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Palladium-Catalyzed Oxalyl Amide Directed Silylation and Germanylation of Amine Derivatives.
Chen, Changpeng; Guan, Mingyu; Zhang, Jingyu; Wen, Zhenkang; Zhao, Yingsheng.
Afiliação
  • Chen C; †Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Materials Science, Soochow University, Suzhou 215123, China.
  • Guan M; †Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Materials Science, Soochow University, Suzhou 215123, China.
  • Wen Z; §College of Chemistry and Chemical Engineering, Shanxi University, Taiyuan 030006, China.
  • Zhao Y; †Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Materials Science, Soochow University, Suzhou 215123, China.
Org Lett ; 17(15): 3646-9, 2015 Aug 07.
Article em En | MEDLINE | ID: mdl-26161949
ABSTRACT
Palladium-catalyzed direct ortho-silylation of oxalyl amide-protected phenylmethanamine and phenethylamine with commercially available disilanes is reported. Germanylation products were also produced under the same reaction conditions. This protocol tolerated oxalyl amide-protected aliphatic amines, which gave γ-C-H silylation products.
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Ano de publicação: 2015 Tipo de documento: Article
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Ano de publicação: 2015 Tipo de documento: Article