InP high power monolithically integrated widely tunable laser and SOA array for hybrid integration.

We present a monolithic InP-based photonic integrated circuit (PIC) consisting of a widely tunable laser master oscillator feeding an array of integrated semiconductor optical amplifiers that are interferometrically combined on-chip in a single-mode waveguide. We demonstrate a stable and efficient on-chip coherent beam combination and obtain up to 240 mW average power from the monolithic PIC, with 30-50 kHz Schawlow-Townes linewidths and >180 mW average power across the extended C-band. We also explored hybrid integration of the InP-based laser and amplifier array PIC with a high quality factor silicon nitride microring resonator. We observe lasing based on gain from the interferometrically combined amplifier array in an external cavity formed via feedback from the silicon nitride microresonator chip; this configuration results in narrowing of the Schawlow-Townes linewidth to ∼3 kHz with 37.9 mW average power at the SiN output facet. This work demonstrates a new approach toward high power, narrow linewidth sources that can be integrated with on-chip single-mode waveguide platforms for potential applications in nonlinear integrated photonics.

Design of a broadband Ge1-xSix electro-absorption modulator based on the Franz-Keldysh effect with thermal tuning.

We present the design of an adiabatic taper coupled Ge1-xSix electro-absorption modulator, which is based on Franz-Keldysh effect. The device has an active region of 0.8×50 µm2, an extinction ratio of more than 6 dB and an insertion loss less than 3 dB at the wavelength of 1550 nm. The operating bandwidth can be broadened to more than 90 nm by an AlN block assisted heater with only 6.2 mW energy consumption. Moreover, the operating wavelength shift caused by material composition deviation can be compensated to the expected wavelength by thermal tuning. This design may play an important role in next-generation, high-density optical integrations for datacom and high-performance computing.

Characterizing pump line phase offset of a single-soliton Kerr comb by dual comb interferometry.

We report phase retrieval of a single-soliton Kerr comb using electric field cross-correlation implemented via dual-comb interferometry. The phase profile of the Kerr comb is acquired through the heterodyne beat between the Kerr comb and an electro-optic comb with a pre-characterized phase profile. The soliton Kerr comb has a nearly flat phase profile, and the pump line is observed to show a phase offset which depends on the pumping parameters. The experimental results are in agreement with numerical simulations.

50-GHz-spaced comb of high-dimensional frequency-bin entangled photons from an on-chip silicon nitride microresonator.

Quantum frequency combs from chip-scale integrated sources are promising candidates for scalable and robust quantum information processing (QIP). However, to use these quantum combs for frequency domain QIP, demonstration of entanglement in the frequency basis, showing that the entangled photons are in a coherent superposition of multiple frequency bins, is required. We present a verification of qubit and qutrit frequency-bin entanglement using an on-chip quantum frequency comb with 40 mode pairs, through a two-photon interference measurement that is based on electro-optic phase modulation. Our demonstrations provide an important contribution in establishing integrated optical microresonators as a source for high-dimensional frequency-bin encoded quantum computing, as well as dense quantum key distribution.

Observation of Breathing Dark Pulses in Normal Dispersion Optical Microresonators.

Breathers are localized waves in nonlinear systems that undergo a periodic variation in time or space. The concept of breathers is useful for describing many nonlinear physical systems including granular lattices, Bose-Einstein condensates, hydrodynamics, plasmas, and optics. In optics, breathers can exist in either the anomalous or the normal dispersion regimes, but they have only been characterized in the former, to our knowledge. Here, externally pumped optical microresonators are used to characterize the breathing dynamics of localized waves in the normal dispersion regime. High-Q optical microresonators featuring normal dispersion can yield mode-locked Kerr combs whose time-domain waveform corresponds to circulating dark pulses in the cavity. We show that with relatively high pump power these Kerr combs can enter a breathing regime, in which the time-domain waveform remains a dark pulse but experiences a periodic modulation on a time scale much slower than the microresonator round trip time. The breathing is observed in the optical frequency domain as a significant difference in the phase and amplitude of the modulation experienced by different spectral lines. In the highly pumped regime, a transition to a chaotic breathing state where the waveform remains dark-pulse-like is also observed, for the first time to our knowledge; such a transition is reversible by reducing the pump power.

Solasodine inhibits human colorectal cancer cells through suppression of the AKT/glycogen synthase kinase-3ß/ß-catenin pathway.

Solasodine is a main active component isolated from Solanum incanum L. that performs a wide range of functions containing anti-oxidant, anti-infection, and neurogenesis promotion. In this study, we explored the influence of solasodine on three types of human colorectal cancer (CRC) cell lines. The results show that solasodine prohibited CRC cell proliferation dose- and time-dependently and impeded CRC cell motility by downregulating MMPs. Solasodine was also found to fuel caspase-cascade reaction and increase the ratio between Bax and Bcl-2 so as to induce CRC cell apoptosis. When cells were pretreated with AKT activator (insulin-like growth factor-1) followed by solasodine, the solasodine-induced apoptosis was partially abrogated by insulin-like growth factor-1. Moreover, solasodine hindered tumor development and stimulated similar mechanisms in vivo. In general, our study provides the first evidence that solasodine has a suppressive effect on CRC cells and that this agent may be a novel therapeutic drug for CRC treatment.

Long-haul coherent communications using microresonator-based frequency combs.

Microresonator-based frequency combs are strong contenders as light sources for wavelength-division multiplexing (WDM). Recent experiments have shown the potential of microresonator combs for replacing a multitude of WDM lasers with a single laser-pumped device. Previous demonstrations have however focused on short-distance few-span links reaching an impressive throughput at the expense of transmission distance. Here we report the first long-haul coherent communication demonstration using a microresonator-based comb source. We modulated polarization multiplexed (PM) quadrature phase-shift keying-data onto the comb lines allowing transmission over more than 6300 km in a single-mode fiber. In a second experiment, we reached beyond 700 km with the PM 16 quadrature amplitude modulation format. To the best of our knowledge, these results represent the longest fiber transmission ever achieved using an integrated comb source.

Direct soliton generation in microresonators.

We investigate, numerically and experimentally, the effect of thermo-optical (TO) chaos on soliton generation dynamics in microresonators. Numerical simulations that include the thermal dynamics show that the generated solitons can either survive or annihilate when the pump laser is scanned from blue to red and then stop at a fixed wavelength; the outcome is stochastic and is strongly related to the number of solitons generated. The random fluctuations of the cavity resonance occurring under TO chaos are also found to trigger delayed spontaneous soliton generation after the laser scan ends, which could enable soliton excitation with slow laser tuning speed. Stochastic soliton annihilation/survival, as well as delayed spontaneous soliton generation, is observed experimentally in a silicon-nitride microresonator.

Soliton repetition rate in a silicon-nitride microresonator.

The repetition rate of a Kerr comb composed of a single soliton in an anomalous group velocity dispersion silicon-nitride microcavity is measured as a function of pump frequency. By comparing operation in the soliton and non-soliton states, the contributions from the Raman soliton self-frequency shift (SSFS) and the thermal effects are evaluated; the SSFS is found to dominate the changes in the repetition rate, similar to silica cavities. The relationship between the changes in the repetition rate and the pump frequency detuning is found to be independent of the nonlinearity coefficient and dispersion of the cavity. Modeling of the repetition rate change by using the generalized Lugiato-Lefever equation is discussed; the Kerr shock is found to have only a minor effect on repetition rate for cavity solitons with duration down to ∼50 fs.

Broadband second-harmonic phase-matching in dispersion engineered slot waveguides.

Parametric optical nonlinearities are usually weak and require both high optical field intensity and phase-matching. Micro/nanophotonics, with strong confinement of light in waveguides of nanometer-scale cross-sections, can provide high field intensity, but is still in need of a solution for phase-matching across a broad bandwidth. In this article, we show that mode-coupling in slot waveguides can engineer the waveguide modal dispersion, and with proper choice of materials, can achieve on-chip broadband second-harmonic phase-matching. A phase-matching bandwidth in the range of 220 nm at mid-infrared can occur for a hetero-slot waveguide consisting of aluminum nitride (AlN) and silicon nitride (SiN). With a high-nonlinearity polymer as cladding material, about 1.76 W(-1)cm(-2) of normalized conversion efficiency in second-harmonic-generation (SHG) and about 23 dB signal gain in degenerate optical parametric amplification (DOPA) can be achieved over a broad bandwidth. An asymmetric-slot waveguide configuration and a thermal tuning scheme are proposed to reduce the fabrication difficulty. This concept of broadband second-harmonic phase-matching can be extended to other nonlinear optical frequency mixing processes, thus expanding the scope of on-chip nonlinear optical applications.

Strip-slot direct mode coupler.

We present a direct strip-slot waveguide mode coupler without any auxiliary structures. Contrary to popular belief, an apparent mode mismatch between strip and slot waveguide does not deteriorate conversion efficiency. Separated electric and magnetic field distributions in a slot waveguide lead to highly efficient modal coupling in the direct strip-slot coupler and result in high conversion efficiency. Accurate experimental characterization shows that the direct strip-slot waveguide mode coupler is capable of up to 96% conversion efficiency with a broad bandwidth. Being simplest and of high efficiency, the direct strip-slot waveguide mode coupler can encourage potential applications of slot waveguides.

Intracavity characterization of micro-comb generation in the single-soliton regime.

Soliton formation in on-chip micro-comb generation balances cavity dispersion and nonlinearity and allows coherent, low-noise comb operation. We study the intracavity waveform of an on-chip microcavity soliton in a silicon nitride microresonator configured with a drop port. Whereas combs measured at the through port are accompanied by a very strong pump line which accounts for >99% of the output power, our experiments reveal that inside the microcavity, most of the power is in the soliton. Time-domain measurements performed at the drop port provide information that directly reflects the intracavity field. Data confirm a train of bright, close to bandwidth-limited pulses, accompanied by a weak continuous wave (CW) background with a small phase shift relative to the comb.

Thermal tuning of Kerr frequency combs in silicon nitride microring resonators.

Microresonator based Kerr frequency comb generation has many attractive features, including ultrabroad spectra, chip-level integration, and low power consumption. Achieving precise tuning control over the comb frequencies will be important for a number of practical applications, but has been little explored for microresonator combs. In this paper, we characterize the thermal tuning of a coherent Kerr frequency comb generated from an on-chip silicon nitride microring. When the microring temperature is changed by ~70 °C with an integrated microheater, the line spacing and center frequency of the comb are tuned respectively by -253 MHz (-3.57 MHz/°C) and by -175 GHz (-2.63 GHz/°C); the latter constitutes 75% of the comb line spacing. From these results we obtain a shift of 25 GHz (362.07 MHz/°C) in the comb carrier-envelope offset frequency. Numerical simulations are performed by taking into account the thermo-optic effects in the waveguide core and cladding. The temperature variation of the comb line spacing predicted from simulations is close to that observed in experiments. The time-dependent thermal response of the microheater based tuning scheme is characterized; time constants of 30.9 µs and 0.71 ms are observed.

Observation of Fermi-Pasta-Ulam Recurrence Induced by Breather Solitons in an Optical Microresonator.

We present, experimentally and numerically, the observation of Fermi-Pasta-Ulam recurrence induced by breather solitons in a high-Q SiN microresonator. Breather solitons can be excited by increasing the pump power at a relatively small pump phase detuning in microresonators. Out of phase power evolution is observed for groups of comb lines around the center of the spectrum compared to groups of lines in the spectral wings. The evolution of the power spectrum is not symmetric with respect to the spectrum center. Numerical simulations based on the generalized Lugiato-Lefever equation are in good agreement with the experimental results and unveil the role of stimulated Raman scattering in the symmetry breaking of the power spectrum evolution. Our results show that optical microresonators can be exploited as a powerful platform for the exploration of soliton dynamics.

Polarization rotation and coupling between silicon waveguide and hybrid plasmonic waveguide.

We present a polarization rotation and coupling scheme that rotates a TE(0) mode in a silicon waveguide and simultaneously couples the rotated mode to a hybrid plasmonic (HP(0)) waveguide mode. Such a polarization rotation can be realized with a partially etched asymmetric hybrid plasmonic waveguide consisting of a silicon strip waveguide, a thin oxide spacer, and a metal cap made from copper, gold, silver or aluminum. Two implementations, one with and one without the tapering of the metal cap are presented, and different taper shapes (linear and exponential) are also analyzed. The devices have large 3 dB conversion bandwidths (over 200 nm at near infrared) and short length (< 5 µm), and achieve a maximum coupling factor of ∼ 78% with a linearly tapered silver metal cap.

A silicon-on-insulator polarization diversity scheme in the mid-infrared.

We propose a silicon-on-insulator (SOI) polarization diversity scheme in the mid-infrared wavelength range. In consideration of absorption loss in silicon dioxide (SiO2), the polarization splitter-rotator (PSR) is designed and optimized with silicon nitride (SiN) upper-cladding and SiO2 lower-cladding. This asymmetry allows the PSR, which consists of mode-conversion tapers and subsequent mode-sorting asymmetric Y-junctions, to be fabricated with a simple one-step etching process. Simulation shows that our PSR has good performance with low mode conversion loss (< 0.25 dB) and low crosstalk (< -18 dB) in a very large wavelength range from 4.0 µm to 4.4 µm. The PSR also exhibits large fabrication tolerance with respect to the size deviations in waveguide width, height and refractive index of the upper-cladding. Additionally, PSR devices based on Y-junctions with SiO2 upper-cladding, and SiN upper- and lower-claddings are designed for potential applications at shorter and longer wavelengths, respectively. These PSR devices could facilitate the development of silicon photonic devices in the mid-infrared.

Broadband and fabrication-tolerant on-chip scalable mode-division multiplexing based on mode-evolution counter-tapered couplers.

A broadband and fabrication-tolerant on-chip scalable mode-division multiplexing (MDM) scheme based on mode-evolution counter-tapered couplers is designed and experimentally demonstrated on a silicon-on-insulator (SOI) platform. Due to the broadband advantage offered by mode evolution, the two-mode MDM link exhibits a very large, -1 dB bandwidth of >180 nm, which is considerably larger than most of the previously reported MDM links whether they are based on mode-interference or evolution. In addition, the performance metrics remain stable for large-device width deviations from the designed valued by -60 nm to 40 nm, and for temperature variations from -25°C to 75°C. This MDM scheme can be readily extended to higher-order mode multiplexing and a three-mode MDM link is measured with less than -10 dB crosstalk from 1.46 to 1.64 µm wavelength range.

Ligand-Free Pd-Catalyzed Double Carbonylation of Aryl Iodides with Amines to α-Ketoamides under Atmospheric Pressure of Carbon Monoxide and at Room Temperature.

A general Pd-catalyzed double carbonylation of aryl iodides with secondary or primary amines to produce α-ketoamides at atmospheric CO pressure has been developed. This transformation proceeds successfully even at room temperature and in the absence of any ligand and additive. A wide range of aryl iodides and amines can be coupled to the desired α-ketoamides in high yields with excellent chemoselectivities. Importantly, the current methodology has been demonstrated to be applied in the synthesis of bioactive molecules and chiral α-ketoamides.

Copper nanorod array assisted silicon waveguide polarization beam splitter.

We present the design of a three-dimensional (3D) polarization beam splitter (PBS) with a copper nanorod array placed between two silicon waveguides. The localized surface plasmon resonance (LSPR) of a metal nanorod array selectively cross-couples transverse electric (TE) mode to the coupler waveguide, while transverse magnetic (TM) mode passes through the original input waveguide without coupling. An ultra-compact and broadband PBS compared to all-dielectric devices is achieved with the LSPR. The output ports of waveguides are designed to support either TM or TE mode only to enhance the extinction ratios. Compared to silver, copper is fully compatible with complementary metal-oxide-semiconductor (CMOS) technology.

Design of a SiO2 top-cladding and compact polarization splitter-rotator based on a rib directional coupler.

A compact polarization splitter-rotator based on a silicon-on-insulator rib asymmetrical directional coupler with SiO2 top-cladding is proposed. Unlike previously reported PSRs which specifically required the top-cladding material to be different from the bottom cladding in order to break the symmetry of the waveguide cross-section, our proposed PSR has no such limitation on the top-cladding due to the horizontal asymmetry of the rib waveguide. In addition, the device is highly compact and has a total length as short as 24 µm. Numerical simulation shows that a high conversion efficiency of ~97% is obtained at the wavelength of 1550 nm. With the width variation of ± 15 nm and the gap variation of ± 50 nm, the PSR still has high ER of 12 dB at the cross-port, showing large fabrication tolerance. This device can be cascaded to improve the performance at the through port and an example of a two-stage PSR is presented. The mode conversion between the strip waveguide and the rib waveguide is also discussed.