A user-friendly FIB lift-out technique to prepare plan-view TEM sample of 2D thin film materials.

Plan-view transmission electron microscopy (TEM) or electron diffraction imaging of a bulk or 2D material can provide detailed information about the structural or atomic arrangement in the material. A systematic and easily implementable approach to preparing site-specific plan-view TEM samples for 2D thin film materials using FIB is discussed that could be routinely used. The methodology has been successfully applied to prepare samples from 2D materials such as, MoS2 thin film, vertically oriented graphene film (VG), as well as heterostructure material SnTiS3. It is worth mentioning that in contrast to planar conventional graphene, VG grows vertically from the substrate and takes nanosheet arrays. Samples prepared using this methodology provide a simple, faster, and precise course in obtaining valuable structural information. The top-view imaging offers various information about the growth nature of the materials suggesting the efficiency of the sample preparation process.

A review of focused ion beam applications in optical fibers.

Focused ion beam (FIB) technology has become a promising technique in micro- and nano-prototyping due to several advantages over its counterparts such as direct (maskless) processing, sub-10 nm feature size, and high reproducibility. Moreover, FIB machining can be effectively implemented on both conventional planar substrates and unconventional curved surfaces such as optical fibers, which are popular as an effective medium for telecommunications. Optical fibers have also been widely used as intrinsically light-coupled substrates to create a wide variety of compact fiber-optic devices by FIB milling diverse micro- and nanostructures onto the fiber surface (endfacet or outer cladding). In this paper, the broad applications of the FIB technology in optical fibers are reviewed. After an introduction to the technology, incorporating the FIB system and its basic operating modes, a brief overview of the lab-on-fiber technology is presented. Furthermore, the typical and most recent applications of the FIB machining in optical fibers for various applications are summarized. Finally, the reviewed work is concluded by suggesting the possible future directions for improving the micro- and nanomachining capabilities of the FIB technology in optical fibers.

Discerning the Contribution of Morphology and Chemistry in Wettability Studies.

The wetting behavior of homogeneous systems is now well understood at the macroscopic scale. However, this understanding offers little predictive power regarding wettability when mesoscopic chemical and morphological heterogeneities come into play. The fundamental interest in the effect of heterogeneity on wettability is derived from its high technological relevance in several industries, including the petroleum industry where wettability is recognized as a key determinant of the overall efficiency of the water-flooding-based enhanced oil recovery process. Here, we demonstrate the use of the atomic force microscopy force curve measurements to distinguish the roles of chemistry and morphology in the wetting properties of rock formations, thus providing a clear interpretation and deeper insight into the wetting behavior of heterogeneous formations. Density functional theory calculations further prove the versatility of our approach by establishing benchmarks on ideal surfaces that differ in chemistry and morphology in a predefined manner.

Gradient-index optical fiber lens for efficient fiber-to-chip coupling.

A gradient-index optical fiber lens is proposed and fabricated on the tip of a single-mode fiber using focused ion beam milling. Second-order effective medium theory is used to design a gradual change in the fill factor, which ensures a parabolic effective refractive index distribution. The proposed fiber lens design is simulated via the three-dimensional finite-difference time-domain method, and demonstrated through confocal optical measurements. At a wavelength of 1550 nm, the fabricated lenses focus a 10.4 µm mode field diameter exiting the fiber into spot sizes between 3-5 µm, located 4-6 µm away from the fiber tip. Direct coupling into a silicon-on-insulator chip is also demonstrated, where the fabricated gradient-index lens has a coupling efficiency comparable to a commercial lensed fiber.