Combining heteronuclear correlation NMR with spin-diffusion to detect relayed Cl-H-H and N-H-H proximities in molecular solids.

Raval, Parth; Trébosc, Julien; Pawlak, Tomasz; Nishiyama, Yusuke; Brown, Steven P; Manjunatha Reddy, G N

Raval, Parth; Trébosc, Julien; Pawlak, Tomasz; Nishiyama, Yusuke; Brown, Steven P; Manjunatha Reddy, G N.

Afiliação

Raval P; University of Lille, CNRS, Centrale Lille Institut, Univ. Artois, UMR 8181-UCCS- Unité de Catalyse et Chimie du Solide, F, 59000, Lille, France.
Trébosc J; Univ. Lille, CNRS, INRAE, Centrale Lille, Univ. Artois, FR 2638 - IMEC - Institut Michel-Eugène Chevreul, F, 59000, Lille, France.
Pawlak T; Centre of Molecular and Macromolecular Studies, Polish Academy of Sciences, Sienkiewicza 112, 90-363, Lodz, Poland.
Nishiyama Y; RIKEN-JEOL Collaboration Centre, RIKEN, Yokohama Campus, Yokohama, Kanagawa, 230-0045, Japan; JEOL RESONANCE Inc., Akishima, Tokyo, 196-8558, Japan.
Brown SP; Department of Physics, University of Warwick, Coventry, CV4 7AL, UK. Electronic address: S.P.Brown@warwick.ac.uk.
Manjunatha Reddy GN; University of Lille, CNRS, Centrale Lille Institut, Univ. Artois, UMR 8181-UCCS- Unité de Catalyse et Chimie du Solide, F, 59000, Lille, France. Electronic address: gnm.reddy@univ-lille.fr.

Solid State Nucl Magn Reson ; 120: 101808, 2022 08.

Article em En | MEDLINE | ID: mdl-35780556

Assuntos

Dopamina; Prótons; Histidina/química; Espectroscopia de Ressonância Magnética/métodos; Ressonância Magnética Nuclear Biomolecular

Palavras-chave

DFT; Fast MAS; GIPAW; HMQC; NMR crystallography; Pharmaceutical; Solid-state NMR; Structure elucidation

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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Prótons / Dopamina Idioma: En Ano de publicação: 2022 Tipo de documento: Article

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