RESUMO
In order to improve the mechanical properties, nutritional value and fresh-keeping ability of conventional sodium alginate edible composite membranes, a new type of edible composite film was prepared by adding water-blocking agent carnauba wax, plasticizer glycerin, antioxidant and nutritional enhancer sodium ascorbate on a basis of traditional sodium alginate composite film. In this study, the physical, mechanical and structural properties of different film components were investigated. The results showed the components did not simply combine, but produced interaction forces which improved the stability and mechanical properties of composite film. When the amount of calcium ascorbate was 0.4%, the water vapor transmittance of the composite film reached a minimum of 0.65 g·mm/(cm2·d·kPa), and the tensile strength and elongation at break reached the maximum, which were 398.64 MPa and 17.93%, respectively. Additionally, the sodium alginate-carnauba wax film exhibited better performance on the preservation of fresh-cut apples. Compared with other composite films, the color and hardness of fresh-cut apples coated with this composite film were better maintained, and the losses of titration acid content and soluble solid content were reduced. Moreover, the weight loss rate, increase in polyphenol oxidase activity and total colony count were inhibited. All results determined that the edible film has good application value in the field of fresh-cut fruit preservation, which provides a theoretical basis for further research on edible film.
Assuntos
Malus , Malus/química , Alginatos/química , Ácido Ascórbico , Conservantes FarmacêuticosRESUMO
The aim of this work was to evaluate the effect of the concentration of gelatin (G) (3-6 g), whey protein (W) (2.5-7.5 g) and chitosan (C) (0.5-2.5 g) on the physical, optical and mechanical properties of composite edible films (CEFs) using the response surface methodology (RSM), as well as optimizing the formulation for the packaging of foods. The results of the study were evaluated via first- and second-order multiple regression analysis to obtain the determination coefficient values with a good fit (R Ë 0.90) for each of the response variables, except for the values of solubility and b*. The individual linear effect of the independent variables (the concentrations of gelatin, whey protein and chitosan) significantly affected (p ≤ 0.05) the water vapor permeability (WVP), strength and solubility of the edible films. The WVP of the edible films varied from 0.90 to 1.62 × 10-11 g.m/Pa.s.m2, the resistance to traction varied from 0.47 MPa to 3.03 MPa and the solubility varied from 51.06% to 87%. The optimized values indicated that the CEF prepared with a quantity of 4 g, 5 g and 3 g of gelatin, whey protein and chitosan, respectively, provided the CEF with a smooth, continuous and transparent surface, with L values that resulted in a light-yellow hue, a lower WVP, a maximum strength (resistance to traction) and a lower solubility. The results revealed that the optimized formulation of the CEF of G-W-C allowed a good validation of the prediction model and could be applied, in an effective manner, to the food packaging industry, which could help in mitigating the environmental issues associated with synthetic packaging materials.
Assuntos
Quitosana/química , Filmes Comestíveis , Gelatina/química , Proteínas do Soro do Leite/química , Permeabilidade , VaporRESUMO
Due to the convenience, fresh-cut vegetables or fruits as the emerging commercial products have attracted much attention in recent years. However, the preservation of food with high quality remains a big challenge. In this study, one novel kind of edible composite film (PAX) consisted of pectin, sodium alginate (SA), and xanthan gum (XG) was well developed. The optimum concentrations for pectin and SA in PAX film based on the shearing viscosity were 6 g/L and 5 g/L, respectively. Upon this condition, the experimental results from the response surface methodology showed that the tensile strength for the optimized PAX (PAXO) film can reach the maximum value of 29.65 MPa at the concentration of 4 g/L XG, 18 g/L glycerol, and 20 g/L CaCl2. The corresponding elongation at break was 19.02% and the water vapor transmission rate was evaluated to be 18.12 × 10-11 g/(m2·s·pa). Furthermore, the nanocomposites in terms of coating or films were used to keep fresh-cut potatoes, where they exhibited different efficiencies in food preservation with the order: PAXO coating + CaCl2 ≈ PAXO coating > PAXO film > sterile water. All the results indicated that the as-prepared PAXO film or PAXO solution could be good candidates in packaging preservation.