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2.
Rev Sci Instrum ; 94(7)2023 Jul 01.
Artigo em Inglês | MEDLINE | ID: mdl-37477554

RESUMO

Laser-driven x-ray backlighting can be used to image fast dynamic processes like the propagation of laser-driven shock waves in matter. We demonstrate and evaluate the feasibility of operating the JUNGFRAU detector designed by PSI, a direct detecting x-ray detector, in environments with extreme electromagnetic pulses. The electromagnetic pulse-protective housing is specifically designed for this detector and optimized for pump-probe experiments at the Petawatt High-Energy Laser for Heavy Ion EXperiments (PHELIX) facility at the GSI Helmholtzzentrum für Schwerionenforschung GmbH. The beryllium x-ray entrance window of the protective housing has a high x-ray transmission of 94% at 8 keV. Measurements have shown that the housing simultaneously provides a relative damping of the electromagnetic field on average higher than 1000 in the frequency range of 100 MHz to 5 GHz. The results demonstrate the feasibility of operating digital detectors in experiments where strong electromagnetic pulses are present.

3.
J Imaging ; 8(9)2022 Aug 24.
Artigo em Inglês | MEDLINE | ID: mdl-36135392

RESUMO

If ancient documents are too fragile to be opened, X-ray imaging can be used to recover the content non-destructively. As an extension to conventional attenuation imaging, dark-field imaging provides access to microscopic structural object information, which can be especially advantageous for materials with weak attenuation contrast, such as certain metal-free inks in paper. With cotton paper and different self-made inks based on authentic recipes, we produced test samples for attenuation and dark-field imaging at a metal-jet X-ray source. The resulting images show letters written in metal-free ink that were recovered via grating-based dark-field imaging. Without the need for synchrotron-like beam quality, these results set the ground for a mobile dark-field imaging setup that could be brought to a library for document scanning, avoiding long transport routes for valuable historic documents.

4.
J Synchrotron Radiat ; 29(Pt 3): 794-806, 2022 May 01.
Artigo em Inglês | MEDLINE | ID: mdl-35511012

RESUMO

The advent of hard X-ray free-electron lasers enables nanoscopic X-ray imaging with sub-picosecond temporal resolution. X-ray grating interferometry offers a phase-sensitive full-field imaging technique where the phase retrieval can be carried out from a single exposure alone. Thus, the method is attractive for imaging applications at X-ray free-electron lasers where intrinsic pulse-to-pulse fluctuations pose a major challenge. In this work, the single-exposure phase imaging capabilities of grating interferometry are characterized by an implementation at the I13-1 beamline of Diamond Light Source (Oxfordshire, UK). For comparison purposes, propagation-based phase contrast imaging was also performed at the same instrument. The characterization is carried out in terms of the quantitativeness and the contrast-to-noise ratio of the phase reconstructions as well as via the achievable spatial resolution. By using a statistical image reconstruction scheme, previous limitations of grating interferometry regarding the spatial resolution can be mitigated as well as the experimental applicability of the technique.

5.
J Imaging ; 7(9)2021 Sep 05.
Artigo em Inglês | MEDLINE | ID: mdl-34564104

RESUMO

X-ray backlighters allow the capture of sharp images of fast dynamic processes due to extremely short exposure times. Moiré imaging enables simultaneously measuring the absorption and differential phase-contrast (DPC) of these processes. Acquiring images with one single shot limits the X-ray photon flux, which can result in noisy images. Increasing the photon statistics by repeating the experiment to gain the same image is not possible if the investigated processes are dynamic and chaotic. Furthermore, to reconstruct the DPC and transmission image, an additional measurement captured in absence of the object is required. For these reference measurements, shot-to-shot fluctuations in X-ray spectra and a source position complicate the averaging of several reference images for noise reduction. Here, two approaches of processing multiple reference images in combination with one single object image are evaluated regarding the image quality. We found that with only five reference images, the contrast-to-noise ratio can be improved by approximately 13% in the DPC image. This promises improvements for short-exposure single-shot acquisitions of rapid processes, such as laser-produced plasma shock-waves in high-energy density experiments at backlighter X-ray sources such as the PHELIX high-power laser facility.

6.
Sci Rep ; 11(1): 4574, 2021 02 25.
Artigo em Inglês | MEDLINE | ID: mdl-33633184

RESUMO

Detailed imaging of the three-dimensionally complex architecture of xylary plants is important for studying biological and mechanical functions of woody plants. Apart from common two-dimensional microscopy, X-ray micro-computed tomography has been established as a three-dimensional (3D) imaging method for studying the hydraulic function of wooden plants. However, this X-ray imaging method can barely reach the resolution needed to see the minute structures (e.g. pit membrane). To complement the xylem structure with 3D views at the nanoscale level, X-ray near-field nano-holotomography (NFH) was applied to analyze the wood species Pinus sylvestris and Fagus sylvatica. The demanded small specimens required focused ion beam (FIB) application. The FIB milling, however, influenced the image quality through gallium implantation on the cell-wall surfaces. The measurements indicated that NFH is appropriate for imaging wood at nanometric resolution. With a 26 nm voxel pitch, the structure of the cell-wall surface in Pinus sylvestris could be visualized in genuine detail. In wood of Fagus sylvatica, the structure of a pit pair, including the pit membrane, between two neighboring fibrous cells could be traced tomographically.

7.
Opt Express ; 28(9): 13553-13568, 2020 Apr 27.
Artigo em Inglês | MEDLINE | ID: mdl-32403827

RESUMO

The combination of grating-based phase-contrast imaging with X-ray microscopy can result in a complicated image formation. Generally, transverse shifts of the interference fringes are nonlinearly dependent on phase differences of the measured wave front. We present an iterative reconstruction scheme based on a regularized maximum likelihood cost function that fully takes this dependency into account. The scheme is validated by numerical simulations. It is particularly advantageous at low photon numbers and when the premises for deconvolution-based reconstructions are not met. Our reconstruction scheme hence enables a broader applicability of X-ray grating interferometry in imaging and wave front sensing.

8.
Opt Express ; 28(4): 5248-5256, 2020 Feb 17.
Artigo em Inglês | MEDLINE | ID: mdl-32121749

RESUMO

The challenge of astronomical intensity interferometry is to detect the small photon-bunching signals of distant sources with a broad optical bandwidth. We have built a Hanbury Brown-Twiss-like laboratory intensity interferometer with a focus on a relatively broad bandwidth (1nm FWHM optical filter) and high photon rates (up to 10MHz) per channel compared to typical (non-astronomical) intensity interferometry applications. As a light source we use a green LED to simulate starlight. The LED has proven to be a compact high-power source of stochastic light with a special advantage of a small emission area, which favours spatial coherence. Using single-photon correlations, we detect a bunching signal in the second-order correlation function with a coherence time of <1ps and an amplitude of <4⋅10-4 and describe signal and background quantitatively for a 40 hours measurement. In this paper we show our setup, present the correlation measurements and compare them to theoretical expectations.

9.
J Imaging ; 6(7)2020 Jul 03.
Artigo em Inglês | MEDLINE | ID: mdl-34460656

RESUMO

For imaging events of extremely short duration, like shock waves or explosions, it is necessary to be able to image the object with a single-shot exposure. A suitable setup is given by a laser-induced X-ray source such as the one that can be found at GSI (Helmholtzzentrum für Schwerionenforschung GmbH) in Darmstadt (Society for Heavy Ion Research), Germany. There, it is possible to direct a pulse from the high-energy laser Petawatt High Energy Laser for Heavy Ion eXperiments (PHELIX) on a tungsten wire to generate a picosecond polychromatic X-ray pulse, called backlighter. For grating-based single-shot phase-contrast imaging of shock waves or exploding wires, it is important to know the weighted mean energy of the X-ray spectrum for choosing a suitable setup. In propagation-based phase-contrast imaging the knowledge of the weighted mean energy is necessary to be able to reconstruct quantitative phase images of unknown objects. Hence, we developed a method to evaluate the weighted mean energy of the X-ray backlighter spectrum using propagation-based phase-contrast images. In a first step wave-field simulations are performed to verify the results. Furthermore, our evaluation is cross-checked with monochromatic synchrotron measurements with known energy at Diamond Light Source (DLS, Didcot, UK) for proof of concepts.

10.
Phys Ther Sport ; 25: 89-93, 2017 May.
Artigo em Inglês | MEDLINE | ID: mdl-28190632

RESUMO

OBJECTIVE: The study aimed to investigate the changes of the perceived area of tape contact during a lumbar tape application that lasted 7 days. DESIGN: Single group, repeated measures study. SETTING: University research laboratory. PARTICIPANTS: Twenty-three healthy collegiate students in sports science. MAIN OUTCOME MEASURES: Perceived area of tape contact was collected by preparing a drawing of their individual perceived tape outline into a printed body image. Measurements were obtained immediately after fixation of the tape (day 0), at day 3 and day 7 during application and 5 min after the release of the application (day 7). RESULTS: There was no significant change of the perceived area of tape contact after 3 days of tape application. A significant decrease in the perceived area of tape contact was detected 7 days after application (p < 0.05) and after detaching the tape (p < 0.01) compared to the first measurement. CONCLUSIONS: Our results indicate that the perception of the area of tape contact of healthy sport students is decreased at 7 days. This effect could not be observed at 3 days. These results provide relevant information for the use of elastic tapes concerning the duration of application in medical therapy.


Assuntos
Fita Atlética , Região Lombossacral , Tato , Adulto , Feminino , Humanos , Masculino , Percepção , Adulto Jovem
11.
Phys Rev Lett ; 114(2): 021101, 2015 Jan 16.
Artigo em Inglês | MEDLINE | ID: mdl-25635539

RESUMO

In the standard diffusive picture for transport of cosmic rays (CRs), a gradient in the CR density induces a typically small, dipolar anisotropy in their arrival directions. This is being widely advertised as a tool for finding nearby sources. However, the predicted dipole amplitude at TeV and PeV energies exceeds the measured one by almost 2 orders of magnitude. Here, we critically examine the validity of this prediction, which is based on averaging over an ensemble of turbulent magnetic fields. We focus on (1) the deviations of the dipole in a particular random realization from the ensemble average, and (2) the possibility of a misalignment between the regular magnetic field and the CR gradient. We find that if the field direction and the gradient direction are close to ∼90°, the dipole amplitude is considerably suppressed and can be reconciled with observations, which sheds light on a long-standing problem. Furthermore, we show that the dipole direction in general does not coincide with the gradient direction, thus hampering the search for nearby sources.

12.
Proc Natl Acad Sci U S A ; 112(40): 12264-71, 2015 Oct 06.
Artigo em Inglês | MEDLINE | ID: mdl-24821791

RESUMO

The details of what constitutes the majority of the mass that makes up dark matter in the Universe remains one of the prime puzzles of cosmology and particle physics today-80 y after the first observational indications. Today, it is widely accepted that dark matter exists and that it is very likely composed of elementary particles, which are weakly interacting and massive [weakly interacting massive particles (WIMPs)]. As important as dark matter is in our understanding of cosmology, the detection of these particles has thus far been elusive. Their primary properties such as mass and interaction cross sections are still unknown. Indirect detection searches for the products of WIMP annihilation or decay. This is generally done through observations of γ-ray photons or cosmic rays. Instruments such as the Fermi large-area telescope, high-energy stereoscopic system, major atmospheric gamma-ray imaging Cherenkov, and very energetic radiation imaging telescope array, combined with the future Cherenkov telescope array, will provide important complementarity to other search techniques. Given the expected sensitivities of all search techniques, we are at a stage where the WIMP scenario is facing stringent tests, and it can be expected that WIMPs will be either be detected or the scenario will be so severely constrained that it will have to be rethought. In this sense, we are on the threshold of discovery. In this article, I will give a general overview of the current status and future expectations for indirect searches of dark matter (WIMP) particles.

13.
Nano Lett ; 13(12): 6189-96, 2013.
Artigo em Inglês | MEDLINE | ID: mdl-24274328

RESUMO

Free-standing semiconductor nanowires in combination with advanced gate-architectures hold an exceptional promise as miniaturized building blocks in future integrated circuits. However, semiconductor nanowires are often corrupted by an increased number of close-by surface states, which are detrimental with respect to their optical and electronic properties. This conceptual challenge hampers their potentials in high-speed electronics and therefore new concepts are needed in order to enhance carrier mobilities. We have introduced a novel type of core-shell nanowire heterostructures that incorporate modulation or remote doping and hence may lead to high-mobility electrons. We demonstrate the validity of such concepts using inelastic light scattering to study single modulation-doped GaAs/Al0.16Ga0.84As core-multishell nanowires grown on silicon. We conclude from a detailed experimental study and theoretical analysis of the observed spin and charge density fluctuations that one- and two-dimensional electron channels are formed in a GaAs coaxial quantum well spatially separated from the donor ions. A total carrier density of about 3 × 10(7) cm(-1) and an electron mobility in the order of 50,000 cm(2)/(V s) are estimated. Spatial mappings of individual GaAs/Al0.16Ga0.84As core-multishell nanowires show inhomogeneous properties along the wires probably related to structural defects. The first demonstration of such unambiguous 1D- and 2D-electron channels and the respective charge carrier properties in these advanced nanowire-based quantum heterostructures is the basis for various novel nanoelectronic and photonic devices.


Assuntos
Arsenicais/química , Gálio/química , Nanofios/química , Semicondutores , Cristalização , Elétrons , Nanotecnologia , Pontos Quânticos/química , Silício/química
14.
Nano Lett ; 13(7): 3011-6, 2013 Jul 10.
Artigo em Inglês | MEDLINE | ID: mdl-23701454

RESUMO

We report on resonant Raman experiments carried out on wurtzite InAs nanowires. Resonant conditions have been obtained by tuning either the excitation energy or the band gap through external high pressure at fixed excitation energy. A complete azimuthal study of the Raman spectra with two laser excitation lines (2.41 and 1.92 eV) has also been performed on a single wire. The measured E2(H) mode resonance indicates that the E1(A) gap is about 2.4 eV, which is considerably reduced with respect to the zinc-blende InAs E1 gap. These findings confirm recent theoretical calculations of crystal phase induced bandstructure modifications.

15.
Nano Lett ; 13(4): 1522-7, 2013 Apr 10.
Artigo em Inglês | MEDLINE | ID: mdl-23517063

RESUMO

By employing various high-resolution metrology techniques we directly probe the material composition profile within GaAs-Al0.3Ga0.7As core-shell nanowires grown by molecular beam epitaxy on silicon. Micro Raman measurements performed along the entire (>10 µm) length of the [111]-oriented nanowires reveal excellent average compositional homogeneity of the nominally Al0.3Ga0.7As shell. In strong contrast, along the radial direction cross-sectional scanning transmission electron microscopy and associated chemical analysis reveal rich structure in the AlGaAs alloy composition due to interface segregation, nanofaceting, and local alloy fluctuations. Most strikingly, we observe a 6-fold Al-rich substructure along the corners of the hexagonal AlGaAs shell where the Al-content is up to x ~ 0.6, a factor of 2 larger than the body of the AlGaAs shell. This is associated with facet-dependent capillarity diffusion due to the nonplanarity of shell growth. A modulation of the Al-content is also found along the radial [110] growth directions of the AlGaAs shell. Besides the ~10(3)-fold enhancement of the photoluminescence yield due to inhibition of nonradiative surface recombination, the AlGaAs shell gives rise to a broadened band of sharp-line luminescence features extending ~150-30 meV below the band gap of Al0.3Ga0.7As. These features are attributed to deep level defects under influence of the observed local alloy fluctuations in the shell.


Assuntos
Ligas/química , Arsenicais/química , Gálio/química , Nanofios/química , Cristalização , Luminescência , Nanoestruturas/química , Tamanho da Partícula , Silício/química , Propriedades de Superfície
16.
ACS Nano ; 7(2): 1400-7, 2013 Feb 26.
Artigo em Inglês | MEDLINE | ID: mdl-23281738

RESUMO

We report on a major modification of the fundamental electronic band structure of AlAs when grown as a nanoscaled wurtzite crystal. Resonant Raman spectra of individual AlAs-GaAs core-shell nanowires display a resonance between 1.83 and 2.18 eV for the AlAs E1(TO) phonon mode. Our findings substantiate the lowest conduction band of wurtzite AlAs to comprise Γ8 symmetry and a low effective mass in agreement with calculations reported recently. The electronic resonance falls below the X, L, and Γ valleys known for AlAs in the zincblende phase. This result points toward a direct nature of wurtzite AlAs and is expected to apply more generally to semiconductors that in the bulk phase exhibit L valleys at lower energies than the conduction band at the Γ point.

17.
Opt Express ; 17(20): 17450-6, 2009 Sep 28.
Artigo em Inglês | MEDLINE | ID: mdl-19907529

RESUMO

We report on the development of a terahertz time-domain technique for measuring the momentum relaxation time of charge carriers in ultrathin semiconductor layers. Making use of the Drude model, our phase sensitive modulation technique directly provides the relaxation time. Time-resolved THz experiments were performed on n-doped GaAs and show precise agreement with data obtained by electrical characterization. The technique is well suited for studying novel materials where parameters such as the charge carriers' effective mass or the carrier density are not known a priori.


Assuntos
Algoritmos , Teste de Materiais/métodos , Membranas Artificiais , Modelos Teóricos , Semicondutores , Espectroscopia Terahertz/métodos , Simulação por Computador , Radiação Terahertz
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