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1.
J Nanosci Nanotechnol ; 20(6): 3424-3431, 2020 06 01.
Artigo em Inglês | MEDLINE | ID: mdl-31748035

RESUMO

The AgBrO3/few-layer g-C3N4 composite photocatalyst has been developed via an in-situ synthetic method. The structure, morphology, light response range, separation and migration efficiency of the photogenerated electron-hole pairs and element valence state of the as-obtained samples have been characterized. The tetracycline was used to discuss the photocatalytic activities of the samples. The photocatalytic degradation mechanism of the as-obtained composites was also researched. The analysis results show that the photocatalytic degradation property of the asobtained composite photocatalyst appears to the tendency of first increasing and then decreasing with increasing the amount of AgBrO3 under visible light illumination. When the mass ratio of AgBrO3 to g-C3N4 is 4:3, in 60 min, the photocatalytic degradation efficiency of the as-obtained composites reaches the maximum of 79%. It is 37% and 45% higher than that of pure AgBrO3 and g-C3N4, respectively. Moreover, the separation and migration efficiency of the photogenerated electron-hole pairs of the as-prepared composites are also enhanced. In addition, superoxide radicals and holes are the dominant active species during the photocatalytic degradation process.


Assuntos
Compostos de Nitrogênio , Tetraciclina , Catálise , Grafite , Luz
2.
J Nanosci Nanotechnol ; 18(7): 4935-4939, 2018 Jul 01.
Artigo em Inglês | MEDLINE | ID: mdl-29442677

RESUMO

The nanosized Bi-doped SnO2/reduced graphene oxide 3D hybrids have been synthesized via one-step hydrothermal method. The structures, morphologies, photocatalytic activities of the as-prepared samples were discussed, respectively. The formation mechanism of the as-prepared hybrids was also proposed. Experimental results indicated that the usage amount of Bi2Sn2O7 obviously affected the photocatalytic performance of the as-prepared products. When it was 450 mg, the as-prepared sample possessed the band gap energy of 1.9 eV and the photocatalytic efficiency of 90% in 210 min for degradation of rhodamine B solution. In addition, triethylene tetramine and the as-prepared carbon hydrogel could act as reductant to synergistically reduce Bi2Sn2O7 into Bi-doped SnO2 particles during the formation of the hybrids.

3.
Artigo em Chinês | WPRIM (Pacífico Ocidental) | ID: wpr-356711

RESUMO

<p><b>OBJECTIVE</b>To elvaulate the antioxidant activity of the pigment of Lycium ruthenicum.</p><p><b>METHOD</b>The antioxidant activities were measured by the effects of the reducing ability, scavenging DPPH. H2O2-induced hemolysis of mice erythrocyte, serum resistance of reactive oxygen species, content of MDA in liver tissue, and swelling effect of mitochondria in liver tissue.</p><p><b>RESULT</b>The pigment of L. ruthenicum could scaveng DPPH* remarkably with IC50 0.164 mg x mL(-1), inhibitte hemolysis of mice erythrocyte evidently with IC50 0.112 mg x mL(-1). The resistant of reactive oxygen species was enhanced by the tested substances, simultanously. The concentration of MDA of peroxidation of lipid in mice liver could be reduced, and the swelling of mice liver mitochondria alse be restrained.</p><p><b>CONCLUSION</b>The pigment of L. ruthenicum has antioxidant activity in tested concentration.</p>


Assuntos
Animais , Camundongos , Antioxidantes , Farmacologia , Compostos de Bifenilo , Metabolismo , Eritrócitos , Sequestradores de Radicais Livres , Farmacologia , Hemólise , Hidrazinas , Metabolismo , Peroxidação de Lipídeos , Fígado , Metabolismo , Lycium , Química , Malondialdeído , Metabolismo , Mitocôndrias Hepáticas , Patologia , Dilatação Mitocondrial , Fenóis , Farmacologia , Picratos , Pigmentos Biológicos , Farmacologia , Plantas Medicinais , Química , Espécies Reativas de Oxigênio
4.
Artigo em Chinês | WPRIM (Pacífico Ocidental) | ID: wpr-351817

RESUMO

<p><b>OBJECTIVE</b>To determine the effects of saponins from Tribulus terrestris (STT) on small intestinal a-glucosidase and postprandial blood glucose levels in rats.</p><p><b>METHOD</b>The inhibitory effects of STT on a-glucosidase extracted from small intestines in rats were carried out in vitro. The blood glucose levels were measured after 60 min when sucrose (2 g x kg(-1)) or glucose (2 g x kg(-1)) was administered orally with STT (100 mg x kg(-1)). After treated with STT (100 mg x kg(-1)) for 14 d, the activities of a-glucosidase were determined daily, as well as the postprandial blood glucose levels after oraly administered sucrose (2 g x kg(-1)).</p><p><b>RESULT</b>STT at concentrations of 0.1, 1 and 10 mg x mL(-1) reduced significantly the activities of alpha-glucosidase with inhibitory rates of (20.83 +/- 1.66)%, (43.73 +/- 2.39)% and (52.62 +/- 2.69)%, respectively. In facts STT (100 mg x kg(-1)) considerably decreased the blood glucose levels which was 52.61% of that of the control in rats co-administered orally with sucrose (2 g x kg(-1)). However, it showed no such effect on the rats co-administered orally with glucose (2 g x kg(-1)). After orally administered of STT for 14 d, the activity of alpha-glucosidase was significantly reduced (P < 0.05) to (58.17 +/- 3.24)% of that those in control. Meanwhile, The rats were oral administered with sucrose, the increase of postprandial blood glucose levels were (69.50 +/- 4.28)% of that in control 60 min later ( P < 0.05).</p><p><b>CONCLUSION</b>It was through inhibiting the activity of a-glucosidase in small intestines that STT significantly retarded the increase in postprandial blood glucose levels in rats.</p>


Assuntos
Animais , Masculino , Ratos , Glicemia , Metabolismo , Medicamentos de Ervas Chinesas , Farmacologia , Intestino Delgado , Plantas Medicinais , Química , Período Pós-Prandial , Ratos Sprague-Dawley , Saponinas , Farmacologia , Tribulus , Química , alfa-Glucosidases , Metabolismo
5.
Artigo em Inglês | WPRIM (Pacífico Ocidental) | ID: wpr-305450

RESUMO

<p><b>OBJECTIVE</b>To investigate the stratification risk of catecholamines-beta-adrenoceptor (beta-AR)-cAMP pathway for cardiogenic death events in patients with congestive heart failure (CHF).</p><p><b>METHODS</b>A total of 83 identified CHF patients with a baseline and follow-up plasma levels of norepinephrine (NE) and epinephrine (E), lymphocytes beta-AR density (Bmax), and intralymphocyte cAMP content in peripheral blood were followed up. Major cardiogenic death events were registered.</p><p><b>RESULTS</b>The period between the initial entry and the last follow-up measurement were 51 +/- 16 months, the total duration of clinical follow-up after the last measurement were 14 +/- 8 months. During follow-up, 39 patients died of cardiogenic (sudden death 17 patients, worsening heart failure 22 patients). Persistence of high NE, E, and cAMP from baseline to follow-up were confirmed as risk predicting factors of cardiovascular events. Persistence NE above 4.0 nmol/L, E above 3.5 nmol/L, and the intralymphocyte cAMP content above 3.5 pmd x mg(-1) x pro(-1) from baseline to follow-up were significant adverse prognostic predictors. The major cardiogenic death events rates per 100 patients-years were 1.33 and 4.82 in patients with NE below and above 4.0 nmol/L (HR: 2.91; 95% CI: 1.08-7.33; P = 0.015); were 1.42 and 4.36 in the patients with E levels below and above 3.5 nmol/L (HR: 2.64; 95% CI: 1.02-6.41; P = 0.019); were 1.81 and 4.67 in the patients with the intralymphocyte cAMP content below and above 3.5 pmd x mg(-1) x pro(-1) (HR: 2.79; 95% CI: 1.04-6.83; P = 0.017), but difference was not significant between the beta-AR density below and above median.</p><p><b>CONCLUSIONS</b>Persistent increase in circulating catecholamines and intralymphocyte cAMP content may increase the long-term mortality in CHF patients.</p>


Assuntos
Idoso , Feminino , Humanos , Masculino , Pessoa de Meia-Idade , Catecolaminas , Sangue , AMP Cíclico , Sangue , Morte Súbita Cardíaca , Epinefrina , Sangue , Insuficiência Cardíaca , Sangue , Mortalidade , Linfócitos , Química , Norepinefrina , Sangue , Receptores Adrenérgicos beta , Sangue
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