RESUMO
OBJECTIVES: This study evaluated the influence of 2% chlorhexidine digluconate (CHX) on the bond strength (BS) of a glass-fibre post to the root canal, regarding the cements (dual-cured resin or resin-modified glass-ionomer cement), the root thirds and the time of storage. METHOD: Eighty bovine roots were selected and endodontically treated, before being randomly assigned to the following groups according to the luting protocol: ARC (RelyX ARC); ARC+CHX; RL (RelyX Luting 2); and RL+CHX. After 24 h of luting, the roots were sliced to obtain 1 mm-thick slices. Half of each group was submitted to either 7-day or 6-month storage in artificial saliva (n=10). The specimens were subjected to push-out tests with a crosshead speed of 0.5 mm/min. The data were analysed with four-way ANOVA and Tukey's test (P≤0.05). The failure modes were analysed with a digital microscope (50× and 200×). RESULTS: ARC yielded a significantly higher BS compared to RL (P<0.001). Despite CHX exerted a significant effect; it depends on the interaction with the luting cement and time (P<0.001). Thus, CHX decreased the values of BS to those of ARC after 6 months (P<0.001). On the 7th day of storage, the ARC+CHX presented higher BS to the cervical and middle thirds compared to RL+CHX (P=0.012). Time solely was not a significant factor (P=0.081). Adhesive cement-dentine type and mixed failures were predominant modes for the ARC groups. For the RL groups, the main failures were adhesive cement-post and mixed modes. CONCLUSIONS: Glass-fibre posts luted with RelyX ARC dual-cure resin cement exhibited higher BS than those luted with RelyX Luting 2 resin-modified glass-ionomer cement. Furthermore, CHX was not effective to improve the BS and negatively affected the BS of RelyX ARC after 6 months of storage. CLINICAL SIGNIFICANCE: The use of chlorhexidine solution seems not to improve the bond strength of fibre posts to root canals, disregarding the composition of the luting cement.
Assuntos
Clorexidina/análogos & derivados , Colagem Dentária , Materiais Dentários/química , Cavidade Pulpar/ultraestrutura , Inibidores Enzimáticos/química , Cimentos de Ionômeros de Vidro/química , Vidro/química , Técnica para Retentor Intrarradicular/instrumentação , Cimentos de Resina/química , Animais , Bis-Fenol A-Glicidil Metacrilato/química , Bovinos , Clorexidina/química , Resinas Compostas/química , Dentina/ultraestrutura , Teste de Materiais , Polietilenoglicóis/química , Ácidos Polimetacrílicos/química , Distribuição Aleatória , Preparo de Canal Radicular/métodos , Saliva Artificial/química , Autocura de Resinas Dentárias , Estresse Mecânico , Propriedades de Superfície , Fatores de Tempo , Ápice Dentário/ultraestruturaRESUMO
PURPOSE: The aim of this study was to evaluate the effects of curing mode and viscosity on the biaxial flexural strength (FS) and modulus (FM) of dual resin cements. METHODS: Eight experimental groups were created (n=12) according to the dual-cured resin cements (Nexus 2/Kerr Corp. and Variolink II/IvoclarVivadent), curing modes (dual or self-cure), and viscosities (low and high). Forty-eight cement discs of each product (0.5 mm thick by 6.0 mm diameter) were fabricated. Half specimens were light - activated for 40 seconds and half were allowed to self-cure. After 10 days, the biaxial flexure test was performed using a universal testing machine (1.27 mm/min, Instron 5844). Data were statistically analyzed by three-way ANOVA and Tukey's test (5%). RESULTS: Light-activation increased FS and FM of resin cements at both viscosities in comparison with self-curing mode. The high viscosity version of light-activated resin cements exhibited higher FS than low viscosity versions. The viscosity of resin and the type of cement did not influence the FM. Light-activation of dual-polymerizing resin cements provided higher FS and FM for both resin cements and viscosities. CONCLUSION: The use of different resin cements with different viscosities may change the biomechanical behavior of these luting materials.
OBJETIVO: O objetivo do estudo é avaliar o efeito do modo de ativação na resistência flexual biaxial (RF) e módulo (MF) em cimentos resinosos duais. METODOLOGIA: Foram formados oito grupos experientais (n=12) de acordo com cimento resinos (Nexus 2/Kerr Corp. and Variolink II/IvoclarVivadent), modo de ativação (dual ou auto-polimerizado) e viscosidade (baixa e alta). Quarenta e oito discos de cada cimento foram fabridados (0,5 mm espessura por 6,0 mm diametro). Metade dos espécimes foram foto-ativados e a outra metade foi deixado para auto-polimerização. Após dez dias, o teste biaxial foi realizado em máquina de ensaio universal (1,27 mm/min, Instron 5844). Os dados foram analisados estatisticamente por ANOVA e teste Tukey (5%). RESULTADOS: A foto-ativação aumentou a RF e RM para os cimentos em ambas as viscosidades em comparação com os grupos auto-polimerizados. A versão alta viscosidade dos cimentos foto-ativados apresentou maior RF que os cimentos em baixa viscosidade. A viscosidade e o tipo de cimento não influenciam o MF. A foto-ativação aumenta os valores de RF e MF para ambos os cimentos e viscosidades. CONCLUSÃO: O uso de diferentes cimentos com diferentes viscosidades pode influenciar o comportamento biomecânico de cimentos resinoso.