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Nat Methods ; 12(3): 244-50, 3 p following 250, 2015 Mar.
Artículo en Inglés | MEDLINE | ID: mdl-25599551

RESUMEN

Specific labeling of biomolecules with bright fluorophores is the keystone of fluorescence microscopy. Genetically encoded self-labeling tag proteins can be coupled to synthetic dyes inside living cells, resulting in brighter reporters than fluorescent proteins. Intracellular labeling using these techniques requires cell-permeable fluorescent ligands, however, limiting utility to a small number of classic fluorophores. Here we describe a simple structural modification that improves the brightness and photostability of dyes while preserving spectral properties and cell permeability. Inspired by molecular modeling, we replaced the N,N-dimethylamino substituents in tetramethylrhodamine with four-membered azetidine rings. This addition of two carbon atoms doubles the quantum efficiency and improves the photon yield of the dye in applications ranging from in vitro single-molecule measurements to super-resolution imaging. The novel substitution is generalizable, yielding a palette of chemical dyes with improved quantum efficiencies that spans the UV and visible range.


Asunto(s)
Colorantes Fluorescentes/química , Microscopía Ultravioleta/métodos , Imagen Molecular/métodos , Azetidinas/química , Técnicas de Química Sintética , Cumarinas/química , Fluoresceína/química , Colorantes Fluorescentes/análisis , Colorantes Fluorescentes/síntesis química , Células HeLa , Humanos , Modelos Moleculares , Teoría Cuántica , Rodaminas/química , Espectrometría de Fluorescencia , Espectrofotometría Ultravioleta/métodos , Relación Estructura-Actividad
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