Effect of ionizing radiation and cariogenic biofilm challenge on root-dentin caries.

OBJECTIVES: To evaluate the effect of ionizing radiation and cariogenic biofilm challenge using two continuous flow models, normal and reduced salivary flow, on the development of initial root-dentin caries lesions. MATERIALS AND METHODS: Microcosm biofilms were grown under two salivary flow rates (0.06 and 0.03 mL min-1) and exposed to 5% sucrose (3 × daily, 0.25 mL min-1, 6 min) dripped over non-irradiated and irradiated root-dentin blocks for up to 7 days. The vibration modes of root dentin, matrix/mineral (M/M), and carbonate/mineral (C/M) ratios were evaluated by FTIR. The mineral density was assessed by micro-CT. RESULTS: With normal salivary flow, FTIR revealed an increase in the organic matrix (amide III) and a decrease in the mineral phase (ν4, ν2 PO43-, AII + ν2 CO32-, C/M) in caries lesions. Irradiated dentin exhibited a reduction in the mineral phase (ν1, ν3 PO43-, ν2 CO32-, C/M). Differences in mineral densities were not significant. With reduced salivary flow, FTIR also revealed increased organic matrix (amide III) for irradiated caries lesions and decrease in mineral phase (v4, v2 PO43-, v2 CO32-, and C/M) in caries lesions. ν1, ν3 PO43- precipitated on the surface of irradiated dentin and a lower mineral density was observed. CONCLUSIONS: Initial caries lesions differed between non-irradiated and irradiated dentin and between normal and reduced salivary flow rates. Significant mineral loss with exposure of the organic matrix and low mineral density were observed for irradiated dentin with a reduced salivary flow rate. CLINICAL RELEVANCE: Ionizing radiation associated with a reduced salivary flow rate enhanced the progression of root-dentin caries.

Influence of radiotherapy on the dentin properties and bond strength.

OBJECTIVES: The objective of this study was to evaluate the biomechanical properties of dentin and the microtensile bond strength (µTBS) performed before or after radiotherapy (RT). MATERIAL AND METHODS: Dentin chemical composition (infrared spectroscopy-FTIR), SEM images, and mechanical properties (Vickers microhardness-VHN and elastic modulus-E) were evaluated comparing no irradiated and irradiate dentin (n = 5). RT was defined by application of 72 Gy (1.8 Gy daily, 5 days per week, during 8 weeks) with sample immersed in distilled water. µTBS evaluated three groups (n = 10): NI-no irradiated; IB-irradiation before restoration; and IA-irradiation after restoration. Resin-dentin sticks (1.0 mm2) were obtained and submitted to µTBS. Analysis of the bonding interface was made by confocal microscopy. RESULTS: After RT, percentage ratio of FTIR analysis showed increased absorption for all bands. SEM image showed a disorganized dentin structure. Two-way ANOVA showed increased VHN (p = 0.005) and decreased E (p < 0.001). For µTBS, one-way ANOVA and Duncan test showed significant differences among groups (p = 0.018). IB group presented the lowest bond strength values. CONCLUSIONS: RT alters the absorption bands and SEM images showed a disorganization of the dentin structure. Mechanical properties were changed with increased VHN and decreased E. µTBS was affected by the radiotherapy and restoration period (before or after). CLINICAL RELEVANCE: RT causes changes that contribute to increased risk of tooth decay. Restorative treatments can be performed using adhesive procedures, but it is preferable to be performed before of the irradiation protocol, to guarantee better adhesive properties to restoration.

Influence of Screw Surface Treatment on Retention of Implant-Supported Fixed Partial Dentures.

The aim of this study was to assess the effect of a diamond-like carbon (DLC) coating on the removal torque of prefabricated implant screws after cyclic loading. Four groups with two crowns supported by two implants (n = 5) were obtained according to splinted and nonsplinted prosthesis, using titanium or DLC screws (splinted crowns with titanium screw [STi], splinted crowns with DLC screw [SC], nonsplinted crowns and titanium screw [NSTi], and nonsplinted crowns and DLC screw [NSC]). The prosthetic screws were tightened at 32 Ncm and retightened, and the specimens were submitted to 106 mechanical cycles (4 Hz/98 N). After cyclic loading, loosening torque was evaluated, and the final measurements were performed. Data were analyzed by two-way analysis of variance and Tukey's test (α = .005). There was statistically significance in the interaction of screw × splinting (P = .003). For the group that used titanium screws, NSTi showed smaller removal torque compared with STi. It was concluded that the use of the DLC coating screws in nonsplinted prosthesis maintain the torque after cyclic loading.

Influence of Resin Cements on Color Stability of Different Ceramic Systems.

The purpose of this study was to evaluate color stability of two dental ceramics cemented with two resin cements, assessing the color difference (ΔE00) by the measurement of L*, a*, b*, c* and h* of transmittance. The combination of two ceramic system (feldspathic and lithium disilicate) and two resin cements - color A3 (RelyX ARC and Variolink II) resulted in 4 groups (n=5). Ten disks-shaped specimens were fabricated for each ceramic system (10x1.5 mm), etched with hydrofluoric acid (10%) and silanized prior to cementation. The color analysis was performed 24 h after cementation of the samples and after 6 months of storage in relative humidity by means of spectrophotometry. The ΔE00 values were analyzed statistically by two-way ANOVA followed by the Tukey test (p<0.05). One-way ANOVA were calculated for the means of individual color coordinates (L*, a*, b*, c* and h*). Two-way ANOVA showed that only the ceramic factor was significant (p=0.003), but there was no difference for the cement factor (p=0.275) nor for the ceramic/cement interaction (p=0.161). The feldspathic ceramic showed the highest values of ΔE00. Variations in L*, a*, b*, c* and h* were more significant for feldspathic ceramic. In conclusion, storage alters similarly the optical properties of the resin cements and feldspathic porcelain was more susceptible to cement color change after aging.

Influence of Resin Cements on Color Stability of Different Ceramic Systems

Abstract The purpose of this study was to evaluate color stability of two dental ceramics cemented with two resin cements, assessing the color difference (ΔE00) by the measurement of L*, a*, b*, c* and h* of transmittance. The combination of two ceramic system (feldspathic and lithium disilicate) and two resin cements - color A3 (RelyX ARC and Variolink II) resulted in 4 groups (n=5). Ten disks-shaped specimens were fabricated for each ceramic system (10x1.5 mm), etched with hydrofluoric acid (10%) and silanized prior to cementation. The color analysis was performed 24 h after cementation of the samples and after 6 months of storage in relative humidity by means of spectrophotometry. The ΔE00 values were analyzed statistically by two-way ANOVA followed by the Tukey test (p<0.05). One-way ANOVA were calculated for the means of individual color coordinates (L*, a*, b*, c* and h*). Two-way ANOVA showed that only the ceramic factor was significant (p=0.003), but there was no difference for the cement factor (p=0.275) nor for the ceramic/cement interaction (p=0.161). The feldspathic ceramic showed the highest values of ΔE00. Variations in L*, a*, b*, c* and h* were more significant for feldspathic ceramic. In conclusion, storage alters similarly the optical properties of the resin cements and feldspathic porcelain was more susceptible to cement color change after aging.

Resumo O objetivo deste estudo foi avaliar a estabilidade da cor de dois sistemas cerâmicos em função de dois cimentos resinosos, avaliando a diferença de cor (ΔE00) pela mensuração de L*, a*, b*, c* e h* de transmitância. Formou-se 4 grupos (n=5) de acordo com as duas cerâmicas (reforçada com dissilicato de lítio e feldspática) e dois cimentos resinosos - cor A3 (RelyX ARC e Variolink II). Dez discos foram confeccionados para cada sistema cerâmico (10 x 1,5 mm), tratados com ácido fluorídrico (10%) e silanizados antes da cimentação. A análise de cor foi feita 24 h após a cimentação das amostras e após 6 meses de armazenamento em umidade relativa por meio de espectrofotometria. ANOVA a dois fatores foi utilizada para análise dos dados de ΔE00 seguido pelo teste de Tukey (p<0,05). ANOVA a um fator foi realizada para avaliação das coordenadas individuais de cor (L*, a*, b*, c* e h*). Apenas o fator cerâmica foi significativo (p=0,003),mas não houve diferença para o fator imento (p=0,275) nem para a interação entre cerâmica e cimento (p=0,161). A cerâmica feldspática apresentou os maiores valores de ΔE00. Variações de L*, a*, b*, c* e h* foram mais significativas para cerâmica feldspática. Concluiu-se que o armazenamento alterou as propriedades ópticas dos cimentos resinosos de forma semelhante e a porcelana feldspática foi mais susceptível à mudança de cor do cimento após o envelhecimento.

Associação de cerâmicas na reabilitação estética do sorriso ­ utilização de cerâmica reforçada por dissilicato de lítio e cerâmica feldspática / Ceramics association in smile aesthetic rehabilitation ­ the use of ceramics reinforced by disilicate lithium and feldspar ceramic

A demanda de pacientes que buscam por tratamentos estéticos dos dentes anteriores está em constante crescimento. A busca incessante pelo desenvolvimento de novos materiais e técnicas odontológicas, visando procedimentos mais conservadores do elemento dental e resultado mais previsível, com excelentes propriedades estéticas e funcionais, tem levado as restaurações dos dentes anteriores a um novo patamar. As cerâmicas têm sido muito estudadas e, com isso, melhoras significativas nas suas propriedades mecânicas e estéticas foram obtidas. Associado a isso, o aperfeiçoamento de técnicas adesivas tornou possível a confecção de peças cerâmicas menos espessas, sem a necessidade de grandes desgastes da estrutura dentária. O aprimoramento do diagnóstico e o planejamento reverso possibilitaram resultados bastante previsíveis. Nesse contexto, o relato de caso apresentado neste artigo descreve a sequência clínica de reabilitação estética dos dentes 11, 12, 21 e 22 empregando facetas indiretas de cerâmica reforçadas por dissilicato de lítio associadas à aplicação de cerâmica feldspática, buscando a reprodução das características naturais dos dentes. O conhecimento da técnica operatória, dos materiais restauradores e a qualidade do trabalho protético são fundamentais para se obter um resultado estético e funcional de excelência (AU).

The number of patients seeking for aesthetic treatments of the anterior teeth is constantly growing. The incessant search for the development of new dental materials and techniques, aiming more conservative procedures of the dental element and more predictable results with excellent aesthetic and functional properties, has led the restoration of anterior teeth to a new level. Ceramics have been studied and thus significant improvements in their mechanical and aesthetic properties were obtained. Associated with this, the improvement of adhesive techniques has made possible the production of thinner ceramic parts without the need of large wear of the tooth structure. Improved diagnosis and reverse planning allowed fairly predictable results. In this context, the case report presented in this article describes the clinical sequence of aesthetic restoration of teeth 11, 12, 21 and 22 employing indirect pottery facets reinforced by lithium disilicate associated with application of feldspar ceramic seeking reproduction of the natural characteristics of teeth. The Knowledge of surgical techniques, restorative materials and the quality of prosthetic work are fundamental to get aesthetic and functional results of excellence (AU).

Correlation between the Mechanical Properties and Structural Characteristics of Different Fiber Posts Systems.

The aim of this study was to evaluate the flexural strength and flexural modulus of different fiber-reinforcement composite (FRC) posts and determine the correlation between mechanical properties and structural characteristics. Eleven brands of fiber posts were analyzed (n=10): Exacto Cônico (Angelus), DT Light SL (VDW), RelyX Fiber Post (3M-Espe), Glassix Radiopaque (Nordim), Para Post Fiber White (Coltène), FRC Postec Plus (Ivoclar), Aestheti-Plus Post (Bisco), Superpost Cônico Estriado (Superdont), Superpost Ultrafine (Superdont), Reforpost (Angelus), and White Post DC (FGM). The posts were loaded in three-point bending test to calculate the flexural strength and flexural modulus using a mechanical testing machine (EMIC 2000 DL) at 0.5 mm/min. Data were submitted to one-way ANOVA and Scott-Knot test (p<0.05). The cross-sections of the posts were examined by scanning electron microscopy (SEM). Correlation between the mechanical properties and each of the structural variables was calculated by Pearson's correlation coefficients (p<0.05). The flexural strength values ranged from 493 to 835 MPa and were directly correlated with the fiber/matrix ratio (p=0.011). The flexural modulus ranged from 4500 to 8824 MPa and was inversely correlated with the number of fibers per mm2 of post (p<0.001). It was concluded that the structural characteristics significantly affected the properties of the FRC posts. The structural characteristic and mechanical properties of fiber glass posts are manufacture-dependent. A linear correlation between flexural strength and fiber/matrix ratio, as well as the flexural modulus and the amount of fiber was found.

Correlation between the Mechanical Properties and Structural Characteristics of Different Fiber Posts Systems

Abstract The aim of this study was to evaluate the flexural strength and flexural modulus of different fiber-reinforcement composite (FRC) posts and determine the correlation between mechanical properties and structural characteristics. Eleven brands of fiber posts were analyzed (n=10): Exacto Cônico (Angelus), DT Light SL (VDW), RelyX Fiber Post (3M-Espe), Glassix Radiopaque (Nordim), Para Post Fiber White (Coltène), FRC Postec Plus (Ivoclar), Aestheti-Plus Post (Bisco), Superpost Cônico Estriado (Superdont), Superpost Ultrafine (Superdont), Reforpost (Angelus), and White Post DC (FGM). The posts were loaded in three-point bending test to calculate the flexural strength and flexural modulus using a mechanical testing machine (EMIC 2000 DL) at 0.5 mm/min. Data were submitted to one-way ANOVA and Scott-Knot test (p<0.05). The cross-sections of the posts were examined by scanning electron microscopy (SEM). Correlation between the mechanical properties and each of the structural variables was calculated by Pearson's correlation coefficients (p<0.05). The flexural strength values ranged from 493 to 835 MPa and were directly correlated with the fiber/matrix ratio (p=0.011). The flexural modulus ranged from 4500 to 8824 MPa and was inversely correlated with the number of fibers per mm2 of post (p<0.001). It was concluded that the structural characteristics significantly affected the properties of the FRC posts. The structural characteristic and mechanical properties of fiber glass posts are manufacture-dependent. A linear correlation between flexural strength and fiber/matrix ratio, as well as the flexural modulus and the amount of fiber was found.

Resumo O objetivo deste estudo foi avaliar a resistência à flexão e módulo de flexão de diferentes pinos reforçados com fibra (PRF) e determinar a correlação entre propriedades mecânicas e características estruturais. Foram analisadas onze marcas de pinos de fibra (n=10): Exacto Cónicos (Angelus), DT Luz SL (VDW), RelyX Fiber Post (3M ESPE), Glassix Radiopaque (Nordim), Pará Publicar Fiber White (Coltène), FRC Postec Plus (Ivoclar), Aestheti-Plus Post (Bisco), Superpost Cónicos Estriado (Superdont), Superpost Ultrafino (Superdont), Reforpost (Angelus), e White Post DC (FGM). Os pinos foram avaliados por meio de ensaio de flexão de três pontos para calcular a resistência à flexão e módulo de flexão utilizando uma máquina de ensaios mecânicos (EMIC 2000 DL) a 0,5 mm/min. Os dados foram submetidos a ANOVA one-way e teste de Scott-Knot (p<0,05). As secções transversais dos pinos foram examinadas usando microscopia eletrônica de varredura (MEV). A correlação entre as propriedades mecânicas e de cada uma das variáveis estruturais foi calculada por coeficientes de correlação de Pearson (p<0,05). Os valores da resistência à flexão variaram de 493-835 MPa e foram diretamente correlacionados com a proporção de fibra/matriz (p=0,011). O módulo de flexão variou de 4500 a 8824 MPa e foi inversamente correlacionado com o número de fibras por mm2 (p<0,001). Concluiu-se que as características estruturais afetam de forma significativa as propriedades dos pinos de fibra. As características estruturais e propriedades mecânicas dos pinos de fibra de vidro são dependentes do processo de fabricação. Existe uma correlação linear entre a resistência à flexão e proporção de fibra/matriz, bem como entre o módulo de flexão e a quantidade de fibras.

Degree of Conversion and Mechanical Properties of Resin Cements Cured Through Different All-Ceramic Systems.

The aim of this study was to verify the degree of conversion (DC), Vickers microhardness (VH) and elastic modulus (E) of resin cements cured through different ceramic systems. One 1.5-mm-thick disc of each ceramic system (feldspathic, lithium dissilicate and zircônia veneered with feldspathic) was used. Three dual-cured (Allcem, Variolink II and RelyX U200) and one chemically-cured (Multilink) resin cements were activated through ceramic discs. For dual-cured resin cements was used a conventional halogen light-curing unit (Optilux 501 at 650 mW/cm2 for 120 s). Samples cured without the ceramic disc were used as control. The samples were stored at 37 °C for 24 h. ATR/FTIR spectrometry was used to evaluate the extent of polymerization in the samples (n=5). Micromechanical properties - VH and E - of the resin cements (n=5) were measured with a dynamic indentation test. Data were statistically analyzed with two-way ANOVA, Tukey's test and Pearson's correlation (α=0.05). DC was affected only by the type of resin cement (p=0.001). For VH, significant interaction was detected between resin cement and ceramic (p=0.045). The dual-cured resin cements showed no significant differences in mean values for E and significantly higher values than the chemically-cured resin cement. The degree of conversion and the mechanical properties of the evaluated resin cements depend on their activation mode and the type of ceramics used in 1.5 mm thickness. The dual-cured resin cements performed better than the chemically-cured resin cement in all studied properties.

Degree of Conversion and Mechanical Properties of Resin Cements Cured Through Different All-Ceramic Systems

Abstract: The aim of this study was to verify the degree of conversion (DC), Vickers microhardness (VH) and elastic modulus (E) of resin cements cured through different ceramic systems. One 1.5-mm-thick disc of each ceramic system (feldspathic, lithium dissilicate and zircônia veneered with feldspathic) was used. Three dual-cured (Allcem, Variolink II and RelyX U200) and one chemically-cured (Multilink) resin cements were activated through ceramic discs. For dual-cured resin cements was used a conventional halogen light-curing unit (Optilux 501 at 650 mW/cm2 for 120 s). Samples cured without the ceramic disc were used as control. The samples were stored at 37 °C for 24 h. ATR/FTIR spectrometry was used to evaluate the extent of polymerization in the samples (n=5). Micromechanical properties - VH and E - of the resin cements (n=5) were measured with a dynamic indentation test. Data were statistically analyzed with two-way ANOVA, Tukey's test and Pearson's correlation (α=0.05). DC was affected only by the type of resin cement (p=0.001). For VH, significant interaction was detected between resin cement and ceramic (p=0.045). The dual-cured resin cements showed no significant differences in mean values for E and significantly higher values than the chemically-cured resin cement. The degree of conversion and the mechanical properties of the evaluated resin cements depend on their activation mode and the type of ceramics used in 1.5 mm thickness. The dual-cured resin cements performed better than the chemically-cured resin cement in all studied properties.

Resumo: O objetivo deste estudo foi mensurar grau de conversão (GC), microdureza Vickers (VH) e módulo de elasticidade (E) de cimentos resinosos polimerizados através de diferentes sistemas cerâmicos. Um disco de 1,5 mm de espessura de cada sistema cerâmico (cerâmica feldspática, dissilicato de lítio e zircônia coberto por cerâmica feldspática) foi utilizado. Três cimentos resinosos duais (Allcem, Variolink II e RelyX U200) e um cimento resinoso quimicamente ativado (Multilink) foram ativados através dos discos de cerâmica. Para os cimentos resinosos duais foi utilizado um aparelho de lâmpada halógena (Optilux 501 a 650 mW/cm2 por 120 s). Amostras polimerizadas sem a interposição do disco de cerâmica foram utilizadas como controle. As amostras foram armazenadas a 37 °C durante 24 h. ATR/FTIR foi utilizado para avaliar a extensão da polimerização nas amostras (n=5). Propriedades micromecânicas - VH e E - dos cimentos resinosos (n=5) foram medidas com um teste dinâmico de indentação. Os dados foram analisados através de análise de variância a dois fatores, teste de Tukey e correlação de Pearson (α=0,05). O GC foi afetado somente pelo tipo de cimento resinoso (p=0,001). Para VH, houve interação entre o tipo de cimento resinoso e o tipo de cerâmica (p=0,045). Os cimentos resinosos duais não apresentaram diferenças significativas nos valores médios de E e valores significativamente maiores que o cimento resinoso quimicamente ativado. O grau de conversão e as propriedades mecânicas dos cimentos resinosos avaliados dependem do seu modo de ativação e do tipo de cerâmica usada na espessura de 1,5 mm. Os cimentos resinosos duais desempenharam melhor que o cimento resinoso quimicamente ativado em todas as propriedades estudadas.