Determination of Deoxynivalenol in Four Traditional Chinese Herbal Medicines by LC-MS-MS / 中国药师
China Pharmacist
; (12): 578-581, 2014.
Article
in Zh
| WPRIM
| ID: wpr-447352
Responsible library:
WPRO
ABSTRACT
Objective:To develop a method for determining deoxynivalenol in four kinds of traditional Chinese herbal medicines. Methods:After being extracted by water, purified by an immunoaffinity column, deoxynivalenol was analyzed by LC-MS-MS. Results:The calibration curve was linear within the range of 2-50 ng·ml-1 for deoxynivalenol. The recovery was 68. 7%-88. 3%. Conclusion:The method is simple, sensitive and accurate in the determination of deoxynivalenol in Semen Ziziphi Spinosae, Semen Sojae Praepara-tum, Semen Coicis and Fructus Psoraleae.
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Index:
WPRIM
Language:
Zh
Journal:
China Pharmacist
Year:
2014
Type:
Article