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First total synthesis of asperilactone B. Revision of absolute stereochemistry of asperilactones B and C.
Djokic, Sanja; Benedekovic, Goran; Kesic, Jelena; Rodic, Marko V; Popsavin, Mirjana; Popsavin, Velimir; Francuz, Jovana.
Afiliação
  • Djokic S; University of Novi Sad, Faculty of Sciences, Department of Chemistry, Biochemistry and Environmental Protection, Trg Dositeja Obradovica 3, 21000 Novi Sad, Serbia. jovana.francuz@dh.uns.ac.rs.
  • Benedekovic G; University of Novi Sad, Faculty of Sciences, Department of Chemistry, Biochemistry and Environmental Protection, Trg Dositeja Obradovica 3, 21000 Novi Sad, Serbia. jovana.francuz@dh.uns.ac.rs.
  • Kesic J; University of Novi Sad, Faculty of Sciences, Department of Chemistry, Biochemistry and Environmental Protection, Trg Dositeja Obradovica 3, 21000 Novi Sad, Serbia. jovana.francuz@dh.uns.ac.rs.
  • Rodic MV; University of Novi Sad, Faculty of Sciences, Department of Chemistry, Biochemistry and Environmental Protection, Trg Dositeja Obradovica 3, 21000 Novi Sad, Serbia. jovana.francuz@dh.uns.ac.rs.
  • Popsavin M; University of Novi Sad, Faculty of Sciences, Department of Chemistry, Biochemistry and Environmental Protection, Trg Dositeja Obradovica 3, 21000 Novi Sad, Serbia. jovana.francuz@dh.uns.ac.rs.
  • Popsavin V; University of Novi Sad, Faculty of Sciences, Department of Chemistry, Biochemistry and Environmental Protection, Trg Dositeja Obradovica 3, 21000 Novi Sad, Serbia. jovana.francuz@dh.uns.ac.rs.
  • Francuz J; Serbian Academy of Sciences and Arts, Kneza Mihaila 35, 11000 Belgrade, Serbia.
Org Biomol Chem ; 22(24): 4864-4867, 2024 Jun 19.
Article em En | MEDLINE | ID: mdl-38747648
ABSTRACT
The first total synthesis and absolute configuration assignment of asperilactone B (I) have been accomplished. Additionally, a revision of the absolute stereochemistry of asperilactone C has been done. The first total synthesis of the opposite enantiomer of asperilactone B (ent-I) has also been achieved, as well as that of C-7 epimers of both asperilactones B (8) and C (9).
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Ano de publicação: 2024 Tipo de documento: Article
Texto completo
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Idioma: En Ano de publicação: 2024 Tipo de documento: Article