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1.
Forensic Sci Res ; 7(4): 748-760, 2022.
Artigo em Inglês | MEDLINE | ID: mdl-36817242

RESUMO

The aim of this study was threefold. First, it analyzed the characteristics of the publication outputs for the Legal Medicine (LM) category using the Web of Science (WoS) database during 2011-2020. Second, it discussed the distribution of the papers for the 25 most productive countries/regions in terms of quality and quantity, such as the h-index and GDP per capita. Finally, it investigated the trend and temporal stability of the journal impact factor (JIF) and determined the percentage of the journal self-citations. The findings suggested that the number of papers, the average number of pages of the papers, the average number of cited references in the papers, the average number of authors per paper, the percentage of open access papers, as well as international and domestic collaboration tended to increase regularly. However, the productivity was limited when compared to the whole WoS database, since there was no significant change in the number of the journals. The countries/regions with the highest number of publications were not those that made the most impact in terms of the widespread impact of the publications. The level of international cooperation and the funding for the research had dramatic impact on the visibility of papers. The average JIF has increased significantly while the journal self-citation rates have decreased in a similar way. The journals have had very stable (have not fluctuated) impact factors over time. During the period studied, the journals with the higher impact factors (Q1, Q2) published many more papers than journals with the lower impact factors (Q3, Q4).

2.
ACS Nano ; 16(1): 111-118, 2022 Jan 25.
Artigo em Inglês | MEDLINE | ID: mdl-34787390

RESUMO

MXenes are two-dimensional metal carbides or nitrides that are currently proposed in many applications thanks to their unique attributes including high conductivity and accessible surface. Recently, a synthetic route was proposed to prepare MXenes from the molten salt etching of precursors allowing for the preparation of MXene (denoted as MS-MXenes, for molten salt MXene) with tuned surface termination groups, resulting in improved electrochemical properties. However, further delamination of as-prepared multilayer MS-MXenes still remains a major challenge. Here, we report on the successful exfoliation of MS-Ti3C2Tx via the intercalation of the organic molecule TBAOH (tetrabutylammonium hydroxide), followed by sonication to separate the layers. The treatment time could be adapted to tune the wetting behavior of the MS-Ti3C2Tx. As a result, a self-supported Cl-terminated MXene film could be prepared by filtration. Finally, MS-Ti3C2Tx used as a Li-ion battery anode could achieve a high specific capacity of 225 mAh g-1 at a 1C rate together with an excellent rate capability of 95 mAh g-1 at 167C. These results also show that tuning of the surface chemistry of MXene is of key importance to this field with the likely result being increased electrochemical performance.

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