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Multimodal x-ray and electron microscopy of the Allende meteorite.
Lo, Yuan Hung; Liao, Chen-Ting; Zhou, Jihan; Rana, Arjun; Bevis, Charles S; Gui, Guan; Enders, Bjoern; Cannon, Kevin M; Yu, Young-Sang; Celestre, Richard; Nowrouzi, Kasra; Shapiro, David; Kapteyn, Henry; Falcone, Roger; Bennett, Chris; Murnane, Margaret; Miao, Jianwei.
Afiliação
  • Lo YH; Department of Physics and Astronomy and California NanoSystems Institute, University of California, Los Angeles, CA 90095, USA.
  • Liao CT; Department of Bioengineering, University of California, Los Angeles, CA 90095, USA.
  • Zhou J; JILA and Department of Physics, University of Colorado and National Institute of Standards and Technology (NIST), Boulder, CO 80309, USA.
  • Rana A; Department of Physics and Astronomy and California NanoSystems Institute, University of California, Los Angeles, CA 90095, USA.
  • Bevis CS; Department of Physics and Astronomy and California NanoSystems Institute, University of California, Los Angeles, CA 90095, USA.
  • Gui G; JILA and Department of Physics, University of Colorado and National Institute of Standards and Technology (NIST), Boulder, CO 80309, USA.
  • Enders B; JILA and Department of Physics, University of Colorado and National Institute of Standards and Technology (NIST), Boulder, CO 80309, USA.
  • Cannon KM; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA.
  • Yu YS; Department of Physics, University of Central Florida, Orlando, FL 32816, USA.
  • Celestre R; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA.
  • Nowrouzi K; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA.
  • Shapiro D; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA.
  • Kapteyn H; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA.
  • Falcone R; JILA and Department of Physics, University of Colorado and National Institute of Standards and Technology (NIST), Boulder, CO 80309, USA.
  • Bennett C; Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA.
  • Murnane M; Department of Physics, University of Central Florida, Orlando, FL 32816, USA.
  • Miao J; JILA and Department of Physics, University of Colorado and National Institute of Standards and Technology (NIST), Boulder, CO 80309, USA.
Sci Adv ; 5(9): eaax3009, 2019 09.
Article em En | MEDLINE | ID: mdl-31555739
ABSTRACT
Multimodal microscopy that combines complementary nanoscale imaging techniques is critical for extracting comprehensive chemical, structural, and functional information, particularly for heterogeneous samples. X-ray microscopy can achieve high-resolution imaging of bulk materials with chemical, magnetic, electronic, and bond orientation contrast, while electron microscopy provides atomic-scale spatial resolution with quantitative elemental composition. Here, we combine x-ray ptychography and scanning transmission x-ray spectromicroscopy with three-dimensional energy-dispersive spectroscopy and electron tomography to perform structural and chemical mapping of an Allende meteorite particle with 15-nm spatial resolution. We use textural and quantitative elemental information to infer the mineral composition and discuss potential processes that occurred before or after accretion. We anticipate that correlative x-ray and electron microscopy overcome the limitations of individual imaging modalities and open up a route to future multiscale nondestructive microscopies of complex functional materials and biological systems.

Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Ano de publicação: 2019 Tipo de documento: Article

Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Ano de publicação: 2019 Tipo de documento: Article