RESUMO
We present a data reduction and visualization approach for the microdomain dynamics in block copolymers and similar structured fluids. Microdomains are reduced to thin smooth lines with colored branching points and visualized with a tool for protein visualization. As a result the temporal evolution of large volume data sets can be perceived within seconds. This approach is demonstrated with simulation results based on the dynamic density functional theory of the ordering of microdomains in a thin film of block copolymers. As an example we discuss the dynamics at the cylinder-to-gyroid grain boundary and compare it to the epitaxial cylinder-to-gyroid phase transition predicted by Matsen [Phys. Rev. Lett. 80, 4470 (1998)].
RESUMO
An approach for automated nanotomography, a layer-by-layer imaging technique based on scanning probe microscopy (SPM), is presented. Stepwise etching and imaging is done in situ in a liquid cell of an SPM. The flow of etching and rinsing solutions after each etching step is controlled with solenoid valves which allow for an automated measuring protocol. The thermal drift and the drift of the piezo scanner is corrected by applying offsets calculated from the cross correlation coefficients between successive images. As an example, we have imaged human bone with approximately 10 nm resolution using tapping mode SPM and successive etching with hydrochloric acid.
