Effect of the thickness of CAD-CAM materials on the shear bond strength of light-polymerized resin cement.

This study aimed to investigate the effect of the thickness of computer aided design-computer aided manufacturing (CAD-CAM) restorative materials on the bond strength of light-polymerized resin cement. Ninety specimens were prepared from three different CAD-CAM materials (a leucite-based glass-ceramic [Empress CAD], a polymer-infiltrated ceramic network [Vita Enamic], and a zirconia-reinforced lithium silicate glass-ceramic [Vita Suprinity]) in different thicknesses (1, 2, and 3 mm). One surface of each specimen was treated by using a single-step self-etching ceramic primer (Monobond Etch & Prime). Light-polymerized resin cement was bonded to treated surfaces by exposure to a light-emitting diode curing unit from the untreated side of the samples. Shear bond strength (SBS) between the ceramic and the resin cement was measured by using a universal testing machine. The leucite-based glass-ceramic had higher SBS values than the other materials at each thickness. For each material, 1 mm-thick specimens had the highest SBS values. The difference between the SBS values of 2 mm- and 3 mm-thick polymer-infiltrated ceramic network was nonsignificant, whereas the SBS values of 2 mm-thick leucite-based glass-ceramic and the zirconia-reinforced lithium silicate glass-ceramic were significantly higher than those of the corresponding 3 mm-thick specimens. The choice of the material and its thickness may be highly important for clinical success when light-polymerized resin cements are used for cementation.

Combined application of femtosecond laser and air-abrasion protocols to monolithic zirconia at different sintering stages: Effects on surface roughness and resin bond strength.

This study aimed to investigate the effects of femtosecond laser (Fs) and/or air-abrasion protocols on surface roughness (Ra) of zirconia and resin bond strength. Eighty zirconia samples were randomly divided into eight subgroups according to surface treatment protocols: Control (C), Air-abrasion before sintering (ABS), Air-abrasion after sintering (AAS), Air-abrasion before and after sintering (ABS + AAS), Fs laser before sintering (FBS), Fs laser before sintering + air-abrasion after sintering (FBS + AAS), Fs laser after sintering (FAS), and Fs laser after sintering + air-abrasion after sintering (FAS + AAS). Measurements of Ra values were obtained using a surface profilometer. Surface morphological properties were evaluated with scanning electron microscopy (SEM), and crystallographic changes were examined by X-Ray diffractometry (XRD). Self-adhesive resin cement was bonded to zirconia samples, and shear bond strength (SBS) tests were performed. The data were statistically analyzed by one-way ANOVA, followed by Tamhane tests. The control group displayed the lowest Ra and SBS values among all groups. The highest Ra and SBS values were found in the FBS and FBS + AAS groups. Air-abrasion applied before sintering significantly increased the Ra of specimens. FAS, FAS + AAS, and ABS + AAS groups exhibited higher SBS values than AAS and ABS (p < .05). Air-abrasion applied after Fs laser did not produce any significant change in the Ra and SBS compared to Fs laser alone (p > .05). Femtosecond laser application may be a promising method to enhance the surface roughness of zirconia and improve resin bond strength. Air-abrasion at pre- and post-sintered stages may also be a viable surface treatment option.

Effect of airborne particle abrasion and sintering order on the surface roughness and shear bond strength between Y-TZP ceramic and resin cement.

This study examined the surface roughness (Ra) and shear bond strength (SBS) of Yttria-stabilized tetragonal zirconia polycrystalline (Y-TZP) ceramic after airborne particle abrasion at different pressures and particle sizes, pre- and post-sintering. Ninety specimens, prepared from Y-TZP ceramic blocks (Vita In-Ceram YZ, Vita Zahnfabrik), were divided into nine subgroups: control, and 50 and 110 µm Al2O3 airborne particle abrasion at 3 and 4 bar pressure, before and after sintering, respectively. According to the sintering order, before and after surface treatments, Ra values were measured using a profilometer. SBS to Y-TZP was assessed after thermocycling, using self-adhesive resin cement (Rely X U200, 3M ESPE). Scanning electron microscopy (SEM) and X-ray diffractometry (XRD) were performed on one specimen per group. All surface-treated samples were rougher than the controls. ABS50-4 (50 µm Al2O3 airborne particle abrasion at 4 bar pressure before sintering), ABS110-3, and ABS110-4 showed the highest Ra values, among all cohorts. The controls displayed lower SBS values than the treated groups (p<0.05), which had statistically similar results to each other. Airborne particle abrasion of pre-sintered Y-TZP, followed by sintering, increased the tetragonal structure contents.

Novel ceramic primer vs. conventional treatment methods: Effects on roughness and bond strength of all-ceramic restorations.

PURPOSE: To compare the influence of various surface treatments on the shear bond strength and surface roughness of lithium disilicate glass-ceramics. METHODS: 60 lithium disilicate ceramic samples were prepared according to the manufacturers' instructions and were divided into six groups according to the surface treatment:Control (C), 5% HF etching for 20 and 60 seconds (E20, E60), Monobond Etch & Prime etching (MEP), Nd:YAG (ND) and Er:YAG (ER) laser irradiation. All groups were treated with a universal primer except group MEP. A self-adhesive resin cement was bonded to all groups. The shear bond strengths of the specimens were measured using a universal testing machine while surface roughness was measured using a profilometer. RESULTS: Kruskal-Wallis and Mann-Whitney U tests revealed significant differences (P< 0.05). The shear bond strength of group E60 was higher than the other groups while surface roughness of groups MEP and ER were highest. CLINICAL SIGNIFICANCE: Monobond Etch & Prime might be a useful method in order to obtain adequate bond strength values.

Influence of the supporting die structures on the fracture strength of all-ceramic materials.

This study investigated the influence of the elastic modulus of supporting dies on the fracture strengths of all-ceramic materials used in dental crowns. Four different types of supporting die materials (dentin, epoxy resin, brass, and stainless steel) (24 per group) were prepared using a milling machine to simulate a mandibular molar all-ceramic core preparation. A total number of 96 zirconia cores were fabricated using a CAD/CAM system. The specimens were divided into two groups. In the first group, cores were cemented to substructures using a dual-cure resin cement. In the second group, cores were not cemented to the supporting dies. The specimens were loaded using a universal testing machine at a crosshead speed of 0.5 mm/min until fracture occurred. Data were statistically analyzed using two-way analysis of variance and Tukey HSD tests (α = 0.05). The geometric models of cores and supporting die materials were developed using finite element method to obtain the stress distribution of the forces. Cemented groups showed statistically higher fracture strength values than non-cemented groups. While ceramic cores on stainless steel dies showed the highest fracture strength values, ceramic cores on dentin dies showed the lowest fracture strength values among the groups. The elastic modulus of the supporting die structure is a significant factor in determining the fracture resistance of all-ceramic crowns. Using supporting die structures that have a low elastic modulus may be suitable for fracture strength tests, in order to accurately reflect clinical conditions.

Effect of dentin bonding and ferrule preparation on the fracture strength of crowned teeth restored with dowels and amalgam cores.

STATEMENT OF PROBLEM: It is necessary to obtain an adequate bond at the core/dentin junction where the majority of failures occur. The effect of recently developed dentin bonding agents on the fracture resistance of endodontically treated teeth at the amalgam core/dentin junction is unclear. PURPOSE: The purpose of this study was to evaluate the effects of 2 dentin bonding agents and a ferrule preparation on the fracture resistance of crowned mandibular premolars incorporating prefabricated dowel and silver amalgam cores. MATERIAL AND METHODS: Sixty extracted mandibular second premolars were divided into 6 groups of 10 each. The coronal portion of each tooth was removed at the cemento-enamel junction (CEJ) in the first 3 groups. In the other groups, teeth were sectioned 1 mm above the CEJ to create a ferrule. After root canal preparations, prefabricated dowels (ParaPost) were placed. The first group served as a control and was tested without application of bonding agents and without incorporation of a ferrule design. In the second and third groups, respectively, an autopolymerizing adhesive (Superbond D-Liner) and a dual-polymerizing adhesive (Panavia F) were applied to tooth surfaces before restorative procedures. For the fourth (ferrule) group, no bonding agent was applied, but a 1-mm ferrule preparation was used. In the fifth (ferrule+D-Liner) and sixth (ferrule+Panavia F) groups, respectively, autopolymerizing and dual-polymerizing bonding agents were used in conjunction with the ferrule preparation. After amalgam core fabrication, Ni-Cr full cast crowns for each group were prepared and cemented. All specimens were stored in water for 1 week and thermal cycled 1000 times between 5 degrees and 55 degrees C. A compressive shear load was applied at an angle of 135 degrees to the crown, and the maximum load at fracture (N) was recorded. The data were analyzed with 1-way ANOVA and Tukey Honestly Significant Difference tests (alpha=.05). RESULTS: Significantly higher fracture strength values were demonstrated for the ferrule+Panavia F (652.5 N), ferrule+D-liner (649.1 N) and ferrule (592.4 N) groups, respectively, than for the other groups. The next highest fracture strength values were found for the D-Liner (485.0 N) and Panavia F (486.3 N) groups. The control group (376.6 N) demonstrated the lowest fracture strength in all test groups (P<.001). CONCLUSION: A ferrule preparation or a bonding agent designed for silver amalgam core-dentin bonding can each increase the fracture strength for teeth receiving cast crowns after endodontic therapy and dowel and amalgam core restorations.