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Introduction and comparison of new EBSD post-processing methodologies.
Wright, Stuart I; Nowell, Matthew M; Lindeman, Scott P; Camus, Patrick P; De Graef, Marc; Jackson, Michael A.
Afiliação
  • Wright SI; EDAX, 392 East 12300 South, Suite H, Draper, UT 84020, USA.
  • Nowell MM; EDAX, 392 East 12300 South, Suite H, Draper, UT 84020, USA.
  • Lindeman SP; EDAX, 392 East 12300 South, Suite H, Draper, UT 84020, USA.
  • Camus PP; EDAX, 91 McKee Drive, Mahwah, NJ 07430, USA.
  • De Graef M; Carnegie Mellon University, Department of Material Science and Engineering, 5000 Forbes Avenue, Pittsburgh, PA 15213, USA.
  • Jackson MA; BlueQuartz Software, 400 S. Pioneer Blvd, Springboro, OH 45066, USA.
Ultramicroscopy ; 159 Pt 1: 81-94, 2015 Dec.
Article em En | MEDLINE | ID: mdl-26342553
ABSTRACT
Electron Backscatter Diffraction (EBSD) provides a useful means for characterizing microstructure. However, it can be difficult to obtain index-able diffraction patterns from some samples. This can lead to noisy maps reconstructed from the scan data. Various post-processing methodologies have been developed to improve the scan data generally based on correlating non-indexed or mis-indexed points with the orientations obtained at neighboring points in the scan grid. Two new approaches are introduced (1) a re-scanning approach using local pattern averaging and (2) using the multiple solutions obtained by the triplet indexing method. These methodologies are applied to samples with noise introduced into the patterns artificially and by the operational settings of the EBSD camera. They are also applied to a heavily deformed and a fine-grained sample. In all cases, both techniques provide an improvement in the resulting scan data, the local pattern averaging providing the most improvement of the two. However, the local pattern averaging is most helpful when the noise in the patterns is due to the camera operating conditions as opposed to inherent challenges in the sample itself. A byproduct of this study was insight into the validity of various indexing success rate metrics. A metric based given by the fraction of points with CI values greater than some tolerance value (0.1 in this case) was confirmed to provide an accurate assessment of the indexing success rate.
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Ano de publicação: 2015 Tipo de documento: Article

Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Ano de publicação: 2015 Tipo de documento: Article