RESUMO
The work accomplished within the participation at the 2012 key comparison of Tc-99 is presented. The solution was standardized for the first time in IFIN-HH by two methods: LSC-TDCR and 4π(PC)ß-γ efficiency tracer. The methods are described and the results are compared. For the LSC-TDCR method, the program TDCR07c, written and provided by P. Cassette, was used for processing the measurement data. The results are 2.1% higher than when applying the TDCR06b program; the higher value, calculated with the software TDCR07c, was used for reporting the final result in the comparison. The tracer used for the 4π(PC)ß-γ efficiency tracer method was a standard (60)Co solution. The sources were prepared from the mixture (60)Co+(99)Tc solution and a general extrapolation curve, type: N(ßTc-99)/(M)(Tc-99)=f [1-ε(Co-60)], was drawn. This value was not used for the final result of the comparison. The difference between the values of activity concentration obtained by the two methods was within the limit of the combined standard uncertainty of the difference of these two results.
RESUMO
This paper presents the work performed at IFIN-HH and at the users' sites, aimed to establish the (18)FDG Romanian PET traceability chain. It summarizes the operations: (i) Absolute standardization of a (18)F solution, by the 4πß(PC)-γ coincidence method; (ii) Control of gamma-ray impurity content and measurement of the activity by gamma ray spectrometry; (iii) Measurement of the half life, for detection of some short/long life positron emitter impurities; (iv) Calibration of the CENTRONIC IG12/20A ionization chamber; (v) Calibration of commercial radionuclide calibrators.
