The effect of speed sintering on the optical properties and microstructure of multi-layered cubic zirconia.

PURPOSE: Speed sintering was introduced to fabricate time-efficient chairside restorations, however, its influence on the microstructure and optical properties of zirconia is still unclear. This study investigated the influence of speed sintering on the microstructure and optical properties of ultra-translucent multi-layered cubic zirconia. MATERIALS AND METHODS: Ultra-translucent cubic zirconia (Katana™ UTML; Kuraray Noritake Dental Inc., Aichi, Japan) was cut into a total of 80 specimens, twenty within each layer of the blank. The specimens were divided into 2 groups: speed and conventional sintering. The translucency parameter, opalescence, chromaticity, and color difference were recorded using a spectrophotometer. Scanning electron microscope images were used for crystallographic analysis. One-way ANOVA and Tukey's post-hoc test (p < 0.05) were used for data analysis. RESULTS: Speed sintering significantly reduced the translucency and opalescence compared to conventional sintering excluding the opalescence of the dentin layer. Chromaticity significantly decreased with speed sintering in less chromatic layers and significantly increased in more chromatic layers. Mean color change ranged between 0.65 and 1.25 across different layers. Mean crystal size decreased with speed sintering. CONCLUSIONS: With speed sintering, translucency, and opalescence decrease while chromaticity increases in the more chromatic layers. Additionally, no clinically perceptible color change was found compared to conventional sintering.

Build angle effect on 3D-printed dental crowns marginal fit using digital light-processing and stereo-lithography technology: an in vitro study.

BACKGROUND: The effect of 3D printing technology and build angle on the marginal fit of printed crowns is unclear. The objective of this research was to use digital light processing (DLP) and stereo-lithography (SLA)-based 3D printing to construct single restorations with varied build angles and to analyze the crowns' marginal fit. METHODS: A prepared resin first molar was scanned utilizing an optical scanner. Three build orientations were used to construct the specimens: 0, 45, and 90º. DLP and SLA technology were used to produce the casting patterns. A digital microscope was used to measure the marginal gaps. The effect of build orientation was statistically analyzed by using Two-way ANOVA followed by pair-wise Tukey test. RESULTS: Two-way ANOVA revealed a significant effect of printer technology and build angle on the marginal discrepancy of 3D printed crowns (p < 0.001). One-way ANOVA revealed that SLA printers (55.6 [± 13.59]) showed significantly better mean [± SD] marginal discrepancy in µm than DLP printers (72 [± 13.67]) (p < 0.001). Regarding build angle, one-way ANOVA revealed significant differences between the different angles. Tukeys post-hoc test revealed that 0° (48.5 [± 9.04]) had the significantly smallest marginal discrepancy followed by 45° (62.5 [± 8.05]) then 90° (80.5 [± 8.99]) (p < 0.001). CONCLUSION: The build orientation affects the marginal discrepancy of single crowns manufactured utilizing DLP and SLA.

Effect of cervical margin relocation on marginal adaptation and microleakage of indirect ceramic restorations.

PURPOSE: This study evaluated the effect of cervical margin relocation (CMR) with two different materials and contamination with hemostatic agents on the margin adaptation and microleakage of ceramic restorations. MATERIALS AND METHODS: Mesial-occlusal-distal cavities were prepared in 60 human first molars and distributed to 3 groups (n = 20) according to the margin relocation procedure. The groups were: group F; flowable composite applied in two 2 mm increments, group B; bulk-fill flowable composite applied as a bulk increment of 4 mm thickness and group C (control); no CMR was done. Each group was subdivided into two subgroups (subgroup N; no hemostatic agent applied and subgroup H; hemostatic agent was applied). In all groups, ceramic inlays were prepared and cemented. The samples were subjected to thermocycling (10,000 cycles). The adaptation of the cervical margin was evaluated with scanning electron microscopy (200×). Samples were then assessed for microleakage analysis with the dye penetration method. Marginal adaptation data were normally distributed and analyzed using two-way ANOVA followed by Tukey's post hoc test. Ordinal microleakage score data were analyzed using cumulative link models followed by the analysis of deviance using Wald chi-square tests. RESULTS: Both CMR and contamination with a hemostatic agent had significant effects on the margin adaptation of the cervical margin. Group C showed the highest adaptation with no significant difference from group F. The lowest adaptation was revealed in group B with a significant difference from group C. Subgroup N (in all groups) showed a statistically higher adaptation than subgroup H. Regarding microleakage assessment, CMR had no significant effect but hemostatic agent application showed a significantly higher microleakage score for all groups. CONCLUSIONS: Both the CMR procedure and contamination with AlCl3 hemostatic agent had a negative effect on marginal adaptation. For microleakage assessment, only contamination with hemostatic agent negatively affected the microleakage with no effect on the margin relocation procedure.

Accuracy and repeatability of different intraoral instruments on shade determination compared to visual shade selection.

OBJECTIVE: To evaluate the accuracy and repeatability of intraoral instruments used for shade determination compared to visual shade selection (VSS). MATERIALS AND METHODS: A total of 20 subjects and 10 observers, balanced by gender, participated in the study. Observers performed VSS of the upper right central incisor from each subject. Instrumental shade determination of the same teeth was performed using a spectrophotometer (Easyshade V) and intraoral scanners (CEREC Omnicam, Primescan, Trios 3 and Trios 4). Vita Classical shade nomenclature was used to record the shade designation for all instruments and VSS. The accuracy of the instruments was determined by comparing the instrument readings with the most frequent visual shade selected. The percentage of accuracy was obtained by comparing the number of agreements with the number of comparisons. The percentage of repeatability was obtained by comparing the number of repeated shades with the number of shade measurements in each group. Accuracy was compared using Cochran Q test followed by pairwise comparisons using multiple McNemar's tests with Bonferroni correction. Repeatability of the instruments was evaluated using Cronbach's alpha. RESULTS: Omnicam showed a significant lower accuracy than the other instruments (p < 0.05). No statistical difference on repeatability was found among the different instruments (p > 0.05). It was not found any statistical differences for VSS accuracy among the observers (p = 0.437) and between genders (p = 0.867). CONCLUSION: Instrumental repeatability (≥75%) and similar accuracy between the best performed instruments (69%-77.5%) and the observers performance (65%-90%) supports the use of high-performance instruments for dental shade determination. CLINICAL SIGNIFICANCE: Most instruments (Easyshade V, Primescan, Trios 3, and Trios 4) showed similar accuracy performance to observers in the VSS.

Effect of Different Preparation Depths for an Inlay-Retained Fixed Partial Denture on the Accuracy of Different Intraoral Scanners: An In Vitro Study.

PURPOSE: The aim was to evaluate the effect of different preparation depths for inlay-retained fixed partial dentures on the accuracy of intraoral scanners. MATERIALS AND METHODS: Tooth preparations for two inlay-retained fixed partial dentures were done and divided according to depth of the preparation. Group A: 2 mm pulpal floor depth, 3 mm gingival floor depth and Group B: 3 mm pulpal floor depth, 4mm gingival floor depth. The CEREC Omnicam 4.4.4, Omnicam 4.6.2. Trios3 and Medit i500 intraoral scanners were used in this study. Tooth preparations were scanned by each scanner 10 times. The STL files obtained from the intraoral scanners were compared to the reference models (trueness) and within each test group (precision) using a 3D comparison software. Data were then statistically analyzed. RESULTS: Regarding trueness, two-way ANOVA revealed significant differences between the different types of scanners (p < 0.001) (Omnicam 4.4.4: 65.09 ± 2.87 Omnicam 4.6.1: 52.73 ± 3.31 Medit i500: 58.45 ± 2.63 Trios 3: 41.79 ± 4.42). Preparation depth had no significant influence on the trueness (p = 0.083). For precision two-way ANOVA revealed significant differences between the different types of scanners (p < 0.001). Preparation depth had no significant influence on the precision (p = 0.111). Statistically significant interactions were found between the different variables. CONCLUSIONS: The depth of preparation did not have an influence on the accuracy of different scanners. However, the type of scanner influenced the accuracy of digital impressions with Trios3 showing the highest accuracy.

Influence of different combinations of CAD-CAM crown and customized abutment materials on the force absorption capacity in implant supported restorations - In vitro study.

OBJECTIVES: To evaluate the force absorption capacity of implant supported restorations utilizing different CAD-CAM materials for the fabrication of crowns and customized abutments. METHODS: 80 titanium inserts were scanned to design customized abutments and crowns. The specimens were divided into four groups (n = 20/material): (Z): zirconia, (P): PEEK, (V): VITA Enamic, and (E): IPS e.max. Each group was subdivided into two subgroups according to customized abutment material: (Z) zirconia, and (P) for PEEK. For the assessment of force absorption, all specimens were loaded in a universal testing machine, applied loads curves were collected from the machine's software, and resulting loads curves were collected from forcemeter below the assembly. The slopes of all curves were analyzed using Two-way multivariate analysis of variance with pairwise comparisons using Tukey Post Hoc test (p < 0.05). RESULTS: The curve progression of the applied and resulting forces varied among the investigated materials for each specimen. For zirconia abutments, ZZ showed the highest slope values of the applied and resulting force curves, followed by EZ, VZ, and PZ demonstrating statistically significant differences (P < .001). As for PEEK abutments, ZP and EP showed the least slope values, followed by PP then VP demonstrating statistically significant differences (P < .001). For Zirconia and e.max crowns, using PEEK abutments significantly increased slope loss. As for PEEK and Vita Enamic crowns changing abutment material did not significantly affect slope loss. SIGNIFICANCE: Combining rigid crown materials with less rigid abutments might enhance their force absorption capacity. However, with less rigid crown materials a stiff substructure might be mandatory to preserve their force absorption behavior.

In vitro evaluation of material dependent force damping behavior of implant-supported restorations using different CAD-CAM materials and luting conditions.

STATEMENT OF PROBLEM: Although force-damping behavior that matches natural teeth may be unobtainable, an optimal combination of crown material and luting agent might have a beneficial effect on the force absorption capacity of implant-supported restorations. However, the force-absorbing behavior of various restorative materials has not yet been satisfactorily investigated. PURPOSE: The purpose of this in vitro study was to evaluate the material dependent force-damping behavior of implant-supported crowns fabricated from different computer-aided design and computer-aided manufacturing (CAD-CAM) materials luted to implant abutments under different conditions. MATERIAL AND METHODS: Titanium inserts (N=84) were screwed to implant analogs, scanned to design zirconia abutments, and divided into 4 groups to receive CAD-CAM fabricated crowns in 4 materials: zirconia, polyetheretherketone (PEEK), polymer-infiltrated ceramics (VITA ENAMIC), and lithium disilicate (e.max). The crowns were subdivided as per the luting agent: none, interim cement, and adhesive resin cement. Measurements were performed by loading specimens in a universal testing machine with an increasing force and measuring the resulting force with a digital forcemeter, followed by image processing and data acquisition. Two-way multivariate analysis of variance (MANOVA) was used to assess all interactions with multiple pairwise comparisons (α=.05). RESULTS: The curve progression of the applied and resulting forces varied significantly among the investigated materials, resulting in differently inclined slopes for each material (P<.001). With no cementation, the mean slope values of the resulting force curves ranged from 77.5 ±0.03 degrees for zirconia, followed by 71.8 ±0.03 degrees for lithium disilicate, 56.2 ±0.1 degrees for polymer-infiltrated ceramics, and 51.1 ±0.01 degrees for polyetheretherketone. With interim cementation, the mean slope values ranged from 75.4 ±0.01 degrees for zirconia, followed by 70.05 ±0.02 degrees for lithium disilicate, 56.1 ±0.02 degrees for polymer-infiltrated ceramics, and 52.2 ±0.1 degrees for polyetheretherketone. As with adhesive cementation, curve slopes ranged from 73.2 ±0.02 degrees for zirconia, followed by 70.5 ±0.2 degrees for lithium disilicate, 55.9 ±0.04 degrees for polymer-infiltrated ceramics, and 52.3 ±0.1 degrees for polyetheretherketone. Slope loss was significant after the cementation of zirconia and lithium disilicate crowns but less significant for polymer-infiltrated ceramics and polyetheretherketone. CONCLUSIONS: Force damping is generally material dependent, yet implant-supported crowns fabricated from resilient materials such as polymer-infiltrated ceramics and PEEK show better force absorption than rigid materials such as zirconia and lithium disilicate ceramics. Furthermore, cementation of rigid materials significantly increased slope loss, indicating enhancement in their force-damping behavior, whereas less-rigid materials benefit less from cementation. Further studies are essential to investigate the effect of prosthetic materials on the stress distribution to the peri-implant bone in the crown-abutment-implant complex.

Accuracy and repeatability of different intraoral scanners on shade determination.

OBJECTIVE: To evaluate the accuracy and repeatability of different intraoral scanners on shade determination. MATERIALS AND METHODS: Ten different shades of Vita Mark II blocks were used. A disc-shape specimen (10 mm in diameter and 1 mm thick) per ceramic block was fabricated. Ten color measurements per specimen were performed by each instrument (Vita Easyshade V [control], 3shape Trios, Cerec Omnicam, Cerec Primescan) and recorded in Vita Classic color system. The number of correct shade match per instrument for each shade was recorded. Instrumental accuracy was compared using Cochran Q test and repeatability was analyzed using Cronbach's alpha. RESULTS: There was a significant difference in the instrumental accuracy for shade determination (p < 0.001). There was no statistical difference between the Easyshade V (78%) and the 3Shape Trios (66%) (p > 0.05), with the latter being similar to the other scanners Primescan(63%) and Omnicam (57%) (p > 0.05). No significant difference was found (p > 0.05) when different shades were evaluated by the same instrument. Similar repeatability was found for the different devices, ranging from 44.3% for Easyshade to 51.9% for Omnicam. CONCLUSION: The evaluated instruments showed less than expected repeatability and accuracy on measuring different dental shades. Therefore, caution should be exercised when using instrumental shade determination, which should be accompanied by experienced human visual assessment. CLINICAL SIGNIFICANCE: The outcome of this study might help clinicians evaluate the performance of intraoral scanners as a shade matching tool.

Effect of photo-polymerization mode on the degree of conversion of resin cement under different ceramic materials.

BACKGROUND: This study evaluated the effect of different polymerization modes and duration on the degree of conversion (DC) of resin cement under different types of ceramics. METHODS: Ceramic materials were divided into 3 groups (N.=60): group 1, Cerasmart; group 2, Vita Enamic; and group 3, Vita Mark II. Each group was then divided into three subgroups (N.=20) according to the polymerization mode (A: low-intensity; B: high-intensity; and C: soft-start). Subgroups were then divided into two further groups according to the polymerization time (I: 10 s; and II: 20 s). DC of light-cured resin cement beneath different kinds of ceramics was tested using FTIR spectroscopy. Results were compared to a control group cured without overlying ceramic. RESULTS: While the type of ceramic and mode of polymerization showed a significant effect on the DC of resin cement, polymerization duration did not. Vita Mark II group showed the highest DC of resin cement followed by Vita Enamic and Cerasmart. High- and low-intensity polymerization modes did not show significant difference, but both showed significantly lower DC when compared to soft start mode. CONCLUSIONS: Type of ceramic and polymerization mode showed a direct effect on the DC of resin cement.

Influence of Preparation Type and Tooth Geometry on the Accuracy of Different Intraoral Scanners.

PURPOSE: To evaluate the influence of preparation design and tooth geometry on the accuracy of scans obtained from three different intraoral scanners (IOS). MATERIALS AND METHODS: Full coverage crown and inlay preparations with known axial wall tapers (6ᵒ and 12ᵒ) were performed on typodont teeth using a computer numerical control machine. Reference models were scanned with a highly accurate reference scanner (Ineos X5) and saved in standard tessellation language (STL) format then each IOS (Omnicam, Trios, and i500) scanned each model 10 times. The STL files obtained from the intraoral scanners were compared to the reference models (trueness) and within each test group (precision). Data were statistically analyzed using three- way ANOVA and one- way ANOVA. RESULTS: When comparing trueness values extracoronal preparations (32.30 ± 11.23 µm) was significantly better than intra-coronal preparation (59.61 ± 16.42 µm). As for opposing wall taper, one-way ANOVA revealed that the more the convergence or divergence between opposing walls the better is the trueness. Significant differences were observed between the scanners. 3 Shape Trios (35.70 ± 14.12 µm) and medit i500 (44.31 ± 11.41 µm) showed no statistically significant differences. However, both showed significantly better precision results when compared to Omnicam (57.83 ± 22.14 µm). CONCLUSION: Extracoronal preparations show better trueness and precision in comparison to intracoronal preparations. Trios and i500 have better trueness and precision than Omnicam. Increasing the taper of the axial wall has a direct effect on trueness of scans obtained from the IOS.

Mechanical behavior of posterior all-ceramic hybrid-abutment-crowns versus hybrid-abutments with separate crowns-A laboratory study.

OBJECTIVE: The purpose of this laboratory study was to evaluate the fatigue resistance, fracture resistance and mode of failure of posterior hybrid-abutment-crown vs. hybrid-abutment with separate crown, both bonded to short titanium bases. MATERIALS AND METHODS: Thirty-two titanium implants were embedded perpendicularly in auto-polymerizing resin. Implant-supported restorations simulating a maxillary first premolar were designed and milled using a CAD/CAM system and divided into 2 groups according to material (n = 16): zirconia (Z) and lithium disilicate (L). Each group was subdivided into two subgroups according to design (n = 8): hybrid-abutment-crown (ZS, LS) and hybrid-abutment with separate crown (ZC, LC). Each group was subjected to 1.2 million cycles of thermo-mechanical fatigue loading in a dual-axis chewing simulator at 120 N load. Surviving specimens were subjected to quasi-static loading in a universal testing machine. Mode of failure was determined under a low magnification optical microscope. RESULTS: During chewing simulation, 18.8% of zirconia and 43.8% of lithium disilicate restorations failed. The fracture resistance median values ranged from 3,730 N for group ZC, 3,400 N for group ZS, 1,295 N for group LS to 849 N for group LC. Group ZC had a statistically significant higher fracture resistance than groups LC and LS; however, it did not differ significantly from group ZS (p ≤ 0.05). Failures were seen in both titanium bases and ceramic superstructure. CONCLUSIONS: Zirconia and lithium disilicate hybrid implant-supported restorations with short (3 mm) titanium bases failed in a considerable number already during chewing simulation. Therefore, despite their high fracture strength the use in the posterior region should be considered critically.

Assessment of marginal adaptation and fracture resistance of endocrown restorations utilizing different machinable blocks subjected to thermomechanical aging.

OBJECTIVE: This in vitro study was conducted to assess the marginal adaptation and fracture resistance of computer aided design/computer aided manufacturer (CAD-CAM) fabricated endocrowns restoring endodontically treated molars using different machinable blocks with thermomechanical loading protocols. MATERIALS AND METHODS: Devitalized mandibular molars were prepared in a standardized way and divided into 4 groups (n = 10) to receive CAD/CAM fabricated endocrowns using four materials (Lithium disilicate ceramics, polymer infiltrated ceramics, zirconia-reinforced lithium silicate ceramics and resin nanoceramics. Marginal gaps (µm) were measured using stereomicroscope before cementation and after cementation. After thermomechanical aging, marginal gap measurements were repeated, and then fracture resistance test was performed. Two-way analysis of variance (ANOVA) and Tukey HSD multiple comparisons were used to assess the effect of material on the marginal gap before, after cementation, and after thermomechanical aging. One Way ANOVA was used to assess the effect of material on the fracture resistance. RESULTS: The difference between marginal gaps values of the tested materials was statistically insignificant but with significant increase after cementation and after thermomechanical aging. Cerasmart endocrowns showed the highest mean fracture load value (1508.5 ± 421.7N) with statistically significant difference than Vita Enamic endocrowns and Celtra Duo. CONCLUSION: The tested materials showed marginal vertical gap readings within the limits of clinically acceptable standards. Resin nanoceramics and lithium disilicate showed the highest values of fracture resistance followed by polymer infiltrated ceramics favoring their use for endocrown restorations. CLINICAL SIGNIFICANCE: The mechanical behavior of ceramic materials varies with the variation of their structure and mechanical properties. Accordingly, further investigation is always needed to explore the biomechanical behavior of recent materials when used as endocrowns before clinical trials.

Fracture resistance and failure modes of polymer infiltrated ceramic endocrown restorations with variations in margin design and occlusal thickness.

PURPOSE: The purpose of this in vitro study was to assess the effect of varying the margin designs and the occlusal thicknesses on the fracture resistance and mode of failures of endodontically treated teeth restored with polymer infiltrated ceramic endocrown restorations. METHODS: Root canal treated mandibular molars were divided into four groups (n=8) and were prepared to receive Computer-Aided Design/Computer-Aided Manufacturing (CAD/CAM) fabricated polymer infiltrated ceramic endocrowns (ENAMIC blocks). Group B2 represents teeth prepared with a butt joint design receiving endocrowns with 2mm occlusal thickness and the same for group B3.5 but with 3.5mm occlusal thickness. Group S2 represents teeth prepared with 1mm shoulder finish line receiving endocrowns with 2mm occlusal thickness and the same for group S3.5 but with 3.5mm occlusal thickness. After cementation and thermal aging, fracture resistance test was performed and failure modes were observed. RESULTS: Group S3.5 showed the highest mean fracture load value (1.27±0.31kN). Endocrowns with shoulder finish line had significantly higher mean fracture resistance values than endocrowns with butt margin (p<0.05). However, the results were not statistically significant regarding the restoration thickness. Evaluation of the fracture modes revealed no statistically significant difference between the modes of failure of tested groups. CONCLUSIONS: For the restoration of endodontically treated teeth, adding a short axial wall and shoulder finish line can increase the fracture resistance. However, further investigations, especially the fatigue behavior, are needed to ensure this effect applies with small increases of restoration thickness.