Effect of Bonding Agent on Metal-Ceramic Bond Strength between Co-Cr Fabricated with Selective Laser Melting and Dental Feldspathic Porcelain.

PURPOSE: To investigate the effect of bonding agent on the bonding strength between Co-Cr dental alloy, prepared by selective laser melting (SLM), and feldspathic porcelain. MATERIALS AND METHODS: The experiments were conducted according to ISO 9693 and the conventional protocols for the production of metal-ceramic dental restorations. After Al2 O3 air-particle abrasion, metal substrates of Co-Cr dental alloy specimens were bonded, using bonding agent (25 specimens), with dental porcelain positioned in layers (opaque, dentin, enamel). Control specimens (25) were also produced without bonding agent. Bonding strength was measured using 3-point bending tests, and the results were statistically analyzed using the t-test and Weibull statistics. Elemental (by SEM/EDS) and crystallographic analyses (by XRD) were conducted on the bonding agent, along cross sections of alloy-porcelain interfaces, and on fracture surfaces. RESULTS: Cohesive fracture occurred (on the porcelain side). The application of the bonding agent decreased the average bonding strength (from 42.27 ± 5.85 to 36.25 ± 3.26 MPa, P = 0.00006), attributed to the nonexisting reaction between the TiO2 -rich bonding agent and the Co-Cr alloy, but it increased the Weibull modulus (from 7.84 to 12.16), which reflects the reliability of the bond in the tested metal-ceramic specimens. CONCLUSIONS: Although the application of bonding agent slightly decreased the bonding strength, all the measured values of the metal-ceramic specimens produced by the SLM technique, with or without the bonding agent, are markedly higher than the minimum value required by ISO 9693 (25 MPa). Moreover, the use of bonding agent favors the increase of the Weibull modulus.

Metal-ceramic bond strength between a feldspathic porcelain and a Co-Cr alloy fabricated with Direct Metal Laser Sintering technique.

PURPOSE: The aim of the present study was to record the metal-ceramic bond strength of a feldspathic dental porcelain and a Co-Cr alloy, using the Direct Metal Laser Sintering technique (DMLS) for the fabrication of metal substrates. MATERIALS AND METHODS: Ten metal substrates were fabricated with powder of a dental Co-Cr alloy using DMLS technique (test group) in dimensions according to ISO 9693. Another ten substrates were fabricated with a casing dental Co-Cr alloy using classic casting technique (control group) for comparison. Another three substrates were fabricated using each technique to record the Modulus of Elasticity (E) of the used alloys. All substrates were examined to record external and internal porosity. Feldspathic porcelain was applied on the substrates. Specimens were tested using the three-point bending test. The failure mode was determined using optical and scanning electron microscopy. The statistical analysis was performed using t-test. RESULTS: Substrates prepared using DMLS technique did not show internal porosity as compared to those produced using the casting technique. The E of control and test group was 222 ± 5.13 GPa and 227 ± 3 GPa, respectively. The bond strength was 51.87 ± 7.50 MPa for test group and 54.60 ± 6.20 MPa for control group. No statistically significant differences between the two groups were recorded. The mode of failure was mainly cohesive for all specimens. CONCLUSION: Specimens produced by the DMLS technique cover the lowest acceptable metal-ceramic bond strength of 25 MPa specified in ISO 9693 and present satisfactory bond strength for clinical use.

The Influence of Thermocycling on the Flexural Strength of a Polyamide Denture Base Material.

OBJECTIVE: The aim of the present study was to evaluate the influence of thermocycling on the flexural strength of a polyamide base denture material. MATERIALS AND METHODS: A polyamide denture base material (Valplast) was tested, whereas a PMMA material (Vertex) was used as a control. Thirty specimens of each material were fabricated for flexural strength testing according to ISO 1567. They were prepared and stored in water at 37°C for 48 hours. The specimens of each material were divided into three equal groups (n=10). Flexural strength testing was performed immediately after water storage and after thermocycling (5°C / 55°C, 2 c/min) for 3000 and 5000 cycles. A three point flexural test was performed on a universal testing machine at a crosshead speed of 5 mm/min. The final flexural strength was calculated using the formula: FS = 3 PL/2 bd2. A two-way ANOVA with post-hoc analysis using Tukey's procedure was applied at .05 level of statistical significance. RESULTS: A statistically significant reduction in flexural strength was recorded after thermocycling at 3000 cycles for PMMA and at 5000 cycles for both materials. The flexural strength of PMMA was significantly higher compared to polyamide for all the conditions tested (p<0.05). CONCLUSION: Thermocycling had a significant adverse effect on the flexural strength of polyamide and PMMA denture base materials.

Color and structural changes of a maxillofacial elastomer: the effects of accelerated photoaging, disinfection and type of pigments.

PURPOSE: The aim of this study was to investigate the color and structural changes of a maxillofacial silicone colored with 2 different pigments, after photoaging and immersion in disinfectants. METHODS: Ninety-six cylindrical specimens were fabricated and divided into 3 equal groups. The specimens of the first group consisted of unpigmented silicone (Multisil Epithetik), those of the second group consisted of unpigmented silicone, colored with red functional liquid pigment (Cosmesil Reactive 0.2% wt). The specimens of the third group were fabricated using unpigmented silicone colored with red powder pigment Cosmesil Dry at 0.2% wt. Specimens of each group were divided into 4 equal subgroups (immersed in soap solution, ethanol 95° or distilled water or placed in a photoaging apparatus for 174 hours). Structural changes were examined by infrared spectroscopy (ATR-FTIR) before and after aging. Color changes (ΔΕ*) were measured using the CIE L*a*b* system. Two-way ANOVA and Tukey's test for post hoc comparison were used at a = 0.05. RESULTS: Infrared spectroscopy showed no structural changes after immersion in solutions and photoaging, for all the materials tested. No statistically significant differences for ΔΕ* among the tested groups were found. CONCLUSIONS: It can be concluded that no structural changes of pigmented and unpigmented silicone elastomers were observed among all aging procedures. Recorded color changes for the materials tested were within the limits of clinical acceptability after all aging procedures. Immersion in distilled water presented the best color stability, whereas photoaging, the poorest, for all materials.

Effect of light aging on silicone-resin bond strength in maxillofacial prostheses.

PURPOSE: The aim of this study was to investigate the effect of accelerated light aging on bond strength of a silicone elastomer to three types of denture resin. MATERIALS AND METHODS: A total of 60 single lap joint specimens were fabricated with auto-, heat-, and photopolymerized (n = 20) resins. An addition-type silicone elastomer (Episil-E) was bonded to resins treated with the same primer (A330-G). Thirty specimens served as controls and were tested after 24 hours, and the remaining were aged under accelerated exposure to daylight for 546 hours (irradiance 765 W/m(2) ). Lap shear joint tests were performed to evaluate bond strength at 50 mm/min crosshead speed. Two-way ANOVA and Tukey's test were carried out to detect statistical significance (p < 0.05). RESULTS: ANOVA showed that the main effect of light aging was the most important factor determining the shear bond strength. The mean bond strength values ranged from 0.096 to 0.136 MPa. The highest values were recorded for auto- (0.131 MPa) and photopolymerized (0.136 MPa) resins after aging. CONCLUSIONS: Accelerated light aging for 546 hours affects the bond strength of an addition-type silicone elastomer to three different denture resins. The bond strength significantly increased after aging for photo- and autopolymerized resins. All the bonds failed adhesively.

Effects of cleansing methods on 3-D surface roughness, gloss and color of a polyamide denture base material.

OBJECTIVE: The purpose of this study was to determine the effects of two denture cleansing methods on 3-D surface roughness, gloss and color of denture base materials. MATERIALS AND METHODS: Thirty disks from nylon (Valplast) and 30 from heat-polymerized acrylic denture base material (Paladon 65) were made and 10 of each material were immersed in water (control), Val-Clean (peroxide cleanser) and Corega Extradent (peroxide cleanser) plus microwaving for a period simulating 30 days of daily cleansing. 3-D surface roughness, gloss and color parameters were measured before and after cleansing using an interferometric profilometer, a gloss meter and a colorimeter. The results were statistically analysed by regression, paired-t, Mann-Whitney and Kruskal-Wallis tests at α = 0.05 level of significance. RESULTS: The results showed significant differences at baseline in L* and b* parameters between materials (p < 0.01), with a significantly lower gloss (p < 0.05) and higher roughness (p < 0.05) for Valplast. After cleansing, Δϵ* was significantly greater in Valplast than Paladon 65 (p < 0.05). Gloss of both materials decreased significantly within the Corega Extradent plus microwave solution (p < 0.05), while roughness increased significantly only for Paladon 65 (p < 0.05). CONCLUSIONS: Valplast was found to have a significantly lower gloss and a higher roughness than Paladon 65 before cleansing. After cleansing, ΔE* increased more in Valplast than in Paladon 65, gloss of both materials decreased and roughness only of Paladon 65 increased within the Corega extradent plus microwaving method.

Color changes in staining solutions of four light-cured indirect resin composites.

The purpose of this study was to investigate the effect of different staining solutions on the color coordinates of indirect light-cured resin composites. 112 discs were made using four indirect composites, Signum+/Haraeus-Kulzer, Sinfony/3M-Espe, GC Gradia/GC, Ena HRi/Micerium, and divided into four groups which immersed in tea, coffee, chocolate and distilled water, at 37 °C, for 4 weeks. The color, before and after immersion for 1, 2, 3 and 4 weeks, was measured according to CIELAB system and ΔL*, Δa*, Δb* and ΔE* values were calculated for all immersion periods. The effect of time, solution and material on primary and secondary color coordinates was estimated using two-way repeated ANOVAs and pairwise comparisons, at a = 0.05. The results showed that coffee strongly affected all the materials (p < 0.05), followed by tea and chocolate. Sinfony presented the highest color change (p < 0.05), due to changes in b* and L* coordinates. Color coordinates were affected differently by material type and solution. In conclusion, this study showed that the color of indirect resin composites was affected by all three examined factors (immersion time, staining solution and material type), in a clinically appreciable level (ΔΕ* > 2.7 U) even from the first week, and in an unacceptable level (ΔΕ* > 5.5 U) in the second, third and fourth week, depending on the staining solution and the material.

In vitro evaluation of shear bond strength and mode of failure of the interface between an indirect composite bonded to fiber-reinforced composite substructures.

PURPOSE: Failures of fixed partial dentures (FPDs) fabricated with fiber-reinforced composites (FRCs) have been attributed to veneering fractures. The aim of the present study was to investigate the shear bond strength and mode of failure between an indirect composite and FRC substructures. MATERIAL AND METHODS: SR Adoro indirect composite was bonded to the following substructures: (a) flat surface made of unidirectional glass fibers (group A), (b) retentive sticks made of unidirectional glass fibers (group B), (c) flat surface made of fiber net (group C), (d) retentive sticks made of fiber net (group D), (e) nickel-chromium dental alloy (control, group E). For every group, 13 specimens were fabricated. All specimens were hydrothermocycled (5000 cycles, 5°C/30 sec, and 55°C/30 sec). A bond test was performed in a testing machine at a 0.5 mm/min crosshead speed according to ISO 10477. The failure mode was determined by examination of the fractured surfaces under an optical microscope. Selected specimens were examined with scanning electron microscope and with energy dispersive spectroscopy for compositional determination. The morphology (flat-sticks) and the type (unidirectional-net) of fibers on the bond strength were estimated. RESULTS: The mean shear bond strength was significantly different between groups E and A (p= 0.044), and groups A and B (p= 0.010). All FRC specimens showed cohesive failure. Group E showed predominantly adhesive failure. The bond strength was higher when sticks or fiber nets were used. CONCLUSIONS: Fiber nets and retentive sticks increase the shear bond strength between FRCs and indirect composite. CLINICAL IMPLICATIONS: In FPDs, the morphology and type of FRC substructures might influence the shear bond strength between the FRC substructure and the indirect veneering composite. With the proper design of these substructures, the number of veneering fractures may be decreased.

Laboratory evaluation of modern plastic brackets.

The aim of the study was to evaluate some properties of modern orthodontic plastic brackets. Seven bracket brands [Aesthetik-Line (AL), Avalon (AV), Brillant (BR), Elegance (EL), OrthoFlex (OF), Silkon Plus (SL), and Spirit MB (SP)] were included in the study. The properties tested were chemical composition, base morphology, slot roughness, Vickers hardness (VH), and shear bond strength (SBS) with enamel.According to the results, the brackets were composed of polyurethane (AV and OF), polyoxymethylene (BR), and Ca-Al-silicate fibre glass-reinforced polycarbonate (AL, EL, SL, and SP). Metallic slots were composed of austenitic stainless steel (EL and SP) and Ag-Cu alloy (AV). The base morphology exhibited distinct designs, employing parallel retentive canals (AV, EL, and OF) or round-angled square protrusions with major retentive elements (AL, BR, and SP) or a combination of both (SL). The SP metallic slot demonstrated the lowest Sz values. No significant differences were found in VH among the brackets before water immersion (19.6-16.9 VH). After 12 weeks immersion, the brackets showed a significant hardness reduction (16.6-12.9 HV). SBS ranged between 111 and 193 N (8-14 MPa) for all brackets, except from SP (59 N/5 MPa). The predominant failure mode was mixed adhesive and cohesive. Most of the plastic brackets presented a base structure capable of adequate bonding to enamel, regardless of their differences in composition. Slot roughness showed differences among groups. All the brackets demonstrated plasticization after prolonged water storage.

The influence of alendronate on osseointegration of nanotreated dental implants in New Zealand rabbits.

OBJECTIVES: Growing clinical demands for stronger and faster bone bonding to the implant have motivated the development of methods enhancing osseointegration. Lately, the application of bisphosphonates (bis) in order to optimize bone healing has become a topic of great interest. N-containing bis, such as alendronate (ALN), are the more potent drugs of this class. It was the aim of this study to determine the effect of ALN on the osseointegration of a well-documented nanotreated implant system in a rabbit femoral condyle model. MATERIAL AND METHODS: Thirty-two adult female New Zealand White rabbits received one implant (3.25 mm in diameter and 10 mm in length) in their left femoral condyle, a week after they were ovariectomized. Half of them were saline treated (control, group A) and the other half were ALN treated (group B). Rabbits from both groups were euthanized after 6 and 12 weeks, respectively. RESULTS: The specimens were evaluated histologically and histomorphometrically. Upon histological evaluation, no obvious differences were found between the control and the treatment group. Implants showed good integration into the bone tissue surrounding them. There were also no statistically significant differences in bone-to-implant contact and the amount of bone tissue in the immediate neighborhood of the implant at both healing periods. CONCLUSIONS: The systemic administration of ALN was not found to affect histological osseointegration of implants in animals with a hormonal status resembling that of postmenopausal healthy women. Further research will be needed to investigate this approach.

The effect of disinfecting solutions on bending properties and weight changes of Co-Cr and Ti-6Al-7Nb alloys for dentures.

We aimed to evaluate the effect of a denture cleanser and NaOCl 5.25% solution on the modulus of elasticity, the ultimate stress, and the weight changes of Co-Cr and Ti-6Al-7Nb alloys. To evaluate the modulus of elasticity and ultimate stress, 24 Co-Cr and 24 Ti-6Al-7Nb castings were fabricated, immersed in Corega Extradent, NaOCl 5.25%, or water in subgroups of six each. Thirty-six castings were produced to evaluate weight changes, 18 Co-Cr and 18 Ti-6Al-7Nb, and immersed in Corega Extradent, NaOCl 5.25%, or water in subgroups of six each. Changes in the modulus of elasticity, ultimate stress, and weight were calculated before and after immersion in the cleanser or NaOCl 5.25% solution for 45 cycles of 10 min each. Two-way analysis of variance ANOVA and Tukey's test at α = 0.05 were used to analyze the data. The modulus of elasticity and the ultimate stress of Co-Cr decreased after immersion in the solutions. The same properties of Ti-6Al-7Nb decreased in NaOCl 5.25% and increased in the other solutions. Weight loss was observed in Co-Cr alloy in both Corega Extradent and NaOCl 5.25%. A weight increase was observed in Co-Cr in water. An increase was observed in Ti-6Al-7Nb in Corega Extradent, NaOCl 5.25%, and water. The highest decrease (P = 0.05) in the modulus of elasticity and ultimate stress in Co-Cr were observed in NaOCl 5.25%, whereas no statistically significant differences (P > 0.05) were observed in Ti-6Al-7Nb in any of the solutions. A statistically significant weight loss (P < 0.05) was observed when Co-Cr was immersed in NaOCl 5.25%, and a statistically significant weight increase (P > 0.05) was observed when Ti-6Al-7Nb was immersed in Corega Extradent. The Co-Cr alloy bending properties after immersion fulfilled ADA Specification No. 14 for satisfactory clinical performance.

Dynamic mechanical properties of a maxillofacial silicone elastomer incorporating a ZnO additive: the effect of artificial aging.

The main objective of the current study was to investigate the dynamic mechanical properties of a room-temperature vulcanizing silicone incorporating different fractions of zinc oxide (ZnO) after indoor and outdoor photoaging. Forty-eight samples were produced by adding different amounts of ZnO into a commercial maxillofacial silicone (EPISIL-E). The samples were divided into 4 groups containing 0.0, 0.2, 0.5, and 1 wt% ZnO additive, respectively. Samples were exposed to sunlight (subgroup 2), ultraviolet (subgroup 3), and fluorescence (subgroup 4) aging, whereas nonaged samples comprised the control subgroup (subgroup 1). Dynamic mechanical analysis was used to determine the storage modulus (E'), loss modulus (E″), and damping capacity (tanδ). General linear statistic model was conducted to evaluate the effects of aging, testing frequency, and composition on the dynamic mechanical properties of the silicone with the ZnO additive. Post hoc analysis was performed using Tukey test. Statistical analysis revealed a significant impact of composition on tanδ (P < 0.05). Aging influenced E' and E″ (P < 0.01). The combination of aging and composition had a significant effect on all dynamic properties (P < 0.01).

Experimental and numerical determination of the mechanical response of teeth with reinforced posts.

The aim of this study was to evaluate the mechanical behavior of endodontically treated teeth restored with fiber reinforced composite posts versus titanium posts, by both experimental testing and numerical simulation (finite element analysis (FEA)). Forty maxillary central incisors were endodontically treated to a size 45 file and then obturated using gutta-percha points and sealer with the lateral condensation technique. The teeth were divided into four groups of ten teeth each. All the posts were of similar dimensions. The first group was restored using carbon fiber reinforced posts (CB), the second and third groups were restored using glass fiber reinforced posts (DP and FW, respectively), and the fourth group (control group) was restored using conventional titanium posts (PP). Half of the specimens of every group were submitted to hydrothermal cycling (2000 cycles, at 5 °C and 55 °C, respectively). All specimens were loaded until failure at a 45° angle with respect to the longitudinal axis at a cross head speed of 0.5 mm min(-1). A two-dimensional finite element model was designed in order to simulate the experimentally obtained results. Mechanical testing revealed that teeth restored with titanium posts exhibited the highest fracture strength. Debonding of the core was the main failure mode observed in glass fiber posts, whereas vertical root fractures were observed in the titanium posts. FEA revealed that the maximum stresses were developed at the interface between the post, dentin and the composite core critical regions in all three cases. Hydrothermal cycling had no significant effect on the fracture behavior of fiber reinforced composite posts.

Colour stability of veneering composites after accelerated aging.

OBJECTIVES: To investigate the colour stability of four indirect composite restorative materials after accelerated aging. METHODS: Four indirect composites (Gradia, Signum+, HFO and Adoro) were used. For each material, six specimens were prepared and subjected to accelerated aging (Suntest CPS+, Atlas, Chicago, IL, USA) according to ISO 7491. A Dr. Lange Microcolor Data Station colorimeter (Braive Instruments, Liege, Belgium) was used to measure specimen colour before and after aging. Measurements were performed according to the CIE L*a*b* system, and the mean L*, a* and b* values for each material were calculated. The equation DeltaE = [(DeltaL*)2 + (Deltaa*)2 + (Deltab*)2](1/2) was used to measure the total colour change (DeltaE), where DeltaL*, Deltaa* and Deltab* are the differences in the respective values before and after aging. One-way ANOVA were used to determine statistically significant differences in DeltaL*, Deltaa*, Deltab* and DeltaE. RESULTS: No statistically significant differences were found in DeltaL*, Deltaa*, Deltab* and DeltaE among the materials tested (PDeltaL*=.063; PDeltaa*=.521; PDeltab*=.984 and PDeltaE=.408). After aging, Gradia specimens showed an increase in lightness (DeltaL*=0.36) and a green-yellow shift (Deltaa*=-1.18, Deltab*=0.6), while Signum+ specimens exhibited an increase in lightness (DeltaL*=0.5) and a green-blue shift (Deltaa*=-0.9, Deltab*=-0.45). HFO specimens exhibited an increase in lightness (DeltaL*=0.75) and a green-yellow shift (Deltaa*=-1.3, Deltab*=0.06), and Adoro specimens exhibited an increase in lightness (DeltaL*=2.07) and a green-yellow shift (Deltaa*=-1.3, Deltab*=0.68). CONCLUSIONS: Colour changes were found to be within accepted values of perceptibility and clinical acceptance after accelerated aging, and no statistically significant differences were found in DeltaL*, Deltaa*, Deltab* and DeltaE among the materials tested.

Molecular toxicology of substances released from resin-based dental restorative materials.

Resin-based dental restorative materials are extensively used today in dentistry. However, significant concerns still remain regarding their biocompatibility. For this reason, significant scientific effort has been focused on the determination of the molecular toxicology of substances released by these biomaterials, using several tools for risk assessment, including exposure assessment, hazard identification and dose-response analysis. These studies have shown that substances released by these materials can cause significant cytotoxic and genotoxic effects, leading to irreversible disturbance of basic cellular functions. The aim of this article is to review current knowledge related to dental composites' molecular toxicology and to give implications for possible improvements concerning their biocompatibility.

The effect of a ceramic coating on the cpTi-porcelain bond strength.

OBJECTIVES: To investigate the bond strength between cpTi and low fusing porcelains after different treatments. METHODS: 72 patterns were covered with a ceramic coating and invested with phosphate-bonded material (group A), another 72 were invested with magnesia material (group B) and all cast with cpTi. 31 solid castings were selected from each group. The castings of group B were ground and sandblasted, while the castings of group A were only sandblasted. Aluminum content of the metal surface was determined by EDS and castings were submitted to a 3-point bending test to determine the modulus of elasticity (E). The porcelains Duceratin Plus, Noritake Ti22 and Triceram were applied respectively and specimens were submitted to a 3-point bending test. The fracture mode and the remaining porcelain were determined by optical microscopy and SEM/EDS. Bond strength and fracture mode were calculated by two-way ANOVA. RESULTS: The E of groups A and B was 98.3 GPa and 98.6 GPa respectively. The bond strength was 26+/-3 MPa (Duceratin Plus), 28+/-3 MPa (Noritake Ti22), 27+/-2 MPa (Triceram) for group A and 24+/-1 MPa, 29+/-2 MPa, 27+/-1 MPa for group B respectively. No significant differences were found for the same porcelain between the two groups (p<0.05). A significant difference was found between Duceratin Plus and Noritake Ti22, for group B (p<0.05). The mode of failure was mainly adhesive for all specimens. A significant reduction in aluminum was recorded in all subgroups. SIGNIFICANCE: The special coating of patterns makes the Ti casting procedure inexpensive, without reducing the metal-ceramic bond strength.

Effectiveness of different adhesive primers on the bond strength between an indirect composite resin and a base metal alloy.

STATEMENT OF PROBLEM: There is a need for achieving reliable chemical bond strength between veneering composites resins and casting alloys through the use of simplified procedures. PURPOSE: The purpose of this study was to examine the shear bond strength of an indirect composite resin to a Ni-Cr alloy, using 4 primers and 2 airborne-particle-abrasion procedures. MATERIAL AND METHODS: Fifty-six Ni-Cr (Heraenium NA) discs, 10 mm in diameter and 1.5 mm in height, were fabricated. Twenty-four discs were airborne-particle abraded with 50-microm Al2O3 particles, while another 24 were airborne-particle abraded with 250-microm Al2O3 particles. The following primers were applied on 6 discs of each airborne-particle-abrasion treatment group: Solidex Metal Photo Primer (MPP50, MPP250), Metal Primer II (MPII50, MPII250), SR Link (SRL50, SRL250), and Tender Bond (TB50, TB250). The Rocatec system was used on another 6 discs, airborne-particle abraded according to the manufacturer's recommendations, which served as the control group (R). Two more discs were airborne-particle abraded with 50-microm and 250-microm Al2O3 particles, respectively, to determine the Al content on their surfaces, without any bonding procedure. The indirect composite resin used was Sinfony. Specimens were thermally cycled (5 degrees C and 55 degrees C, 30-second dwell time, 5000 cycles) and tested in shear mode in a universal testing machine. The failure mode was determined with an optical microscope, and selected specimens were subjected to energy dispersive spectroscopy (EDS). Mean bond strength values were analyzed using 2-way ANOVA followed by Tukey's multiple comparison tests (alpha=.05) and compared to the control group using 1-way ANOVA followed by Tukey's multiple comparison tests (alpha=.05). RESULTS: The groups abraded with 50-microm particles exhibited significantly higher bond strength compared to the groups abraded with 250-microm particles. Group MPII50 exhibited the highest mean value (17.4 +/-2 MPa). Groups MPP50, MPP250, and TB50, TB250 showed adhesive failures and significantly lower bond strength compared to group R. Groups MPII50, MPII250, and SRL50, SRL250 showed combination failures and no significant difference compared with group R. EDS revealed interfacial rather than adhesive failures. CONCLUSIONS: Airborne-particle abrasion with 50-microm Al2O3 particles may result in improved bond strength, independent of the primer used. The bond strength of Metal Primer II and SR Link specimens was comparable to that of specimens treated with Rocatec.

Shear bond strength of a light-cured veneering composite to fiber-reinforced composite substrates.

PURPOSE: The aim of this study was to compare the shear bond strength of a veneering composite to 2 differently treated fiber-reinforced composite (FRC) substrates and to a base metal alloy. MATERIALS AND METHODS: A veneering composite (SR Adoro) was bonded to the following substrates: (1) a nickel-chromium base metal alloy (control, group A), (2) an FRC substructure (Vectris) with a flat surface (group B), and (3) an FRC substructure (Vectris) with retentive rods 0.5 x 0.5 mm in cross section and 10 mm in length, positioned parallel to each other at a distance of 0.5 mm (group C). Thirty-nine specimens were fabricated and divided into 3 groups of equal size. All specimens were thermocycled for 5,000 cycles at 5 degrees C and 55 degrees C with dwell time of 30 seconds in each bath. Evaluation of shear bond strength was performed at a constant crosshead speed of 0.5 mm/min according to ISO 10477. RESULTS: The mean values for the shear bond strength were 19.29 MPa for the control group (group A), 16.66 MPa for group B, and 16.74 MPa for group C. Despite a tendency to higher bond strength of group A specimens, no statistically significant difference was recorded between the groups (P > .05). CONCLUSIONS: No statistically significant difference was found between the metal and FRC substructures. Retentive rods on the FRO substructure do not seem to increase the bond strength significantly.

Surface characterization of three titanium dental implants.

PURPOSE: The aim of this study was to evaluate topographically and compositionally the rough surface of 3 different commercial titanium dental implants. MATERIALS: Bio Com Standard, Osseotite Implant, and Fixture MT Osseospeed were analyzed using scanning electron microscopy, atomic force microscopy, and energy dispersive spectroscopy. RESULTS: The scanning electron microscopy and atomic force microscopy analyses showed that the rough surface of Bio Com Standard presents numerous impressions superimposed by sharp pits, of Osseotite Implant many discrete sharp pits, and of Fixture MT Osseospeed a mixed feature appearance. The energy dispersive spectroscopy analysis of the rough implant surfaces revealed a small trace of Si found on the surface of Osseotite Implant. Fixture MT Osseospeed showed a nonhomogeneous distribution of the detected elements. CONCLUSION: The examined implants had a different rough surface topography, which was directly dependent on the type of treatment used. The differences concerning the surface morphology were leading in a characteristic nanotopography, which might influence the biologic activities at the implant-tissue interface. Surface oxygen concentrations also indicated differences in the oxide layer width between the examined implants, being minimal in Osseotite Implant and maximal in Fixture MT Osseospeed.

Color stability and degree of cure of direct composite restoratives after accelerated aging.

PURPOSE: This study evaluated the color changes and amount of remaining C = C bonds (%RDB) in three dental composites after hydrothermal- and photoaging. METHODS AND MATERIALS: The materials tested were Estelite sigma, Filtek Supreme and Tetric Ceram. Specimens were fabricated from each material and subjected to L* a* b* colorimetry and FTIR spectroscopy before and after aging. Statistical evaluation of the deltaL,* deltaa,* deltab,* deltaE and %deltaRDB data was performed by one-way ANOVA and Tukey's test. The %RDB data before and after aging were statistically analyzed using two-way ANOVA and Student-Newman-Keuls test. In all cases an alpha = 0.05 significance level was used. RESULTS: No statistically significant differences were found in deltaL*, deltaa*, deltaE and %deltaRDB among the materials tested. Tetric Ceram demonstrated a significant difference in deltab*. All the materials showed visually perceptible (deltaE >1) but clinically acceptable values (deltaE < 3.3). Within each material group, statistically significant differences in %RDB were noticed before and after aging (p < 0.05). Filtek Supreme presented the lowest %RDB before aging, with Tetric Ceram presenting the lowest %RDB after aging (p < 0.05). The %deltaRDB mean values were statistically significantly different among all the groups tested. No correlation was found between deltaE and %deltaRDB.