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1.
IET Nanobiotechnol ; 6(3): 110-4, 2012 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-22894535

RESUMO

The development of green experimental processes for the synthesis of nanoparticles is a need in the field of nanotechnology. In the present study, the authors reported rapid synthesis of silver nanoparticles using fresh leaves extract of Cymbopogan citratus (lemongrass) with increased stability. The synthesised silver nanoparticles were found to be stable for several months. UV-visible spectrophotometric analysis was carried out to assess the synthesis of silver nanoparticles. The synthesised silver nanoparticles were further characterised by using nanoparticle tracking analyser (NTA), transmission electron microscope (TEM) and energy-dispersive x-ray spectra (EDX). The NTA results showed that the mean size was found to be 32 nm. Silver nanoparticles with controlled size and shape were observed under TEM micrograph. The EDX of the nanoparticles confirmed the presence of elemental silver. These silver nanoparticles showed enhanced quorum quenching activity against Staphylococcus aureus biofilm and prevention of biofilm formation which can be seen under inverted microscope (40X). In the near future, silver nanoparticles synthesised using green methods may be used in the treatment of infections caused by a highly antibiotic resistant biofilm.


Assuntos
Biofilmes/efeitos dos fármacos , Nanopartículas Metálicas/química , Percepção de Quorum/efeitos dos fármacos , Prata/farmacologia , Staphylococcus aureus/efeitos dos fármacos , Staphylococcus aureus/fisiologia , Antibacterianos/química , Antibacterianos/farmacologia , Microscopia Eletrônica de Transmissão , Prata/química , Espectrofotometria Ultravioleta
2.
J Hazard Mater ; 154(1-3): 88-95, 2008 Jun 15.
Artigo em Inglês | MEDLINE | ID: mdl-18006151

RESUMO

The present study was carried out to investigate the potential of cement hydrated at various time intervals for the removal of excess F- from aqueous solution by using batch adsorption studies. The influence of different adsorption parameters, viz. effect of adsorbent dose, initial concentration, pH, interfering ions and contact time were studied for their optimization. It was observed that the adsorbent exhibited reasonably significant F- removal over a wide range of pH. The presence of carbonate and bicarbonate ions in aqueous solution were found to affect the F- removal indicating that these anions compete with the sorption of F- on adsorbent. The equilibrium adsorption data were fitted well for both the Freundlich and Langmuir isotherms and the adsorption capacities were calculated. Comparative studies for F- removal in simulated and field water show relatively higher F- removal in simulated water. XRD and SEM patterns of the hydrated cement were recorded to get better insight into the mechanism of adsorption process. From the experimental results, it may be concluded that HC was an efficient and economical adsorbent for F- removal.


Assuntos
Materiais de Construção , Fluoretos/química , Poluentes Químicos da Água/química , Purificação da Água/métodos , Adsorção , Concentração de Íons de Hidrogênio , Cinética , Abastecimento de Água
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