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A Method for Synthesis of 3-Hydroxy-1-indanones via Cu-Catalyzed Intramolecular Annulation Reactions.
He, Guoxue; Wu, Chenglin; Zhou, Jianhui; Yang, Qiaolan; Zhang, Chunmei; Zhou, Yu; Zhang, Huabei; Liu, Hong.
Afiliação
  • He G; Key Laboratory of Radiopharmaceuticals of Ministry of Education, College of Chemistry , Beijing Normal University , No. 19 Xinjiekouwai Street, Haidian District , Beijing 100875 , People's Republic of China.
  • Wu C; State Key Laboratory of Drug Research and Key Laboratory of Receptor Research , Shanghai Institute of Materia Medica, Chinese Academy of Sciences , 555 Zu Chong Zhi Road , Shanghai 201203 , China.
  • Zhou J; State Key Laboratory of Drug Research and Key Laboratory of Receptor Research , Shanghai Institute of Materia Medica, Chinese Academy of Sciences , 555 Zu Chong Zhi Road , Shanghai 201203 , China.
  • Yang Q; State Key Laboratory of Drug Research and Key Laboratory of Receptor Research , Shanghai Institute of Materia Medica, Chinese Academy of Sciences , 555 Zu Chong Zhi Road , Shanghai 201203 , China.
  • Zhang C; State Key Laboratory of Drug Research and Key Laboratory of Receptor Research , Shanghai Institute of Materia Medica, Chinese Academy of Sciences , 555 Zu Chong Zhi Road , Shanghai 201203 , China.
  • Zhou Y; State Key Laboratory of Drug Research and Key Laboratory of Receptor Research , Shanghai Institute of Materia Medica, Chinese Academy of Sciences , 555 Zu Chong Zhi Road , Shanghai 201203 , China.
  • Zhang H; Key Laboratory of Radiopharmaceuticals of Ministry of Education, College of Chemistry , Beijing Normal University , No. 19 Xinjiekouwai Street, Haidian District , Beijing 100875 , People's Republic of China.
  • Liu H; State Key Laboratory of Drug Research and Key Laboratory of Receptor Research , Shanghai Institute of Materia Medica, Chinese Academy of Sciences , 555 Zu Chong Zhi Road , Shanghai 201203 , China.
J Org Chem ; 83(21): 13356-13362, 2018 11 02.
Article em En | MEDLINE | ID: mdl-30295478
We report a facile and highly efficient method that copper-catalyzed intramolecular annulation to synthesize 3-hydroxy-1-indanones employing simple 2-ethynylbenzaldehyde as starting materials was achieved successfully. This protocol provided a simple synthetic approach to afford 3-hydroxy-1-indanones under mild conditions in good to excellent yields.
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Ano de publicação: 2018 Tipo de documento: Article
Texto completo
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Ano de publicação: 2018 Tipo de documento: Article