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1.
Food Chem ; 444: 138674, 2024 Jun 30.
Artigo em Inglês | MEDLINE | ID: mdl-38335687

RESUMO

To develop rapid detection techniques for liquid eggs' adulteration, three types of adulterations were considered: water dilution, manipulation of yolk ratio in whole egg, and blending different varieties of egg white or yolk. Objective: Establish detection techniques utilizing colorimetry, electrochemistry, and interfacial fingerprinting for these adulterations, respectively. Results: Colorimetry allows for detection (1 min·sample-1) of water dilution through linear (R2 ≥ 0.984) and exponential fitting (R2 ≥ 0.992); Electrochemistry enables detection (6 min·sample-1, R2 ≥ 0.979) of the adulteration of yolk ratio in whole egg; Interfacial fingerprinting technique effectively detects (detection duration: 10 min·sample-1, detection limit: 1.0-10.0 wt%) the adulteration of different varieties of egg white. Subsequently, through 3D-fluorescence microscopy (interface height variation: 22.49-573.45 µm), interfacial tension variation (65.54-35.48 mN·m-1), contact angle variation (89.7°-32.9°), particle size range (free water: 0.94-14.29 µm; protein aggregation: 6.57-10.76 µm), and etc., interfacial fingerprinting mechanism was elucidated. This research contributes novel insights into the detection of adulteration in liquid eggs.


Assuntos
Galinhas , Colorimetria , Animais , Eletroquímica , Ovos/análise , Água , Gema de Ovo
2.
Materials (Basel) ; 11(10)2018 Sep 25.
Artigo em Inglês | MEDLINE | ID: mdl-30257477

RESUMO

The laser scanning strategy has an important influence on the surface quality, residual stress, and deformation of the molten metal (deformation behavior). A divisional scanning strategy is an effective means used to reduce the internal stress of the selective laser melting (SLM) metal part. In order to understand and optimize the divisional scanning strategy, three divisional scanning strategies and an S-shaped orthogonal scanning strategy are used to produce 316L steel parts in this study. The influence of scanning strategy on the produced parts is verified from the aspects of densification, residual stress distribution and deformation. Experiments show that the 316L steel alloy parts adopted spiral divisional scanning strategy can not only obtain the densification of 99.37%, but they also effectively improve the distribution of residual stress and control the deformation degree of the produced parts. Among them, the spiral divisional scanning sample has the smallest residual stress in plane direction, and its σx and σy stress are controlled within 204 MPa and 103 MPa. The above results show that the spiral divisional scanning is the most conducive strategy to obtain higher residual stress performance of SLM 316L steel parts.

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