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[Study on the determination of 28 inorganic elements in sunflower seeds by ICP-OES/ICP-MS].
Liu, Hong-Wei; Qin, Zong-Hui; Xie, Hua-Lin; Cao, Shu.
Afiliação
  • Liu HW; College of Material and Chemical Engineering, Hunan Institute of Technology, Hengyang 421002, China. hwl0466@163.com
Guang Pu Xue Yu Guang Pu Fen Xi ; 33(1): 224-7, 2013 Jan.
Article em Zh | MEDLINE | ID: mdl-23586261
The present paper describes a simple method for the determination of trace elements in sunflower seeds by using inductively coupled plasma optical emission spectrometry (ICP-OES) and inductively coupled plasma spectrometry (ICP-MS). HNO3 + H2O2 were used to achieve the complete decomposition of the organic matrix in a closed-vessel microwave oven. The contents of 10 trace elements (Al, B, Ca, Fe, K, Mg, Na, Si, P and S) in sunflower seeds were determined by ICP-OES while 18 trace elements (As, Ba, Cd, Co, Cr, Cu, Li, Mn, Mo, Ni, Pb, Rb, Sr, Sn, Sb, Ti, V and Zn) were determined by ICP-MS. The rice reference material (GBW10045) was used as standard reference materials. The results showed a good agreement between measured and certified values for all analytes. The concentrations of necessary micro elements Ca, K, Mg, P and S were higher. This method was simple, sensitive and precise and can perform simultaneous multi-elements determination of sunflower seeds.
Assuntos
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Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Sementes / Espectrofotometria Atômica / Espectrometria de Massas / Helianthus / Íons Idioma: Zh Ano de publicação: 2013 Tipo de documento: Article
Buscar no Google
Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Sementes / Espectrofotometria Atômica / Espectrometria de Massas / Helianthus / Íons Idioma: Zh Ano de publicação: 2013 Tipo de documento: Article