxiliary gas pressure at a T-junction connecting the first dimension (1D) and second dimension (2D) columns during the modulation period (PM), temporarily stopping the 1D flow. The valve is then closed for the duration of a pulse width (pw) to "re-inject" temporally focused 1D eluate onto the 2D column for separation. This flow modulation technique is observed to be compatible with TOFMS detection using a 2D flow rate of 4 ml/min for the separation of a 90-component test mixture. A 25 min separation window using a PM = 1 s and pw = 200 ms for full modulation (and 100% duty cycle) provided an average 1Wb = 4.5 s and 2Wb = 130 ms for a 2D peak capacity of nc,2D = 2700 (100 peaks per min). The detector response enhancement factor (DREF) serves as a metric for the enhanced sensitivity of the modulated relative to the unmodulated 1D peaks, with DREFs ranging between 10 and 20 and about a 5-fold improvement in signal-to-noise ratio (S/N). The bilinear "quality" of the GC × GC data is studied using the chemometric method parallel factor analysis (PARAFAC). Since PARAFAC requires sufficiently trilinear data, the reproducibility of the 2D peak shape for a given analyte is confirmed using lack-of-fit (LOF) and percent variation (R2) metrics. The limit-of-detection (LOD) for the representative analyte hexadecane is determined using PARAFAC, providing an LOD of 0.7 ppb (±0.03 ppb) for three replicates. Seven heavily overlapped analytes are also fully resolved by PARAFAC down to the part-per-million (ppm) concentration level, producing reproducible spectra with a majority of spectral match values (MV) over 800 (RSD ≤ 7.1%). This study provides promising results for DPGM as a flow modulation technique compatible with GC × GC-TOFMS, providing high sensitivity data suitable for chemometric analysis.


Assuntos
Cromatografia Gasosa-Espectrometria de Massas/métodos , Espectrometria de Massas/métodos , Pressão , Alcanos/química , Análise Fatorial , Limite de Detecção , Reprodutibilidade dos Testes
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