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1.
Guang Pu Xue Yu Guang Pu Fen Xi ; 22(4): 689-90, 2002 Aug.
Artigo em Chinês | MEDLINE | ID: mdl-12938402

RESUMO

This paper report the development of the determination of Na in anticoagulant sodium heparin by flame atomic absorption spectrophotometry. The method is convenient and the results show good precision and accuracy. The relative standard deviation (RSD) is 2.4% and the rate of recovery is 100.9%.


Assuntos
Anticoagulantes/química , Heparina/química , Sódio/análise , Sensibilidade e Especificidade , Espectrofotometria Atômica/métodos
2.
Guang Pu Xue Yu Guang Pu Fen Xi ; 22(4): 691-2, 2002 Aug.
Artigo em Chinês | MEDLINE | ID: mdl-12938403

RESUMO

Trace metal selenium in milk cow serums has determined by graphite furnace atomic absorption spectrometry with matrix modifier. It's found that addition the solution of 0.1% Ni(NO3)2 as matrix modifier, the ash temperature will increase up to 1,000 degrees C. 600 degrees C is practically used for ash temperature. D2 lamp is used for background correction. Selenium in milk cow serums was directly determined after addition of 0.1% Ni(NO3)2 without digestion. The method is convenient to determine element in milk cow serum. The results show that the method has good precision and accuracy. The relative standard deviation of selenium. Determination was 4.9%, and the rates of recovery were 93.3%-104%.


Assuntos
Selênio/sangue , Animais , Bovinos , Feminino , Grafite , Lactação/metabolismo , Espectrofotometria Atômica/métodos
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