Effect of resin composite shade on digital fiber-optic transillumination imaging in vitro.

Digital imaging fiber-optic transillumination (DIFOTI) devices have been used to detect caries, a technique without using X-rays. However, the effects of resin composites (RCs) shades on the images acquired with DIFOTI devices have not been investigated. Thus, this study aimed to elucidate the influence of RC shade on the images obtained with DIFOTI technique. Three shades (A1, A3, and Opaque) for each of four flowable RCs were filled on a cavity prepared in a left mandibular first premolar obtained from a donated body. Then, transmission images with a DIFOTI device (DIAGNOcam; KaVo, Biberach, Germany) were acquired, and the average lightness values of the images in the RC and enamel were used to calculate differences between those areas. To clarify the influence of the optical translucency and color on DIFOTI images, the color parameters (L*, a* and b*) of each RC were obtained with black and white backgrounds. The color differences between the backgrounds were calculated as transparency parameter (TP) values. The number of repetitions was set to 10. Differences in the lightness value of the shades varied in each RC. The difference in lightness was significantly associated with the TP value and color parameters of L* (p < 0.01), with negative (R = - 0.81) and positive (R = 0.84) correlations, respectively. In conclusion, DIFOTI images of RCs with high optical translucency resembled those of the natural tooth structure.

Effect of speed sintering of monolithic zirconia with different yttria contents on color and crystal phase.

This study evaluated the color and microstructure of monolithic zirconia crowns with different yttrium oxide (Y2 O3 ) contents treated by conventional or speed sintering. Four types of zirconia ceramics were assessed: two monolayer zirconia, and two multilayer zirconia. The monolithic zirconia crowns were fabricated using a dental computer-aided design/computer-aided manufacturing (CAD/CAM) system and in two shades (A2 and BL). After milling, the zirconia crowns were sintered using either speed sintering or conventional sintering. For each combination of zirconia (4), shade (2), and sintering condition (2), the color parameters were determined at three positions of each of nine crowns using a non-contact dental spectrophotometer. In addition, the zirconia phases in the specimens were quantified using X-ray diffractometry. Significant differences in the ΔE00 values at different measurement positions were observed for the Multi2 crown of the BL shade group. The color difference resulting from conventional and speed sintering programs was not affected by the difference in yttria content of Mono1, Mono2, and Multi1. However, in Multi2, containing 3Y-TZP and 5Y-PSZ, a color change was caused by the use of speed sintering. Therefore, when performing speed sintering with Multi2, it is necessary to select the color in consideration of these results or take measures for staining.

Effect of fiber post length and abutment height on fracture resistance of endodontically treated premolars prepared for zirconia crowns.

The purpose of this study was to compare the fracture resistance, mode of fracture, and stress distribution of endodontically treated teeth prepared with three different fiber post lengths and two different abutment heights, using both experimental and finite element (FE) approaches. Forty-eight human maxillary premolars with two roots were selected and endodontically treated. The teeth were randomly distributed into six equally sized groups (n = 8) with different combinations of post lengths (7.5, 11, and 15 mm) and abutment heights (3 and 5 mm). All the teeth restored with glass fiber post (Rely X Fiber Post, 3M ESPE, USA) and a full zirconia crown. All the specimens were thermocycled and then loaded to failure at an oblique angle of 135°. Statistical analysis was performed for the effects of post length and abutment height on failure loads using ANOVA and Tukey's honestly significant difference test. In addition, corresponding FE models of a premolar restored with a glass fiber post were developed to examine mechanical responses. The factor of post length (P < 0.01) had a significant effect on failure load. The abutment height (P > 0.05) did not have a significant effect on failure load. The highest mean fracture resistance was recorded for the 15 mm post length and 5 mm abutment height test group, which was significantly more resistant to fracture than the 7.5 mm post and 5 mm abutment height group (P < 0.05). The FE analysis showed the peak compression and tension stress values of 7.5 mm post length were higher than that of 11 and 15 mm post length. The stress value of remaining tooth decreased as the post length was increased. Within the limitations of this experimental and FE analysis study, increasing the post length inside the root of endodontically treated premolar teeth restored with glass-fiber posts increase the fracture resistance to non-axial forces. Failure mode is more favorable with reduced abutment heights.

Influence of increment thickness on light transmission, degree of conversion and micro hardness of bulk fill composites.

This study evaluated characteristics of light transmission, degree of monomer conversion and surface microhardness of bulk fill, conventional and fiber-reinforced resin based composites (RBCs) through different incremental thicknesses of resin composite. Working hypotheses was that there are differences in transmission of blue light through RBCs of different kinds and that the thickness of the increments influence the degree of monomer conversion of RBCs. Six bulk fill, three conventional nanohybrid, one short fiber reinforced and one flowable RBCs were evaluated. For each material, four different incremental thicknesses (1, 2, 3 and 4 mm) were considered (n = 5). The specimens were prepared in cylindrical Teflon molds that are open at the top and the bottom sides and cured for 40 s by applying the curing unit. After curing process, the specimens were ground with a silicon carbide paper with a grit size of 1200 and 4000, and then stored dry at 37 °C for 24 h. Light transmission, degree of monomer conversion, surface microhardness were measured and data were analyzed using ANOVA (p = 0.05). There were differences in light transmission of resin composites of various types and brands. Low-viscous bulk fill and short fiber-reinforced RBCs presented higher light transmission compared to resin composites of higher viscosity. Reduced light transmission and lower surface microhardness and DC % at bottom side of the specimen suggests that more attention needs to be paid to ensure proper curing of the resin composite in deep cavities.

Effect of accelerated aging on the fracture toughness of zirconias.

STATEMENT OF PROBLEM: Low temperature degradation (LTD) of yttria-stabilized tetragonal zirconia polycrystals (Y-TZP) is of concern. PURPOSE: The purpose of this in vitro study was to assess the effect of accelerated aging on the Vickers hardness and fracture toughness of a newly developed Y-TZP and 2 primary Y-TZPs. MATERIAL AND METHODS: Two primary 3 mol% Y-TZP, Lava (LA), Everest Zirconium Soft (EV), and a new 3 mol% Y-TZP, ZirTough (NZ) were assessed. Specimens (n=30 each brand) of 10 × 10 × 3 mm were hydrothermally treated for accelerated aging to examine LTD. Five conditions were used (n = 5 per condition) as follows: control group (no aging); 5 hours at 134°C/0.2 MPa (5h-134°C); 100 hours at 134°C/0.2 MPa (100 h-134°C); 5 hours at 180°C/1.0 MPa (5 h-180°C); and 20 hours at 180°C/1.0 MPa (20 h-180°C). Fracture toughness was measured by using the indentation fracture (IF) method under a loading of 294 N and calculated from the obtained measurements. To observe differences in particle composition and fracture patterns, mirror-polished test specimens (n=5 each brand) were re-sintered at 1200°C for 1 hour as a thermal etching process, and a Vickers indenter was pressed into the test specimens according to the IF method. Test piece surfaces and cracks were observed with scanning electron microscopy (SEM). One-way ANOVA and the post- hoc (Scheffé test were used to examine) interlevel significant differences (α=.05). RESULTS: The Vickers hardness and fracture toughness were as follows: 1319 HV and 7.36 MPa · m(1/2) for LA, and 1371 HV and 6.76 MPa · m(1/2) for EV in no aging; 1334 HV and 7.02 MPa · m(1/2) for LA, and 1346 HV and 6.07 MPa · m(1/2) for EV in 5h-134°C. No significant differences were found between no aging and 5h-134°C for LA and EV for Vickers hardness and fracture toughness. Measurements could not be made for LA and EV for 100 h-134°C, 5h-180°C, or 20 h-180°C because of fractures in the surface layer. For NZ, Vickers hardness and fracture toughness were as follows: 1261 HV and 15.60 MPa · m(1/2) in no aging; 1217 HV and 14.98 MPa · m(1/2) in 5h-134°C; 1231 HV and 15.13 MPa · m(1/2) in 100 h-134°C; 1252 HV and 15.51 MPa · m(1/2) in 5h-180°C; 1224 HV and 15.01 MPa · m(1/2) in 20 h-180°C. No significant differences were shown in the Vickers hardness and fracture toughness. SEM observations after the thermal etching processing of NZ showed zirconia particles and scattered alumina particles. CONCLUSION: Measurements with LA and EV could only be made for no aging and 5h-134°C, and no significant differences were found in Vickers hardness and fracture toughness. Measurements were made with NZ under all conditions and no significant differences were found in Vickers hardness and fracture toughness.

Three-dimensional finite element analysis of anterior two-unit cantilever resin-bonded fixed dental prostheses.

The aim of this study was to evaluate the influence of different framework materials on biomechanical behaviour of anterior two-unit cantilever resin-bonded fixed dental prostheses (RBFDPs). A three-dimensional finite element model of a two-unit cantilever RBFDP replacing a maxillary lateral incisor was created. Five framework materials were evaluated: direct fibre-reinforced composite (FRC-Z250), indirect fibre-reinforced composite (FRC-ES), gold alloy (M), glass ceramic (GC), and zirconia (ZI). Finite element analysis was performed and stress distribution was evaluated. A similar stress pattern, with stress concentrations in the connector area, was observed in RBFDPs for all materials. Maximal principal stress showed a decreasing order: ZI>M>GC>FRC-ES>FRC-Z250. The maximum displacement of RBFDPs was higher for FRC-Z250 and FRC-ES than for M, GC, and ZI. FE analysis depicted differences in location of the maximum stress at the luting cement interface between materials. For FRC-Z250 and FRC-ES, the maximum stress was located in the upper part of the proximal area of the retainer, whereas, for M, GC, and ZI, the maximum stress was located at the cervical outline of the retainer. The present study revealed differences in biomechanical behaviour between all RBFDPs. The general observation was that a RBFDP made of FRC provided a more favourable stress distribution.

Structural stability of posterior retainer design for resin-bonded prostheses: a 3D finite element study.

The purpose of this in vitro study was to compare the stress distribution and natural frequency of different shape and thickness retainer designs for maxillary posterior resin-bonded prostheses using finite element (FE) method. A 3D FE model of a three unit posterior resin-bonded prosthesis analysis model was generated. Three different shaped retainer designs, viz. C-shaped (three axial surface wraparounds), D-shaped (three axial surface wraparounds with central groove) and O-shaped (360° wraparounds), and three different thicknesses, viz., 0.4, 0.8, and 1.2 mm, resin-bonded prostheses were used in this study. The resin-bonded prosthesis analysis model was imported into an FE analysis software (ANSYS 10.0, ANSYS, USA) and attribution of material properties. The nodes at the bottom surface of the roots were assigned fixed zero displacement in the three spatial dimensions. A simulated angle of 45° loading of a 100 N force was applied to the node of the pontic lingual cusp surface. The stress distributions and corresponding natural frequencies were analyzed and resolved. The C-shaped retainer for 0.4 mm thickness recorded the greatest von Mises stresses of 71.4 MPa for all three groups. C-shaped, D-shaped and O-shaped retainer presented natural frequencies 3,988, 7,754, and 10,494 Hz, respectively. D-shaped retainer and O-shaped retainer increased natural frequencies and structural rigidity over the traditional C-shaped retainer. The maximum von Mises stresses values of the remaining tooth and prosthesis decreased with greater retainer thickness. D-shaped retainer and O-shaped retainer increased natural frequencies and structural rigidity over the traditional C-shaped retainer.

Reliability of mixed dentition space analysis using a digital model obtained from an optical impression: a preliminary study.

OBJECTIVE: While mixed dentition space analysis is a common practice in pediatric dentistry, digital models created using an intraoral scanner are not as widely used in clinical settings. This preliminary study used a very small sample size with one reference model and aimed to (1) compare the accuracy of mixed dentition space analysis using a digital model obtained from an optical impression with that of conventional plaster model-based analysis and (2) assess inter-examiner differences. RESULTS: The space required for the mandibular permanent canine and premolars and arch length discrepancy were calculated using each model. The largest significant difference between plaster- and digital model-based analyses was identified when the right arch length discrepancy was considered (-0.49 mm; 95% confidence interval: -0.95-0.03); however, the value was considered clinically insignificant. Significant inter-examiner differences were observed for six items of the plaster model; however, no such differences were observed when using the digital model. In conclusion, digital model space analysis may have the same level of accuracy as conventional plaster model analysis and likely results in smaller inter-examiner differences than plaster model analysis.

Effect of low-temperature degradation and sintering protocols on the color of monolithic zirconia crowns with different yttria contents.

This study investigated the effects of low-temperature degradation (LTD) on the L*, a*, and b* values of highly translucent zirconia crowns. Four types of zirconia disks with different yttria contents (IPS e.max ZirCAD LT, IPS e.max ZirCAD MT, IPS e.max ZirCAD MT Multi, IPS e.max ZirCAD Prime, Ivoclar) and two shades (A2 and BL) were used. A crown was manufactured using four types of zirconia and LTD treated. Color measurements were performed, and the color difference (ΔE00) before and after LTD was calculated. The microstructure was determined through X-ray fluorescence and X-ray diffractometry. Highly translucent zirconia crowns showed greater changes in the a* and b* values than in the L* value after LTD, regardless of the shade. The Multi2 crowns exhibited a discernible color change due to the LTD treatment. The X-ray fluorescence results did not reveal any apparent change in the microstructure between sintering programs for all zirconia specimens.

Effect of water temperature on cyclic fatigue properties of glass-fiber-reinforced hybrid composite resin and its fracture pattern after flexural testing.

PURPOSE: To evaluate in vitro the influence of dynamic loading applied to a glass-fiber-reinforced hybrid composite resin on its flexural strength in a moist, simulated oral environment. MATERIALS AND METHODS: Three-point flexural strength specimens were subjected to cyclic loading in water at 37°C and 55°C to investigate the influence of immersion temperature on impact fatigue properties. Specimens were subjected to cyclic impact loading at 1 Hz for up to 5 × 105 cycles to obtain the number of cycles to failure, the number of unbroken specimens after 5 × 105 cycles, and the residual flexural strength of unbroken specimens. Maximum loads of 100, 200, and 300 N were chosen for both the non-reinforced and the glass-fiber reinforced hybrid composite resins. RESULTS: The mean residual flexural strength for 100 N impact loading at temperatures of 37°C and 55°C was 634 and 636 MPa, respectively. All specimens fractured at fewer than 5 × 105 cycles for loads of 200 and 300 N. CONCLUSION: Reduced numbers of cycles to fracture and lower fatigue values were observed as both the maximum load and immersion temperature increased.

Composite resin reinforced with pre-tensioned fibers: a three-dimensional finite element study on stress distribution.

Pre-tensioned construction material is utilized in engineering applications of high strength demands. The purpose of this study was to evaluate the effect of the pre-tensioning fibers of fiber-reinforced composite (FRC) using three-dimensional finite element (FE) analysis. The 3D FE models of particulate composite resin (CR), FRC and composite resin reinforced with pre-tensioned fibers (PRE-T-FRC) were constructed. The uniaxial three-point bending test was simulated using FE analysis to calculate the principal stress distribution. In the FRC and PRE-T-FRC, stresses were higher than CR, and they were located in the fiber. However, the maximum principal stress value at the composite of PRE-T-FRC was lower than the FRC and CR. Composite resin reinforced with pre-tensioned fibers was advantageous for stress distribution and lowering the stress at the composite itself. Experimental studies on physical properties of pre-tensioned FRC are encouraged to be conducted.

Accuracy of three-dimensional finite element modeling using two different dental cone beam computed tomography systems.

The aim of this study is to evaluate the accuracy of dental ceramic object three dimensional (3D) finite element model constructed directly from two different dental cone beam computed tomography (CT) systems. CT scanned one 10.0 × 10.0 × 20.0 mm block and one 8.0 × 10.0 × 40.0 mm block of an 8-step wedge. All 3D finite element (FE) models were created from CT images. Each 3D FE model measured the length of the directions X, Y, and Z that corresponded to an original specimen using the measurement function between two points on the Mechanical Finder software package. The measurements and practical value were compared with the CT image and the accuracy of the reproduced measurements was examined. No significant differences were found between Alphard-3030 on the Z axis and ProMax 3D on the Y axis of the block. In addition, there were also no significant differences observed between Alphard-3030 on the Y axis and ProMax 3D on the X axis compared with Alphard-3030 on the Z axis and ProMax 3D on the Y axis for the step-wedge. The results suggest that measurement of the dimensions of cone beam CT images could be useful in applications where both good reproducibility and accuracy of FE models are required.

Influence of toothbrush abrasion on the surface characteristics of CAD/CAM composite resin blocks with shade gradations.

Crown restorations in anterior region are recommended highly color-reproductivity because of aesthetic reason. Composite resin block with several shade gradations is especially produced for anterior restorations. To clarify the durability of an aesthetic, the effect of toothbrush abrasion on surface properties was performed. Composite-resin blocks without shade gradation and a ceramic block were used as controls. All specimens were prepared using #2000 SiC paper and polished using an aluminum oxide polishing paste. Toothbrush abrasion tests were carried out for 20,000 cycles at a frequency of 2 Hz with 2.0 N load. Gloss and surface roughness were measured before and after toothbrush abrasion. The number of repetitions was set to five. It was clarified that tooth brushing caused to decrease in the gloss and to increase in the surface roughness with significant negative correlations between these results not only in composite-resin blocks without shade gradation but also in those with gradation.

The Effects of Different Molding Orientations, Highly Accelerated Aging, and Water Absorption on the Flexural Strength of Polyether Ether Ketone (PEEK) Fabricated by Fused Deposition Modeling.

Rising prices are currently a problem in the world. In particular, the abnormal increases in the price of metals, which are often used in dental prosthetics, have increased the burden of dental costs on the public. There is therefore an urgent need to develop prosthetic devices made from materials that are not affected by the global situation and that have excellent biocompatibility and mechanical properties comparable to those of metals. Polyether ether ketone (PEEK) is a promising alternative to metal in dentistry. This study compared the effects of different molding orientations, highly accelerated aging, and water absorption on the flexural strength of PEEK fabricated by fused deposition modeling (FDM) and examined its potential for dental applications. The flexural strength of PEEK stacked at 0° to the molding stage (0° PF), with and without highly accelerated aging, was significantly greater than for the other molding orientations. As with PD, the maximum test load for 0° PF was measured without fracture. PEEK stacked at 45° (45° PF) and 90° (90° PF) to the molding stage easily fractured, as the applied load pulled the stacked layers. No statistically significant difference was found between the flexural strength of 45° PF and 90° PF. The flexural strength decreased under all conditions due to defects in the crystal structure of PEEK caused by highly accelerated aging.

Mechanical and surface properties of additive manufactured zirconia under the different building directions.

PURPOSE: This study investigates the mechanical and surface properties of zirconia manufactured using additive manufacturing (AM) technology and the effect of the building direction on the mechanical and surface properties. METHODS: Specimens were prepared using ZrO2 paste (3DMix ZrO2; 3DCeram) and a three-dimensional printing system (CeraMaker 900; 3DCeram) based on the principles of stereolithography (SLA). The mechanical properties (flexural strength, Vickers hardness, fracture toughness, elastic modulus, and Poisson's ratio) and surface properties (chemical composition and surface observation) were evaluated for three building directions (parallel, diagonal, and perpendicular) to investigate the relationship between the building directions and the anisotropy of the mechanical and surface properties of SLA-manufactured zirconia. Statistical analysis was performed using a one-way analysis of variance and Tukey's honestly significant difference test. RESULTS: The highest flexural strength was obtained for a perpendicular building direction. The flexural strength was significantly higher in the perpendicular direction than in the parallel and diagonal directions; it was also significantly higher in the diagonal direction than in the parallel direction (P<0.05). The Vickers hardness, fracture toughness, elastic modulus, Poisson's ratio, and chemical composition did not differ significantly. Microstructural observations revealed that the layers, large crystals, and pores were more prominent in the parallel direction. CONCLUSIONS: The flexural strength and surface structure of the tested SLA-manufactured zirconia were influenced by the building direction; however, other mechanical properties remained unaffected. The layer boundaries affected the anisotropic behavior of the builds to a certain extent, owing to the layer-by-layer production method.

The effect of low-temperature degradation and building directions on the mechanical properties of additive-manufactured zirconia.

This study aimed to investigate the effect of low-temperature degradation (LTD) on the mechanical properties of additive-manufactured zirconia. In addition, the mechanical properties of additive-manufactured were compared with those before aging under similar experimental conditions. This study prepared stereolithography apparatus fabricated zirconia specimens with flexural strength, modulus of elasticity, Vickers hardness, and fracture toughness. The specimen position data were set as parallel (0°), diagonal (45°), and perpendicular (90°) to the direction of the building. The LTD condition was 5 h under 134ºC and 0.2 MPa in an autoclave. It was found that the 0° direction differed significantly from all other conditions before and after aging, and the highest flexural strength was obtained when the additive specimen was manufactured perpendicular to the building direction. However, the results indicate that there is a negligible effect of aging on the mechanical properties of additive-manufactured zirconia.

Effect of 3D printing system and post-curing atmosphere on micro- and nano-wear of additive-manufactured occlusal splint materials.

Although additive manufacturing has been widely applied for occlusal splint (OS) fabrication, it is still unclear whether 3D printing system and post-curing atmosphere would play a role in the wear resistance of additive-manufactured OS. Therefore, the aim of this study was to evaluate the effect of 3D printing system (liquid crystal display (LCD) and digital light processing (DLP)) and post-curing atmosphere (air and nitrogen gas (N2)) on the wear resistance of hard and soft OS materials for additive-manufactured OSs (KeySplint® Hard and Soft). The evaluated properties were microwear (by two-body wear test) and nano-wear resistances (by nanoindentation wear test) as well as flexural strength and flexural modulus (by three-point bending test), surface microhardness (by Vickers hardness test), and nanoscale elastic modulus (reduced elastic modulus) and nano surface hardness (by nanoindentation test). For the hard material, the surface microhardness, microwear resistance, reduced elastic modulus, nano surface hardness, and nano-wear resistance were significantly affected by the printing system (p < 0.05), while all the evaluated properties except flexural modulus were significantly affected by the post-curing atmosphere (p < 0.05). Meanwhile, both the printing system and post-curing atmosphere significantly affected all the evaluated properties (p < 0.05). The specimens additive-manufactured by DLP printer tended to show higher wear resistance in the hard material groups and lower wear resistance in the soft material groups when compared to those by LCD printer. The post-curing at N2 atmosphere significantly enhanced the microwear resistance of hard material groups additive-manufactured by the DLP printer (p < 0.05) and soft material groups additive-manufactured by the LCD printer (p < 0.01), while it significantly enhanced the nano-wear resistance of both hard and soft material groups regardless of the printing system (p < 0.01). It can be concluded that 3D printing system and post-curing atmosphere affect the micro- and nano-wear resistance of tested additively manufactured OS materials. In addition, it can be also concluded that the optical printing system providing higher wear resistance depends on the material type, and using nitrogen gas as a protection gas during post-curing enhances the wear resistance of tested materials.

Finite element analysis to compare stress distribution of connector of lithia disilicate-reinforced glass-ceramic and zirconia-based fixed partial denture.

This study used finite element method to analyze the stress distribution in connector of ceramic-based bilayer structures, in simulation of dental crown-like structures with a functional but weak veneer layer bonded onto a strong core layer. The purpose of this study was to evaluate the stress distribution at veneer/core interface of 2 different core materials [Yttria-stabilized tetragonal zirconia polycrystals (Y-TZP) and lithia disilicate-reinforced glass-ceramic] using three-dimensional finite element analysis. Within the limitations of this study, finite element analysis showed that stress concentrations were located at the veneer/core interface of the connector in Y-TZP core models. The general observation was that compared with Y-TZP, lithia disilicate-reinforced glass-ceramic showed a relatively stable stress value and had a minor effect on the stress concentration susceptibility.

Application of fused deposition modeling technology for fabrication jigs of three-point bending test for dental composite resins.

This study aimed to clarify the application possibility of the fused deposition modeling (FDM) technology on the fabrication of jigs for a flexural test of dental composite resins (CRs). Three types of jigs were prepared to carry out three-point bending tests; 3D printed jig including support rollers, 3D printed jig with stainless-steel support rollers, and stainless-steel jig and stainless-steel support rollers. An FDM 3D printer with polylactic acid filament was used to produce 3D printed jigs. For evaluation of flexural strength, two types, packable and flowable, of composite resins were selected to prepare specimens. Three-point bending tests were performed using a universal testing machine. Then flexural strength and flexural elastic modulus were calculated. Specimen preparation and three-point bending test were conducted according to the ISO 4049:2019. All experiments were repeated 20 times. Flexural strength and flexural elastic modulus of packable CR were significantly larger than those of flowable. However, there were no significant differences among the jigs in both results. Consequently, FDM technology could be applied to fabricate jigs for the flexural test of CRs, and the mechanical properties could be evaluated as accurately as a stainless-steel jig.

Effect of cyclic impact load on shear bond strength of zirconium dioxide ceramics.

PURPOSE: To investigate the influence of cyclic impact load and the number of load cycles on compressive shear bond strength under the three different cements. MATERIALS AND METHODS: The following materials were used: Super Bond C&B (SB) and Panavia Fluoro Cement (PF) as adhesive resin cements, Fuji Luting (FL) as a resin-modified glass-ionomer cement, and zirconium dioxide ceramics as adherend. Before the shear bond test, three different impact loading conditions (compressive direction, shear direction, and no impact) and the number of load cycles (1 to 106 cycles), were performed. A total of 189 specimens (n = 3/group) were randomly assigned to groups and tested. A cyclic impact test was performed by applying a load of 98N at a distance of 40 mm and a loading cycle frequency of 1 Hz. All results were statistically analyzed with two-way ANOVA and Tukey's multiple comparison test. RESULTS: Shear bond strengths of SB, PF, and FL subjected to no cyclic impact load were 21.6 to 53.8 MPa in SB, 27.0 to 63.6 MPa in PF, and 20.0 to 35.9 MPa in FL. The shear bond strength of SB and PF increased to a certain degree from one to 105 cycles, while FL did likewise from one to 104 cycles. CONCLUSION: The shear bond strengths of SB, PF, and FL were greatest without cyclic impact, followed by compressive and then shear cyclic impact.