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1.
Foods ; 13(4)2024 Feb 08.
Artigo em Inglês | MEDLINE | ID: mdl-38397497

RESUMO

The effects of hot air (HAD), vacuum (VAD) and conductive (CD) drying on the chemical and textural profiles of Cucurbita maxima pulp were investigated to find suitable drying conditions to avoid postharvest losses of pumpkin. The results showed that the drying methods had a significant effect (p < 0.05) on the chemical and textural profiles of pumpkin pulp. The ash content was lower in VAD (up to 7.65%) than in HAD (up to 9.88%) and CD pulp (up to 9.21%). The samples of HAD, CD and VAD had a higher fat content, up to 3.07, 2.66 and 2.51%, respectively, than fresh pulp (1.55%). The total fibre content is lower for VAD (up to 8.78%) than for HAD (up to 15.43%) and CD pulp (13.94%). HAD pulp at 70 °C (~15.51%) and VAD and CD pulp processed between 50 and 60 °C (~22%) are good sources of protein. HAD and CD pulp at 70 °C and VAD at 50 °C resulted in a high sugar content (up to 83.23%). In addition to drying, the extraction time of 40 min used in ultrasound-assisted extraction is optimal, especially for protein and sugar recovery in dried samples. Drying also led to strong changes in the textural properties of the pulp, so that an excellent dried intermediate product is the one obtained using HAD at a temperature of 70 °C and an airflow of 0.5 m/s.

2.
Plant Foods Hum Nutr ; 75(3): 427-433, 2020 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-32572675

RESUMO

In this paper, high-hydrostatic pressure extraction (HHPE) as an emerging food processing and preservation technique constitutes an alternative to conventional thermal treatment that has been used for extraction of polyphenols from tomato peel waste generated by the canning industry. The impact of time (5 and 10 min), temperature (25, 35, 45 and 55 °C) and solvents (water, 1% HCl, 50 and 70% methanol with and without addition of HCl, and 50 and 70% ethanol), at a constant pressure of 600 MPa, has been evaluated in this paper with respect to polyphenols' yields. The results showed a significant (p < 0.05) variation in the contents of a great number of phenolic compounds in respect of the applied temperatures and solvents. On the other hand, the time invested in HHPE had no effect on polyphenols' yields. Among phenolic compounds, the p-coumaric acid (p-CA) and chlorogenic acid derivative (ChA der) are predominant, i.e., 0.57 to 67.41 mg/kg and 1.29 to 58.57 mg/kg, respectively, depending on the solvents and temperatures used. In particular, methanol (50 and 70%) at temperatures of 45 and 55 °C enhanced the recovery of polyphenols in comparison to other utilised solvents. In conclusion, this paper puts forth the theory that by applying HHPE with minimal expenditure of time, it is possible to achieve efficient production of polyphenols from low-cost tomato peel waste, generating income both for producers and agri-food industries.


Assuntos
Polifenóis , Solanum lycopersicum , Antioxidantes , Cromatografia Líquida de Alta Pressão , Pressão Hidrostática , Extratos Vegetais , Solventes
3.
Food Chem ; 266: 47-55, 2018 Nov 15.
Artigo em Inglês | MEDLINE | ID: mdl-30381214

RESUMO

Pectin is the methylated ester of polygalacturonic acid and has a wide range of applications. It can be used in food and animal feed as well as in pharmaceutical and cosmetic products. Pectin is traditionally used as a gelling agent in fruit-based products, as a stabilizer in some fruit juices and milk drinks and fruit filling for bakery and confectionary products, but their potential applications differ according to their chemical composition. Therefore, at this stage of development, it is of a great importance to find fast, reliable methods to not only identify and quantify pectin, but also to determine its chemical structure and composition when it is extracted from plant matrices, wastes and by-products. The present review will focus on the analytical tools used to identify and quantify the amount of pectin obtained from plant matrices, wastes and by-products as well as determining its chemical and structural composition.


Assuntos
Técnicas de Química Analítica/métodos , Análise de Alimentos/métodos , Pectinas/análise , Pectinas/isolamento & purificação , Plantas/química , Resíduos/análise , Animais , Sucos de Frutas e Vegetais/análise
4.
Food Chem ; 198: 93-100, 2016 May 01.
Artigo em Inglês | MEDLINE | ID: mdl-26769509

RESUMO

Pectin was extracted from tomato waste using two different extraction methods to assess its potential utilization as an alternative source of commercial pectin production. Tomato waste was treated with ammonium oxalate/oxalic acid by conventional extraction (CE), under reflux and ultrasound assisted extraction (UAE) at 37 kHz and temperatures of 60 °C and 80 °C. The pectin obtained from these methods was analysed and compared in terms of yield, chemical properties and structure. Among examined methods, CE at 60 °C resulted with the highest yield, but UAE during 15 min of sonication produced the pectin of better quality (anhydrouronic acid, methoxy and calcium pectate contents and degree of esterification). NMR and FTIR spectroscopy of isolated pectins revealed predominantly esterified structure, irrespective of extraction conditions. The comparison of the pectin yields obtained after extraction at 80 °C, indicate that similar values were found at times of 24h and 15 min for CE and UAE, respectively. According to obtained results it can be concluded that main advantage of UAE is considerable shortening of extraction procedure with strong emphasis on environmental friendly processing approach. Therefore, these results suggested that UAE could be used as an efficient technique for the extraction of pectin from tomato waste and by-products.


Assuntos
Espectroscopia de Ressonância Magnética/métodos , Pectinas/química , Solanum lycopersicum/química , Sonicação/métodos , Ultrassom/métodos
5.
J Sci Food Agric ; 90(14): 2419-26, 2010 Nov.
Artigo em Inglês | MEDLINE | ID: mdl-20672336

RESUMO

BACKGROUND: In this work the influence of essential onion oil (EOO) on the protection of tinplates was compared with dioctyl sebacate oil (DOS) and epoxy phenolic lacquers, which are frequently used in the food canning industry. RESULTS: When EOO as the protective layer instead of DOS oil was used, tinplate porosity, measured electrochemically (7.58 ± 1.97 µA cm(-2) and 23.0 ± 1.3 µA cm(-2), respectively), and iron coating mass, calculated from AAS data (1.52 ± 0.15 mg m(-2) and 3.14 ± 0.42, respectively), was much lower indicating better corrosion protection. At higher storing temperature (36 °C) the addition of EOO to canned tomato purée enhanced the formation of hydrogen with time. The increasing volume fraction of H(2) (from 34.0 to 90.9% for cans without nitrates, and from 33.8 to 89.2% for cans with nitrates) is an indicator that corrosion takes place. CONCLUSION: As the use of EOO improves the protection of tinplate compared with DOS oil, and is almost as effective as epoxy phenolic lacquer, the addition of EOO can be recommended due to lower cost of canned food production and enhanced organoleptic properties, but the storage temperature has to be lower then 36 °C.


Assuntos
Contaminação de Alimentos/prevenção & controle , Embalagem de Alimentos/métodos , Conservação de Alimentos/métodos , Ferro/química , Óleos Voláteis/química , Cebolas/química , Estanho/química , Corrosão , Compostos de Epóxi , Hidrogênio/química , Óleos Industriais , Laca , Solanum lycopersicum , Nitratos/química , Temperatura
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