RESUMO
PURPOSE: The aim of this in vitro study was to evaluate the color stability and degree of conversion (DC) of dual-cure and light-cure cements and flowable composites after thermal aging. MATERIALS AND METHODS: A total of 50 human incisors were prepared and divided into six groups (n = 10). Veneers were fabricated using IPS Empress Direct composite resin were bonded with three types of luting agents: Light-cured, conventional dual, and flowable composite according to the manufacturer's instructions. The groups were as follows: Filtek Z350XT Flow/Single Bond 2, RelyX ARC/Single Bond 2, RelyX Veneer/Single Bond 2, Tetric N-Flow/Tetric N-Bond, and Variolink II/Tetric N-Bond. Commission Internationale de l'Éclairage L*, a* and b* color coordinates were measured 24 h after cementation procedure with a color spectrophotometer and reevaluated after 10,000 thermal cycles. To evaluate the DC 50 specimens (n = 10) of each resin material were obtained and Fourier transform infrared spectroscopy was used to evaluate the absorption spectra. Statistical analysis was performed with one-way ANOVA and Tukey's test (α = 0.05). RESULTS: No statistically significant differences in ΔE* occurred after aging. The greatest change in lightness occurred in the Variolink II resin cement. Changes in red-green hue were very small for the same cement and largest in the Tetric N-Flow flowable resin composite, while the greatest change in blue-yellow hue was a yellowing of the RelyX ARC luting cement. RelyX ARC exhibited the highest DC, and there were no statistically significant differences in DC among the other cements. CONCLUSIONS: Resin-based luting agent might affect the final of ceramic veneer restorations. The thermal aging affected the final color of the evaluated materials, and these were regarded as clinically unacceptable (ΔE >3.3).
RESUMO
OBJECTIVE: This study evaluated the effect of the composite photoactivation mode on microtensile bond strength and Knoop microhardness. METHODS: Standard class I cavities (3 x 4 x 3mm) were restored with two adhesives systems, Single Bond (SB) and Clearfil SE Bond (CE), and the TPH composite. The photoactivation of the composite was carried out using three modes: Conventional (CO: 400 mW/cm(2) x 40s), Soft-Start (SS: 100 mW/cm(2) x 10s+600 mW/cm(2) x 30s) and Pulse-Delay (PD: 100 mW/cm(2) x 3s+3 min wait+600 mW/cm(2) x 37s). For the microtensile test, beams obtained from the buccal wall bond interface were tested under tension at 0.5mm/min crosshead speed until failure. For the microhardness test, the restorations were sectioned in the mesio-distal direction and indentations were made on the internal composite surface of each half at three different depths. Data of two tests were analyzed using two-way ANOVA and LSMeans (alpha=0.05). RESULTS: In the microtensile test, SS presented the highest values. PD presented intermediate values without differing significantly from the other modes. For adhesives, SB presented the highest values. In the microhardness test, PD presented the highest values, differing significantly from SS. CO presented intermediate values but without any statistical difference from the others. The SS-CE interaction presented the lowest values with statistical differences from all the others. SIGNIFICANCE: By the SS technique, the highest bond strength was obtained. However, this technique made it possible for the adhesive system to intervene with the hardness of the composite.