A large-area plate radiator with in situ temperature homogenization for thermographic imager calibration.

Large-area plate radiators with a high emissivity and uniform temperature distribution are needed as reference sources for calibrating infrared imagers and camera systems. However, achieving very uniform temperature distribution over a large area is technically challenging, especially at high temperatures. We present a large-area plate radiator with an improved uniformity in its surface temperature distribution for the calibration of infrared thermographic imagers. It is based on an industrial plate radiator which is temperature homogenized in situ by using the Data Reference Method (DRM) developed at the Physikalisch-Technische Bundesanstalt. The DRM takes three spatially shifted pictures of the plate radiator with a thermographic imager, and using this information, it calculates both the nonuniformity in the temperature distribution of the plate radiator and the nonuniformity in the response of the thermographic imager used for imaging the scene. The surface of the applied plate radiator is 300 mm × 300 mm and it operates in a temperature range from 30 °C to 600 °C. The surface is segmented into 9 different parts of identical size whose temperature can be individually controlled. The in situ controlled plate radiator system developed uses an infrared camera, whose detector is corrected for its response inhomogeneity using the DRM. This camera permanently monitors the plate radiator, and from these data, the temperature distribution of the plate is homogenized. Through this method, the homogeneity of the plate radiator can be considerably improved compared to the non-actively regulated mode of operation. For example, at a nominal temperature of 400 °C, without the in situ homogenization procedure, 90% of the plate area has a radiation temperature in the range from 391.7 °C to 403.6 °C. Applying the in situ homogenization procedure leads to 90% of the plate area having a radiation temperature in the range from 394.2 °C to 401.2 °C.

Report on the CCT Supplementary Comparison S1 of Infrared Spectral Normal Emittance/Emissivity.

The National Measurement Institutes (NMIs) of the United States, Germany, France, Italy and Japan, have joined in an inter-laboratory comparison of their infrared spectral emittance scales. This action is part of a series of supplementary inter-laboratory comparisons (including thermal conductivity and thermal diffusivity) sponsored by the Consultative Committee on Thermometry (CCT) Task Group on Thermophysical Quantities (TG-ThQ). The objective of this collaborative work is to strengthen the major operative National Measurement Institutes' infrared spectral emittance scales and consequently the consistency of radiative properties measurements carried out worldwide. The comparison has been performed over a spectral range of 2 µm to 14 µm, and a temperature range from 23 °C to 800 °C. Artefacts included in the comparison are potential standards: oxidized inconel, boron nitride, and silicon carbide. The measurement instrumentation and techniques used for emittance scales are unique for each NMI, including the temperature ranges covered as well as the artefact sizes required. For example, all three common types of spectral instruments are represented: dispersive grating monochromator, Fourier transform and filter-based spectrometers. More than 2000 data points (combinations of material, wavelength and temperature) were compared. Ninety-eight percent (98%) of the data points were in agreement, with differences to weighted mean values less than the expanded uncertainties calculated from the individual NMI uncertainties and uncertainties related to the comparison process.

A highly linear superconducting bolometer for quantitative THz Fourier transform spectroscopy.

A superconducting transition edge sensor (TES) bolometer operating in the spectral range from 0.1 THz to 3 THz was designed. It is especially intended for Fourier transform spectroscopy and features a higher dynamic range and a highly linear response at a similar response compared to commercially available silicon composite bolometers. The design is based on a thin film metal mesh absorber, a superconducting thermistor and Si3N4 membrane technology. A prototype was set up, characterized and successfully used in first applications.

Nonuniformity correction of imaging systems with a spatially nonhomogeneous radiation source.

We present a novel method of nonuniformity correction of imaging systems in a wide optical spectral range by applying a radiation source with an unknown and spatially nonhomogeneous radiance or radiance temperature distribution. The benefit of this method is that it can be applied with radiation sources of arbitrary spatial radiance or radiance temperature distribution and only requires the sufficient temporal stability of this distribution during the measurement process. The method is based on the recording of several (at least three) images of a radiation source and a purposeful row- and line-shift of these sequent images in relation to the first primary image. The mathematical procedure is explained in detail. Its numerical verification with a source of a predefined nonhomogenous radiance distribution and a thermal imager of a predefined nonuniform focal plane array responsivity is presented.

Method for the calibration of the spectral irradiance of tungsten filament transfer standard sources traceable to synchrotron radiation.

The spectral irradiance calibration of tungsten strip and spiral filament lamps applying synchrotron radiation revealed that the spectral irradiance in the wavelength range from 280 to 400 nm can be well approximated by blackbody radiation according to Planck's law. Consequently, the spectral irradiance of the filament lamp can then be described by an effective irradiance temperature, which would be beneficial for practical measurements. Including the emissivity of tungsten into the approximation, the model can be expanded to visible and near-infrared wavelength regions. The effective irradiance temperature dependence of the lamp current was investigated and appeared to be close to linear.

State-of-the art comparability of corrected emission spectra. 1. Spectral correction with physical transfer standards and spectral fluorescence standards by expert laboratories.

The development of fluorescence applications in the life and material sciences has proceeded largely without sufficient concern for the measurement uncertainties related to the characterization of fluorescence instruments. In this first part of a two-part series on the state-of-the-art comparability of corrected emission spectra, four National Metrology Institutes active in high-precision steady-state fluorometry performed a first comparison of fluorescence measurement capabilities by evaluating physical transfer standard (PTS)-based and reference material (RM)-based calibration methods. To identify achievable comparability and sources of error in instrument calibration, the emission spectra of three test dyes in the wavelength region from 300 to 770 nm were corrected and compared using both calibration methods. The results, obtained for typical spectrofluorometric (0°/90° transmitting) and colorimetric (45°/0° front-face) measurement geometries, demonstrated a comparability of corrected emission spectra within a relative standard uncertainty of 4.2% for PTS- and 2.4% for RM-based spectral correction when measurements and calibrations were performed under identical conditions. Moreover, the emission spectra of RMs F001 to F005, certified by BAM, Federal Institute for Materials Research and Testing, were confirmed. These RMs were subsequently used for the assessment of the comparability of RM-based corrected emission spectra of field laboratories using common commercial spectrofluorometers and routine measurement conditions in part 2 of this series (subsequent paper in this issue).

State-of-the art comparability of corrected emission spectra. 2. Field laboratory assessment of calibration performance using spectral fluorescence standards.

In the second part of this two-part series on the state-of-the-art comparability of corrected emission spectra, we have extended this assessment to the broader community of fluorescence spectroscopists by involving 12 field laboratories that were randomly selected on the basis of their fluorescence measuring equipment. These laboratories performed a reference material (RM)-based fluorometer calibration with commercially available spectral fluorescence standards following a standard operating procedure that involved routine measurement conditions and the data evaluation software LINKCORR developed and provided by the Federal Institute for Materials Research and Testing (BAM). This instrument-specific emission correction curve was subsequently used for the determination of the corrected emission spectra of three test dyes, X, QS, and Y, revealing an average accuracy of 6.8% for the corrected emission spectra. This compares well with the relative standard uncertainties of 4.2% for physical standard-based spectral corrections demonstrated in the first part of this study (previous paper in this issue) involving an international group of four expert laboratories. The excellent comparability of the measurements of the field laboratories also demonstrates the effectiveness of RM-based correction procedures.

Optical methods for power measurementof terahertz radiation.

Precision power measurements of terahertz (THz) radiation are required to establish metrological applications in the THz spectral range. However, traceability to the International System of Units (SI) has been missing in the THz region in the past. The Physikalisch-Technische Bundesanstalt (PTB), as the national metrology institute of Germany, determines the spectral responsivity of detectors for THz radiation by using two complementary optical methods: source- and detector-based radiometry. Both approaches have been successfully prototyped, and a pyroelectric THz detector with a well-defined aperture is used to verify the consistency of the two independent calibration methods. These primary investigations led to the design of a new measurement facility for the determination of THz radiant power and the responsivity calibration of THz detectors traceable to the SI.