NORD: NO Relaxation Delay NMR Spectroscopy.
Angew Chem Int Ed Engl
; 60(24): 13587-13590, 2021 06 07.
Article
em En
| MEDLINE
| ID: mdl-33783935
ABSTRACT
The novel concept of NORD (NO relaxation delay) NMR spectroscopy is introduced. The idea is to design concatenated experiments in a way that the magnetization used in the first relaxes toward equilibrium during the second and vice versa, thus saving instrument time. Applications include complete well-resolved 1 H-1 H and 1 H-13 C one-bond and long-range correlation maps of an 80â
mM solution of a trisaccharide recorded in less than two minutes and hydrocortisone with extensive spectral overlap.
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Coleções:
01-internacional
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MEDLINE
Idioma:
En
Ano de publicação:
2021
Tipo de documento:
Article