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XANES/EPR Evidence of the Oxidation of Nickel(II) Quinolinylpropioamide and Its Application in Csp3 -H Functionalization.
Hao, Wenyan; Sha, Yuchen; Deng, Yi; Luo, Yi; Zeng, Li; Tang, Shan; Weng, Yue; Chiang, Chien-Wei; Lei, Aiwen.
Afiliación
  • Hao W; National Research Center for Carbohydrate Synthesis, Jiangxi Normal University, Nanchang, 330022, P.R. China.
  • Sha Y; College of Chemistry and Molecular Sciences, Institute for Advanced Studies (IAS), Wuhan University, Wuhan, 430072, P.R. China.
  • Deng Y; College of Chemistry and Molecular Sciences, Institute for Advanced Studies (IAS), Wuhan University, Wuhan, 430072, P.R. China.
  • Luo Y; College of Chemistry and Molecular Sciences, Institute for Advanced Studies (IAS), Wuhan University, Wuhan, 430072, P.R. China.
  • Zeng L; College of Chemistry and Molecular Sciences, Institute for Advanced Studies (IAS), Wuhan University, Wuhan, 430072, P.R. China.
  • Tang S; College of Chemistry and Molecular Sciences, Institute for Advanced Studies (IAS), Wuhan University, Wuhan, 430072, P.R. China.
  • Weng Y; College of Chemistry and Molecular Sciences, Institute for Advanced Studies (IAS), Wuhan University, Wuhan, 430072, P.R. China.
  • Chiang CW; National Synchrotron Radiation Research Center (NSRRC), Hsinchu Science Park, Hsinchu, Taiwan.
  • Lei A; College of Chemistry and Molecular Sciences, Institute for Advanced Studies (IAS), Wuhan University, Wuhan, 430072, P.R. China.
Chemistry ; 25(19): 4931-4934, 2019 Apr 01.
Article en En | MEDLINE | ID: mdl-30768816
ABSTRACT
An in situ generated oxidation species of nickel quinolinylpropioamide intermediate was produced. Characterization by X-ray absorption near edge structure (XANES) and EPR provides complementary insights into this oxidized nickel species. With aliphatic amides and isocyanides as substrates, a nickel-catalyzed facile synthesis of structurally diverse five-membered lactams could be achieved.
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Texto completo: 1 Colección: 01-internacional Banco de datos: MEDLINE Idioma: En Revista: Chemistry Asunto de la revista: QUIMICA Año: 2019 Tipo del documento: Article
Texto completo
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XML
PubMed Links
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Texto completo: 1 Colección: 01-internacional Banco de datos: MEDLINE Idioma: En Revista: Chemistry Asunto de la revista: QUIMICA Año: 2019 Tipo del documento: Article