How reproducible is the acoustical characterization of porous media?

There is a considerable number of research publications on the characterization of porous media that is carried out in accordance with ISO 10534-2 (International Standards Organization, Geneva, Switzerland, 2001) and/or ISO 9053 (International Standards Organization, Geneva, Switzerland, 1991). According to the Web of ScienceTM (last accessed 22 September 2016) there were 339 publications in the Journal of the Acoustical Society of America alone which deal with the acoustics of porous media. However, the reproducibility of these characterization procedures is not well understood. This paper deals with the reproducibility of some standard characterization procedures for acoustic porous materials. The paper is an extension of the work published by Horoshenkov, Khan, Bécot, Jaouen, Sgard, Renault, Amirouche, Pompoli, Prodi, Bonfiglio, Pispola, Asdrubali, Hübelt, Atalla, Amédin, Lauriks, and Boeckx [J. Acoust. Soc. Am. 122(1), 345-353 (2007)]. In this paper, independent laboratory measurements were performed on the same material specimens so that the naturally occurring inhomogeneity in materials was controlled. It also presented the reproducibility data for the characteristic impedance, complex wavenumber, and for some related pore structure properties. This work can be helpful to better understand the tolerances of these material characterization procedures so improvements can be developed to reduce experimental errors and improve the reproducibility between laboratories.

Reproducibility experiments on measuring acoustical properties of rigid-frame porous media (round-robin tests).

This paper reports the results of reproducibility experiments on the interlaboratory characterization of the acoustical properties of three types of consolidated porous media: granulated porous rubber, reticulated foam, and fiberglass. The measurements are conducted in several independent laboratories in Europe and North America. The studied acoustical characteristics are the surface complex acoustic impedance at normal incidence and plane wave absorption coefficient which are determined using the standard impedance tube method. The paper provides detailed procedures related to sample preparation and installation and it discusses the dispersion in the acoustical material property observed between individual material samples and laboratories. The importance of the boundary conditions, homogeneity of the porous material structure, and stability of the adopted signal processing method are highlighted.

Acoustical measurement of the shear modulus for thin porous layers.

Simulations performed with the Biot theory show that for thin porous layers, a shear mode of the structure can be induced by a point-source in air located close to the layer. The simulations show that this mode is present around frequencies where the quarter wavelength of the shear Biot wave is equal to the thickness of the samples and show that it can be acoustically detected from the fast variations with frequency of the location of a pole of the reflection coefficient close to grazing incidence. The mode has been detected with this method for two reticulated plastic foams. For one of the foams studied, the velocity and the damping of the Rayleigh wave have been measured on a thicker layer of the same medium at higher frequencies, giving a real part of the shear modulus close to the one obtained from the measured location of the pole. The strong coupling of the shear mode with the acoustic field in air allows the measurement of the shear modulus without mechanical excitation.