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Analyst ; 119(9): 2101-4, 1994 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-7978333

RESUMO

A flow injection spectrophotometric method has been developed for the determination of aspartame in dietary products using ninhydrin as a colorimetric reagent. The reaction was conducted in a 1 + 1 v/v methanol-isopropanol medium also containing potassium hydroxide. The absorbance measurements were made at 603 nm. The results obtained for the determination of aspartame in table sweetener, pudding, gelatin, and refreshment (i.e., a powder dissolved in water for drinking) are in good agreement with the results obtained using a conventional manual procedure (correlation coefficient, r = 0.9984). Thirty-six results were obtained per hour, and the relative standard deviation was less than 3.5% (n = 6) for all samples. The detection limit (three times the signal blank/slope) was 3.8 x 10(-5) mol l-1 of aspartame.


Assuntos
Aspartame/análise , Análise de Injeção de Fluxo , Análise de Alimentos , Espectrofotometria
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