ABSTRACT
AIM To study the chemical constituents from Polygonum posumbu.METHODS The 95％ ethanol extract from P.posumbu was isolated and purified by silica,Sephadex LH-20 and recrystallization,then the structures of obtained compounds were identified by physicochemical properties and spectral data.RESULTS Fourteen compounds were isolated and identified as n-hexacosanol (1),n-tetradecanoic acid (2),β-sitosterol (3),daucosterol (4),gallic acid (5),quercetin-3-O-(2″-O-galloyl)-β-D-glucopyranoside (6),quercetin-3-O-β-D-glucopyranoside (7),quercetin (8),o-phthalic acid bis-(2-ethyl decyl)-ester (9),inositol (10),sucrose (11),succinic acid (12),n-butyl-β-D-fructopyranoside (13),α-D-glucose (14).CONCLUSION Compounds 1,2,9,10 and 14 are isolated from genus Polygonum for the first time,compounds 1-14 are isolated from this plant for the first time
ABSTRACT
AIM To study the chemical constituents of Fallopia multiflora (Thunb.) Harald.var.cillinerve (Nakai) A.J.Li.METHODS The 95％ ethanol extract of the roots from F.multiflora was isolated and purified by silica column and Sephadex LH-20,then the structures of obtained compounds were identified by physicochemical properties and spectral data.RESULTS Ten compounds were isolated and identified as β-sitosterol (1),daucosterol (2),gallic acid (3),succinic acid (4),α-D-glucose (5),Annulatin 3'-O-β-D-xyloside (6),kaempferitrin (7),inotodisaccharide (8),n-butyl-β-D-fructopyranoside (9),erythritol (10).CONCLUSION Compounds 6-10 are isolated from genus Fallopia for the first time,compounds 3-10 are isolated from this plant for the first time.
ABSTRACT
AIM To study the chemical constituents of the secondary metabolites of endophytic fungi DL02 from Saposhnikovia divaricata (Turcz.) Schischk.and their biological activities.METHODS The ethyl acetate and methanol extract leavening from S.divaricata was isolated and purified by silica and Sephadex LH-20,then the structures of obtained compounds were identified by physicochemical properties and spectral data.The antifungal and antibacterial activities were determined by the minimum inhibitory concentration method.RESULTS Seven compounds were isolated and identified as β-sitosterol (1),kojic acid (2),stigmasta-7,22-diene-3β,5α,6α-triol (3),uracil (4),allantoin (5),erythritol (6) and adenosine (7).Compound 4 had strong inhibitory effects on pseudomonas aeruginosa with the MIC values of 31.3 μg/mL.CONCLUSION Compounds 2-5 and 7 are isolated from this fungus for the first time.Compounds 4-5 have strong biological activities.
ABSTRACT
<p><b>OBJECTIVE</b>To investigate the constituents of Ervatamia hainanensis systematically.</p><p><b>METHOD</b>Various chromatographic techniques were applied to isolate and purify the constituents of this plant. The structures were elucidated by spectroscopic analysis.</p><p><b>RESULT</b>Eight compounds were obtained, which were identified as alpha-amyrin acetate (1), 11-oxo-alpha-amyrin acetate (2), beta-sitosterol (3), cycloart-23-ene-3beta, 25-diol(4), cycloart-25-ene-3beta, 24-diol (5), 5alpha, 8alpha-epidioxyergosta-6, 22-dien-3beta-ol (6), ibogamin-3-one (7), beta-daucosterol (8).</p><p><b>CONCLUSION</b>Compounds 1, 2, 4- 7 were isolated from this plant for the first time.</p>