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1.
Rev Sci Instrum ; 85(5): 054101, 2014 May.
Artigo em Inglês | MEDLINE | ID: mdl-24880386

RESUMO

A novel liquid injection vapor generator (LIVG) is demonstrated that is amenable to low vapor pressure explosives, 2,4,6-trinitrotoluene and hexahydro-1,3,5-trinitro-1,3,5-triazine. The LIVG operates in a continuous manner, providing a constant and stable vapor output over a period of days and whose concentration can be extended over as much as three orders of magnitude. In addition, a large test atmosphere chamber attached to the LIVG is described, which enables the generation of a stable test atmosphere with controllable humidity and temperature. The size of the chamber allows for the complete insertion of testing instruments or arrays of materials into a uniform test atmosphere, and various electrical feedthroughs, insertion ports, and sealed doors permit simple and effective access to the sample chamber and its vapor.

2.
Appl Opt ; 48(4): B126-36, 2009 Feb 01.
Artigo em Inglês | MEDLINE | ID: mdl-19183570

RESUMO

We describe the development and performance evaluation of a system for optical interrogation, subsequent selection, and collection of individual aerosol particles entrained in an inlet air stream. Elastic scatter and laser-induced fluorescence obtained from single particles on-the-fly provide compositional information for classification criteria. Individual particles could then be selectively electrically charged and captured to a conductive substrate with an electric potential. The optical subsystem also includes a novel two-beam velocimeter to provide accurate downstream timing. Good overall quantitative performance values are reported for particles in the size range of 1-8 microm at mean rates up to 4 kHz.


Assuntos
Aerossóis/análise , Aerossóis/química , Algoritmos , Monitoramento Ambiental/métodos , Análise de Injeção de Fluxo/métodos , Lasers , Espectrometria de Fluorescência/métodos , Tamanho da Partícula , Material Particulado/análise , Material Particulado/química , Reprodutibilidade dos Testes , Sensibilidade e Especificidade
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