Preparation and characterization of active Cirish fructans-fish gelatin film: Physicochemical, antioxidant, and antimicrobial properties.

This study was aimed to evaluate the film-forming ability and characterization of ultrasonically extracted Cirish fructans (CF) and CF-cold-water fish gelatin (G) composite films. The film-forming solutions were prepared at different levels (CF100-0G, CF75-G25, CF50-G50, CF25-G75, and CF0-G100) and the corresponding data were analyzed based on one-way analysis of variance. The results indicated that CF addition led to an impressive increase in composite films thickness (69.38-86.45 µm), moisture content (16.05%-27.8%), surface hydrophobicity, tensile strength (5.73-17.89 MPa), elongation at break (0.83%-1.66%), Young's modulus (77.12-88.15 MPa), and Tg (38.83-47.4°C) which CF75-G25 had the highest values. Meanwhile, the solubility (77.12%-88.15%), WVP (1.89-2.86 × 10-10gm-1 s-1 Pa-1), and oxygen permeability (1.53-3.26 × 1014 cm3 m-1 s-1 Pa-1) of the composite films decreased. The FTIR spectra indicated the protein-polysaccharide interactions and revealed that the secondary structure of gelatin was shifted from triple-helix structure (1661 cm-1) toward α-helix structure (1650-1657 cm-1) when CF was incorporated. The microstructure observations indicated that unlike gelatin film, CF film exhibited the smooth and uniform surface without cracks and phase separation. It was found that CF films had high total phenolic content (6.73 mg GEA g-1) and showed DPPH radical scavenging activity (67.86%). On the other hand, it showed inherent antimicrobial activity against both gram-positive and gram-negative bacteria. The results indicated that CF and CF-cold fish gelatin have great potential as active films with improved physical, mechanical, and barrier properties.

Loading lime by-product into derivative cellulose carrier for food enrichment.

The objective here is to enrich orange juice through encapsulated lime by-product extract (LBE) through freeze-drying, in order to increase lime by-product consumption, in addition to increasing nutrition value of orange juice. The properties of both the LBE and microparticles are measured. The total polyphenolic compound (TPC) was measured to be 34.5 ± 0.5 (mg gallic acid/g LBE). The obtained value of encapsulation efficiency (EE) was within the 55%-70% range. The encapsulation method was satisfactory. The particle size is within 10-21 µm range, and differences between all treatments were statistically notable (p < 0.05). The lack of melting peaks in the thermal profiles by differential scanning calorimeter (DSC) of microparticles confirmed that hesperidin was well embedded in the polymeric cover. According to the sensory evaluations of orange juice which was enriched with LBE microparticles, the bitter taste was not perceived in some treatments.