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1.
Int J Biol Macromol ; : 134310, 2024 Jul 31.
Artigo em Inglês | MEDLINE | ID: mdl-39094863

RESUMO

In unmanned aircraft applications, electromagnetic wave (EMW) absorbers suffer from defects in narrow absorption bands and poor mechanical properties. To solve the problems, a lightweight multilayer stealth structure with wide broadband absorption performance and excellent mechanical properties was designed and prepared by adjusting microscopically the number of multi-walled carbon nanotubes (MWCNT) and modulating macroscopically the thickness-matching relationship of the structure to promote the absorption of EMW synergistically. Under the MWCNT of 30 wt% and the depletion layer with the thickness of 0.2 mm, the effective absorption bandwidth (EAB) covers the entire Ku-band while maintaining a minimum reflection loss (RL) of -15 dB. Besides, the radar cross-sectional area attenuation is as high as 23.1 dBm2, as well as the mechanical properties of the radar absorbing structures (RAS) were improved significantly due to the reducing structural density from balsa wood and the enhancement effect of glass fiber mats (GFM). The study constructed balsa-based RAS with excellent EMW absorbing and mechanical properties from both micro-nano scale and macro-structure, providing a research route for designing high-performance and lightweight stealth structures.

2.
Hua Xi Kou Qiang Yi Xue Za Zhi ; 42(4): 538-542, 2024 Aug 01.
Artigo em Inglês, Chinês | MEDLINE | ID: mdl-39049643

RESUMO

This study explores the potential application of computer aided design (CAD)/computer aided manufac-turing (CAM) for one-piece glass fiber posts and cores in restoring tooth defects post-removal of a broken fiber post using a digital guide plate. This paper reports a fractured left upper incisor fiber post removed using a customized needle and digital guide plate. Following root canal retreatment, CAD/CAM integrated fiber post-core and zirconia full crown restoration were completed. The occlusion testing was conducted using the T-Scan Ⅲ system. This study offers insights for managing secondary repair after fiber post fractures.


Assuntos
Vidro , Técnica para Retentor Intrarradicular , Humanos , Desenho Assistido por Computador , Incisivo/cirurgia , Zircônio , Coroas , Tratamento do Canal Radicular
3.
Sci Bull (Beijing) ; 2024 Jul 15.
Artigo em Inglês | MEDLINE | ID: mdl-39060214

RESUMO

Direct synthesis of graphene on nonmetallic substrates via chemical vapor deposition (CVD) has become a frontier research realm targeting transfer-free applications of CVD graphene. However, the stable mass production of graphene with a favorable growth rate and quality remains a grand challenge. Herein, graphene glass fiber fabric (GGFF) was successfully developed through the controllable growth of graphene on non-catalytic glass fiber fabric, employing a synergistic binary-precursor CVD strategy to alleviate the dilemma between growth rate and quality. The binary precursors consisted of acetylene and acetone, where acetylene with high decomposition efficiency fed rapid graphene growth while oxygen-containing acetone was adopted for improving the layer uniformity and quality. Notably, the bifurcating introducing-confluent premixing (BI-CP) system was self-built for the controllable introduction of gas and liquid precursors, enabling the stable production of GGFF. GGFF features solar absorption and infrared emission properties, based on which the self-adaptive dual-mode thermal management film was developed. This film can automatically switch between heating and cooling modes by spontaneously perceiving the temperature, achieving excellent thermal management performances with heating and cooling power of ∼501.2 and ∼108.6 W m-2, respectively. These findings unlock a new strategy for the large-scale batch production of graphene materials and inspire advanced possibilities for further applications.

4.
Polymers (Basel) ; 16(13)2024 Jul 05.
Artigo em Inglês | MEDLINE | ID: mdl-39000780

RESUMO

This paper presents experimental results from three-point bending tests for a composite made of quadriaxial glass fiber fabrics and an epoxy resin. Two composites were tested, one with 8 layers and the other with 16 layers; both had the same matrix (the epoxy resin). Tests were carried out, using five different test rates from 10 mm/min to 1000 mm/min. The following parameters were recorded and calculated: Young's modulus, flexural stress, flexural strain, energy, force, and all four for the first peak. The experimental data reveal no sensitivity for these materials based on the test rates, at least for the analyzed range; but, the characteristics for the thicker composite, with 16 layers of fabric, are slightly lower than those for the thinner composite, with 8 layers. The results pointed out that, for the same thickness of composite, certain characteristics, such as stress at the first peak, the flexural modulus, strain at the first peak, and energy at the first peak, are not sensitive to the test rate in the range 10-1000 mm/min. The energy at the first peak is double for the 16-layer composite compared to the 8-layer composite, but the specific energy (as energy on cross-sectional area) has close values: 103.47 kJ/m2 for the 8-layer composite and 106.51 kJ/m2 for the 16-layer composite. The results recommend this composite for applications in components with resistance to bending or for low-velocity impact protection.

5.
Artigo em Inglês | MEDLINE | ID: mdl-39071211

RESUMO

Background: Severe caries in early childhood is a concern for both children receiving dental treatment and their parents. This dental disease progresses rapidly and quickly damages the coronal part of the tooth. When there is insufficient coronal structure to support a coronal restoration, using intracanal components following root canal treatment increases tooth resistance and helps provide retention for the coronal restoration. This study compared the shear bond strength of three types of intracanal posts (composite resin post, reverse metal post, and fiber post) in severely damaged primary anterior teeth. Methods: This in vitro study was conducted on 30 extracted anterior primary teeth with at least two-thirds of healthy roots and no prior pulp treatment. The teeth were randomly divided into three groups of 10: group 1: composite resin post with 8th generation universal bonding, group 2: reverse metal post with GC restorative glass cement, and group 3: fiber post with GC restorative glass cement. After placing the post, the samples were restored with a height of 3 mm from cementoenamel junction (CEJ) using an Anterior GC Gradia Packable composite resin. All the samples underwent 500 cycles of thermocycling in a hot water bath at 55±2 °C and a cold water bath at 5±2 °C. The shear strength of the samples was then evaluated using an electromechanical universal testing machine at a rate of 1 mm/min and at a location 2 mm coronal to the CEJ in terms of megapascals. Results: The average shear bond strength of composite resin posts with 8th generation bonding application was 8.02220 MPa, reverse metal posts with glass ionomer application was 13.8600 MPa, and fiber posts with glass ionomer application was 9.7400 MPa. Conclusion: Based on these findings, it can be concluded that the highest shear bond strength in this study was related to the reverse metal post, and the lowest shear bond strength was related to the composite resin post. According to the results, reverse metal posts demonstrated better shear bond strength than composite resin posts and fiber posts (P<0.05).

6.
J Control Release ; 372: 648-660, 2024 Aug.
Artigo em Inglês | MEDLINE | ID: mdl-38936743

RESUMO

In vitro-In vivo correlation (IVIVC) is a main focus of the pharmaceutical industry, academia and the regulatory sectors, as this is an effective modelling tool to predict drug product in vivo performance based on in vitro release data and serve as a surrogate for bioequivalence studies, significantly reducing the need for clinical studies. Till now, IVIVCs have not been successfully developed for in situ forming implants due to the significantly different in vitro and in vivo drug release profiles that are typically achieved for these dosage forms. This is not unexpected considering the unique complexity of the drug release mechanisms of these products. Using risperidone in situ forming implants as a model, the current work focuses on: 1) identification of critical attributes of in vitro release testing methods that may contribute to differences in in vitro and in vivo drug release from in situ forming implants; and 2) optimization of the in vitro release method, with the aim of developing Level A IVIVCs for risperidone implants. Dissolution methods based on a novel Teflon shape controlling adapter along with a water non-dissolvable glass fiber membrane (GF/F) instead of a water dissolvable PVA film (named as GF/F-Teflon adapter and PVA-Teflon adapter, respectively), and an in-house fabricated Glass slide adapter were used to investigate the impact of: the surface-to-volume ratio, water uptake ratio, phase separation rate (measured by NMP release in 24 h post injection in vitro or in vivo), and mechanical pressure on the drug release patterns. The surface-to-volume ratio and water uptake were shown to be more critical in vitro release testing method attributes compared to the phase separation rate and mechanical pressure. The Glass slide adapter-based dissolution method, which allowed for the formation of depots with bio-mimicking surface-to-volume ratios and sufficient water uptake, has the ability to generate bio-relevant degradation profiles as well as in vitro release profiles for risperidone implants. For the first time, a Level A IVIVC (rabbit model) has been successfully developed for in situ forming implants. Release data for implant formulations with slightly different PLGA molecular weights (MWs) were used to develop the IVIVC. The predictability of the model passed external validation using the reference listed drug (RLD), Perseris®. IVIVC could not be developed when formulations with different PLGA molar ratios of lactic acid to glycolic acid (L/G) were included. The present work provides a comprehensive understanding of the impact of the testing method attributes on drug release from in situ forming implants, which is a valuable practice for level A IVIVC development.


Assuntos
Implantes de Medicamento , Liberação Controlada de Fármacos , Risperidona , Risperidona/administração & dosagem , Risperidona/farmacocinética , Risperidona/química , Antipsicóticos/administração & dosagem , Antipsicóticos/farmacocinética , Antipsicóticos/química , Animais , Solubilidade
7.
Polymers (Basel) ; 16(12)2024 Jun 13.
Artigo em Inglês | MEDLINE | ID: mdl-38932031

RESUMO

With the rapid development of electronic information technology, higher requirements have been put forward for the dielectric properties and load-bearing capacity of materials. In continuous glass fiber-reinforced thermoplastic composites, polypropylene matrix is a non-polar polymer with a very low dielectric constant and dielectric loss, but polypropylene is extremely flammable which greatly limits its application. Aiming at the better application of flame retardant-modified continuous glass fiber-reinforced polypropylene composites (FR/GF/PP) in the field of electronic communication, the effects of four different kinds of flame retardants (Decabromodiphenyl ethane (DBDPE), halogen-free one-component flame retardant (MONO), halogen-free compound flame retardant (MULTI), and intumescent flame retardant (IFR)) on the properties of FR/GF/PP were compared, including the mechanical properties, dielectric properties and flame-retardant properties. The results showed that among the FR/GF/PP, IFR has the highest performance in mechanical properties, MULTI has better performance in LOI, DBDPE and IFR have better performance in flame retardant rating, and DBDPE and IFR have lower dielectric properties. Finally, gray relational analysis is applied to propose an approach for selecting the optimal combination (flame retardant type and flame-retardant content) of comprehensive performance. In the application exemplified in this paper, the performance of IFR-3-modified GF/PP is optimized.

8.
J Clin Med ; 13(12)2024 Jun 14.
Artigo em Inglês | MEDLINE | ID: mdl-38930007

RESUMO

(1) Background: Cementation of glass fiber posts to root canals has been associated with various failures, especially debonding. This narrative review aims to present the contemporary concepts concerning the adhesive cementation of glass fiber post and to discuss the optimal management of these factors. (2) Methods: Electronic search was performed in MEDLINE/Pub Med and Google Scholar using selected keywords examining the parameters post length, surface treatment of glass fiber posts, post space preparation and dentin pretreatment, resin cement selection, adhesive systems and hybrid layer formation, and clinical techniques. (3) Results: The search led to the selection of 44 articles. Epoxy resin-based endodontic sealers are recommended and the use of temporary cement in the root canal should be avoided. The minimum length of a glass fiber post adhesively cemented to a root canal is 5 mm. Irrigating the root canals with chlorhexidine, MTAD, or EDTA (alone or in combination with NaOCl) after post space preparation seems to enhance the bond strength. Silane application on the surface of the post seems to be beneficial. Concerning resin cements and adhesive systems, the results were rather inconclusive. Finally, resin cement should be applied inside the root canal with an elongation tip and photoactivation should be delayed. (4) Conclusions: Contemporary concepts of adhesive cementation of glass fiber posts can indeed improve the bond between glass fiber posts, resin cement, and root canal dentin, however, evidence coming from long-term randomized prospective clinical trials is needed in order to obtain safer conclusions.

9.
Int J Biol Macromol ; 274(Pt 2): 133470, 2024 Aug.
Artigo em Inglês | MEDLINE | ID: mdl-38942401

RESUMO

Passive daytime radiative cooling (PDRC) technology offers a green and sustainable strategy for cooling, eliminating the need for external energy sources through its exceptional efficiency in heat radiation and sunlight reflection. Despite its benefits, the widespread usage of non-biodegradable PDRC materials has unfortunately caused environmental pollution and resource wastage. Furthermore, the effectiveness of outdoor PDRC materials can be significantly diminished by rainfall. In this work, a superhydrophobic composite aerogel composed of stereocomplex-type polylactide and ultra-fine glass fiber has been successfully developed through simple physical blending and freeze-drying, which exhibits low thermal conductivity (36.26 mW m-1 K-1) and superhydrophobicity (water contact angle up to 150°). Additionally, its high solar reflectance (91.68 %) and strong infrared emissivity (93.95 %) enable it to effectively lower surface temperatures during daytime, resulting in a cooling effect of approximately 3.8 °C below the ambient temperature during the midday heat of summer, with a cooling power of 68 W/m2. This aerogel offers an environmentally friendly and sustainable approach for the utilization of radiative refrigeration materials, paving the way for environmental protection and sustainable development.


Assuntos
Géis , Vidro , Interações Hidrofóbicas e Hidrofílicas , Poliésteres , Vidro/química , Poliésteres/química , Géis/química , Condutividade Térmica , Temperatura Baixa , Temperatura
10.
Polymers (Basel) ; 16(9)2024 Apr 29.
Artigo em Inglês | MEDLINE | ID: mdl-38732707

RESUMO

A cost-effective solution to the problems that the automotive industry is facing nowadays regarding regulations on emissions and fuel efficiency is to achieve weight reduction of automobile parts. Glass fiber-reinforced polymers are regularly used to manufacture various components, and some parts may also contain thermoplastic elastomers for toughness improvement. This work aimed to investigate the effect of styrene-(ethylene-co-butylene)-styrene triblock copolymer (E) and treated fly ash (C) on the morphological, thermal, and mechanical properties of long glass fiber (G)-reinforced polypropylene (PP). Results showed that the composites obtained through melt processing methods presented similar thermal stability and improved (nano)mechanical properties compared to 25-30 wt.% G-reinforced PP composites (PP-25G/PP-30G). Specifically, the impact strength and surface hardness were greatly improved. The addition of 20 wt.% E led to a 25-39% increase in impact strength and surface elasticity, while the addition of 6.5 wt.% C led to a 16% increase in surface hardness. The composite based on 25 wt.% G, 6.5 wt.% C, and 20 wt.% E presented the best-balanced properties (8-17% increase in impact strength, 38-41% increase in axial strain, and 35% increase in surface hardness) compared with PP-30G/PP-25G. Structural and morphological analysis confirmed the presence of a strong interaction between the components that make the composites. Based on these results, the PP-G-E-C composites could be presented as a viable material for automotive applications.

11.
Polymers (Basel) ; 16(9)2024 May 04.
Artigo em Inglês | MEDLINE | ID: mdl-38732757

RESUMO

This study aimed to evaluate the effect of direct restorations using unidirectional glass fiber orientations and a short-fiber-reinforced composite (SFRC) on the fracture resistance of endodontically treated premolars with mesio-occluso-distal cavities. Ninety double-rooted premolars were selected. Fifteen teeth were left intact/as a control group. The endodontic treatment and cavity preparations of seventy-five teeth were performed and divided into five experimental groups: Resin composite (RC), modified transfixed technique + RC, circumferential technique + RC, cavity floor technique + RC, and SFRC + RC. All teeth were fractured under oblique static loading at a 30° angle using a universal testing machine. The fracture patterns were observed and classified. Data were analyzed with one-way analysis of variance, Pearson chi-square, and Tukey HSD post hoc tests (p = 0.05). The highest fracture strength values were obtained in intact teeth (599.336 N), followed by modified transfixed + RC treated teeth (496.58 N), SFRC + RC treated teeth (469.62 N), RC (443.51 N), circumferential + RC treated teeth (442.835 N), and cavity floor + RC treated teeth (404.623 N) (p < 0.05). There was no significant difference between the RC and the circumferential technique + RC (p > 0.05). Unrepairable fractures were observed at low rates (20%) in the modified transfixed + RC and SFRC + RC teeth, and at higher rates in RC (73.3%), cavity floor + RC (60%), and circumferential + RC (80%) teeth. The application of an SFRC or the modified transfixed technique yielded an improved fracture strength and the fracture pattern of ETPs being restored with a universal injectable composite.

12.
Sensors (Basel) ; 24(9)2024 Apr 25.
Artigo em Inglês | MEDLINE | ID: mdl-38732853

RESUMO

The multimodal and dispersive character of ultrasonic guided waves (UGW) offers the potential for non-destructive evaluation of fiber-reinforced composite (FRC) materials. In this study, a methodology for in situ stiffness assessment of FRCs using UGWs is introduced. The proposed methodology involves a comparison between measured wave speeds of the fundamental symmetric and antisymmetric guided wave modes with a pre-established dataset of UGW speeds and translation of them to corresponding stiffness properties, i.e., ABD-components, in an inverse manner. The dispersion relations of guided waves have been calculated using the semi-analytical finite element method. First, the performance of the proposed methodology has been assessed numerically. It has been demonstrated that each of the independent ABD-components of the considered laminate can be approximated with an error lower than 10.4% compared to its actual value. The extensional and bending stiffness properties can be approximated within an average error of 3.6% and 9.0%, respectively. Secondly, the performance of the proposed methodology has been assessed experimentally. This experimental assessment has been performed on a glass fiber-reinforced composite plate and the results were compared to mechanical tensile and four-point bending tests on coupons cut from the plate. Larger differences between the estimated ABD-components according to UGW and mechanical testing were observed. These differences were partly attributed to the variation in material properties across the test plate and the averaging of properties over the measurement area.

13.
BMC Oral Health ; 24(1): 523, 2024 May 03.
Artigo em Inglês | MEDLINE | ID: mdl-38702708

RESUMO

BACKGROUND: The rising demand for improved aesthetics has driven the utilization of recently introduced aesthetic materials for creating custom post and core restorations. However, information regarding the fracture resistance of these materials remains unclear, which limits their practical use as custom post and core restorations in clinical applications. AIM OF THE STUDY: This study aimed to evaluate the fracture resistance of three non-metallic esthetic post and core restorations and their modes of failure. MATERIALS AND METHODS: Thirty-nine single-rooted human maxillary central incisors were endodontically treated. A standardized post space preparation of 9mm length was performed to all teeth to receive custom-made post and core restorations. The prepared teeth were randomly allocated to receive a post and core restoration made of one of the following materials (n=13): glass fiber-reinforced composite (FRC), polyetheretherketone (PEEK) and polymer-infiltrated ceramic-network (PICN). An intraoral scanner was used to scan all teeth including the post spaces. Computer-aided design and computer-aided manufacturing (CAD-CAM) was used to fabricate post and core restorations. Post and core restorations were cemented using self-adhesive resin cement. All specimens were subjected to fracture resistance testing using a universal testing machine. Failure mode analysis was assessed using a stereomicroscope and SEM. The data was statistically analyzed using One-Way ANOVA test followed by multiple pairwise comparisons using Bonferroni adjusted significance level. RESULTS: Custom PEEK post and core restorations displayed the least fracture load values at 286.16 ± 67.09 N. In contrast, FRC exhibited the highest average fracture load at 452.60 ± 105.90 N, closely followed by PICN at 426.76 ± 77.99 N. In terms of failure modes, 46.2% of specimens with PICN were deemed non-restorable, while for PEEK and FRC, these percentages were 58.8% and 61.5%, respectively. CONCLUSIONS: Within the limitation of this study, both FRC and PICN demonstrated good performance regarding fracture resistance, surpassing that of PEEK.


Assuntos
Resinas Compostas , Desenho Assistido por Computador , Falha de Restauração Dentária , Estética Dentária , Técnica para Retentor Intrarradicular , Humanos , Cerâmica , Análise do Estresse Dentário , Benzofenonas , Incisivo/lesões , Materiais Dentários/química , Polietilenoglicóis , Cetonas/química , Polímeros , Vidro , Teste de Materiais , Planejamento de Prótese Dentária
14.
Adv Mater ; 36(24): e2313752, 2024 Jun.
Artigo em Inglês | MEDLINE | ID: mdl-38576272

RESUMO

Conventional conductive materials such as metals are crucial functional components of conductive systems in diverse electronic instruments. However, their severe intrinsic impedance mismatch with air dielectric causes strong reflection of incident electromagnetic waves, and the resulting low electromagnetic transmissivity typically interferes with surrounding electromagnetic signal communications in modern multifunction-integrated instruments. Herein, graphene glass fiber fabric (GGFF) that merges intrinsic electrical and electromagnetic properties of graphene with dielectric attributes and highly porous macrostructure of glass fiber fabric (GFF) is innovatively developed. Using a novel decoupling chemical vapor deposition growth strategy, high-quality and layer-limited graphene is prepared on noncatalytic nonmetallic GFF in a controlled manner; this is pivotal to realizing GGFF with the desired compatibility among high conductivity, low electromagnetic reflectivity, and high electromagnetic transmissivity. At the same sheet resistance over a wide range of values (250-3000 Ω·sq-1), the GGFF exhibits significantly lower electromagnetic reflectivity (by 0.42-0.51) and higher transmissivity (by 0.27-0.62) than those of its metal-based conductive counterpart (CuGFF). The material design strategy reported herein provides a constructive solution to eliminate the incompatibility between electrical conductivity and electromagnetic transmissivity faced by conventional conductive materials, spotlighting the applicability of GGFF in electric heating scenarios in radar, antenna, and stealth systems.

15.
Photodiagnosis Photodyn Ther ; 47: 104076, 2024 Jun.
Artigo em Inglês | MEDLINE | ID: mdl-38582390

RESUMO

AIMS: Impact of different post-space disinfectants (Saline, Sodium hypochlorite (NaOCl) followed by ethylene-diamine-tetra-acetic acid (EDTA) and curcumin activated by microbubble emulsion (MBE) on the Vickers hardness (VH) of root canal dentin and extrusion bond strength (EBS) of Glass fiber post (GFP) and PEEK post. METHODS: Ninety maxillary central incisors having fully formed roots were included. After the specimen's disinfection, root canal treatment was completed. Post space was prepared by removing gutta-percha using gates glidden drills. Teeth were then arbitrarily allocated into three groups based on the methods of disinfection regime used. Group 1: Saline, Group 2: NaOCl+ EDTA and Group 3: Curcumin activated by MBE (n = 30). Analysis of VH of radicular dentin was performed using a micro-Vickers tester on ten samples from each group. After post-space disinfection, twenty specimens from each group were further divided into two subgroups (n = 10) In group-1A 2A, and 3A, GFP was used. Whereas, prefabricated PEEK posts were used in 1B, 2B, and 3B subgroups. The PBS and failure modes were performed using a universal testing machine and stereomicroscope respectively. Data was analyzed using ANOVA and Tukey post hoc test to identify significant variations among groups concerning the MH and EBS of the different posts used (p = 0.05). RESULTS: Group 2 (5.25 % NaOCl + 17 % EDTA) (0.15 ± 0.02 GPa) treated specimens presented lowest scores of VH. However, Group 1 (Saline) irrigated canals displayed the highest scores of surface hardness (0.25 ± 0.07 GPa). Additionally, a cervical third of 3A (CP activated by MBE + GFP) (11.22 ± 0.79 MPa) presented the highest scores of bond integrity. Whereas Group 1B (Saline + PEEK post) treated specimens presented the lowest scores of PBS (4.15 ± 0.15 MPa). CONCLUSION: Curcumin activated by microbubble emulsion for disinfection of canal dentin demonstrated favorable VH. Similarly, glass fiber post-cemented in radicular walls disinfected with curcumin activated with MBE showed promising post-bond integrity to the canal dentin.


Assuntos
Benzofenonas , Curcumina , Ácido Edético , Vidro , Polietilenoglicóis , Polímeros , Hipoclorito de Sódio , Humanos , Polietilenoglicóis/química , Ácido Edético/farmacologia , Polímeros/química , Curcumina/farmacologia , Hipoclorito de Sódio/farmacologia , Fármacos Fotossensibilizantes/farmacologia , Técnica para Retentor Intrarradicular , Emulsões , Dureza , Teste de Materiais , Colagem Dentária/métodos , Desinfecção/métodos
16.
Clin Cosmet Investig Dent ; 16: 75-89, 2024.
Artigo em Inglês | MEDLINE | ID: mdl-38632981

RESUMO

Introduction: Endodontically treated teeth (ETT) undergo extensive structure change and experience high stress during biomechanical function. Stress distribution is influenced by the restoration material and the type of bond between material and tooth structure. The selection of materials that can distribute stress will affect the resistance and retention of ETT to mastication forces, thus biomechanical functions were achieved. Composite has mechanical properties similar to dentin, it can transmit and distribute stresses throughout the tooth surface. The disadvantage of composites in large cavities is their lack of toughness. The addition of fiber to composites can increase their toughness. Purpose: This research is to determine the stress distribution of a fiber-reinforced composite made of polyethylene and e-glass on the mesiolingual cavity of ETT. Materials and Methods: A three-dimensional model of the mandibular molar was prepared for cavity preparation and the formation of restorations using SolidWorks 2021. The models were analyzed with Abaqus 2020 to determine stress concentrations after given vertical and oblique loading. Results: The maximum and minimum principal stress data were obtained to assess material resistance and interfacial damage criterion. Polyethylene fiber shows a more homogeneous stress distribution because the modulus of elasticity is close to the dentin and has a thickness that can reduce the volume of the composite. The E-glass shows the stress concentration on the circumferential fiber and cavity floor. Conclusion: The stress distribution of fiber-reinforced composite on the buccolingual cavity of ETT using the finite element method did not show structural failure in the polyethylene group because the maximum and minimum principal stresses were lower than the strength of the material. Interfacial bond failure occurs at the enamel portion. The maximum and minimum principal values of e-glass indicate structural failure in the circumferential fiber and the base fiber because the stress exceeds the strength of the material. Interfacial bond failure occurred on the circumferential and the cavity floor.

17.
Materials (Basel) ; 17(7)2024 Mar 22.
Artigo em Inglês | MEDLINE | ID: mdl-38611967

RESUMO

In this paper, the glass-fiber-fabric-reinforced resin-based absorbing composites were prepared, and their microwave-absorbing properties were studied via simulation and experiment. The simulation results show that the absorption bandwidth of the absorbing material can cover the X\C\S band, respectively, at different thicknesses. The minimum reflection loss (RL) of the composite with a thickness of 2.2 mm is -27.4 dB at 5.95 GHz. However, the experiment results are quite different from those of the simulation. The metallographic results indicate that it is the change of the mass fraction of the absorbents in the composites after curing that causes the difference. According to the metallographic results, three shape approximation methods were proposed to calculate the real mass ratio of the absorbents in the composites, namely, parallelogram approximation, bows approximation, and elliptical approximation. Meanwhile, the structural parameter Kf was introduced to optimize the calculation results. The electromagnetic parameters of the material based on the calculation results were measured, and the results show that the simulation results obtained via bow approximation have a better coincidence to the experiment results, and the mass ratio of the absorbent raises by around 9.95%, which lays a foundation for the subsequent design of microwave-absorbing composites.

18.
Heliyon ; 10(8): e28388, 2024 Apr 30.
Artigo em Inglês | MEDLINE | ID: mdl-38638992

RESUMO

Carbon nanotube (CNT) reinforcement can lead to a new way to enhance the properties of composites by transforming the reinforcement phases into nanoscale fillers. In this study, the buckling response of functionally graded CNT-reinforced composite (FG-CNTRC) sandwich beams was investigated experimentally and analytically. The top and bottom plates of the sandwich beams were composed of carbon fiber laminated composite layers and hard core. The hard core was made of a pultruded glass fiber-reinforced polymer (GFRP) profile. The layers of FG-CNTRC surfaces were reinforced with different proportions of CNT. The reference sample was made of only a pultruded GFRP profile. In the study, the reference sample and four samples with CNT were tested under compression. The largest buckling load difference between the reference sample and the sample with CNT was 37.7%. The difference between the analytical calculation results and experimental results was obtained with an approximation of 0.49%-4.92%. Finally, the buckling, debonding, interlaminar cracks, and fiber breakage were observed in the samples.

19.
Materials (Basel) ; 17(5)2024 Feb 26.
Artigo em Inglês | MEDLINE | ID: mdl-38473538

RESUMO

To address the issues of insufficient strength and poor precision in polystyrene forming parts during the selective laser sintering process, a ternary composite of polystyrene/glass fiber/hollow glass microbeads was prepared through co-modification by incorporating glass fiber and hollow glass microbeads into polystyrene using a mechanical mixing method. The bending strength and dimensional accuracy of the sintered composites were investigated by conducting an orthogonal test and analysis of variance to study the effects of laser power, scanning speed, scanning spacing, and delamination thickness. The process parameters were optimized and selected to determine the optimal combination. The results demonstrated that when considering bending strength and Z-dimensional accuracy as evaluation criteria for terpolymer sintered parts, the optimum process parameters are as follows: laser power of 24 W, scanning speed of 1600 mm/s, scanning spacing of 0.24 mm, and delamination thickness of 0.22 mm. Under these optimal process parameters, the bending strength of sintered parts reaches 6.12 MPa with a relative error in the Z-dimension of only 0.87%. The bending strength of pure polystyrene sintered parts is enhanced by 15.69% under the same conditions, while the relative error in the Z-dimension is reduced by 63.45%. It improves the forming strength and precision of polystyrene in the selective laser sintering process and achieves the effect of enhancement and modification, which provides a reference and a new direction for exploring polystyrene-based high-performance composites and expands the application scope of selective laser sintering technology.

20.
Materials (Basel) ; 17(6)2024 Mar 19.
Artigo em Inglês | MEDLINE | ID: mdl-38541561

RESUMO

The purpose of this study is to use acoustic emission (AE) technology to explore the changes in the interface and mechanical properties of GF/VER composite materials after being treated with NaOH and to analyze the optimal modification conditions and damage propagation process. The results showed that the GF surface became rougher, and the number of reactive groups increased after treating the GF with a NaOH solution. This treatment enhanced the interfacial adhesion between the GF and VER, which increased the interfacial shear strength by 25.31% for monofilament draw specimens and 27.48% for fiber bundle draw specimens compared to those before the GF was modified. When the modification conditions were a NaOH solution concentration of 2 mol/L and a treatment time of 48 h, the flexural strength of the GF/VER composites reached a peak value of 346.72 MPa, which was enhanced by 20.96% compared with before the GF was modified. The process of damage fracture can be classified into six types: matrix cracking, interface debonding, fiber pullout, fiber relaxation, matrix delamination, and fiber breakage, and the frequency ranges of these failure mechanisms are 0~100 kHz, 100~250 kHz, 250~380 kHz, 380~450 kHz, 450~600 kHz, and 600 kHz and above, respectively. This paper elucidates the fracture process of GF/VER composites in three-point bending. It establishes the relationship between the AE signal and the interfacial and force properties of GF/VER composites, realizing the classification of the damage process and characterizing the mechanism. The frequency ranges of damage types and failure mechanisms found in this study offer important guidance for the design and improvement of composite materials. These results are of great significance for enhancing the interfacial properties of composites, assessing the damage and fracture behaviors, and implementing health monitoring.

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