Development of a dual point humidity sensor using POF based on twisted fiber structure.

The humidity has often been measured through a single point sensor. Where, the humidity could be varied at different locations as well as depending on environmental conditions. The present paper developed the dual point humidity measuring sensor by using a polymer optical fiber (POF) based on a single illuminating fiber. The sensor's basic structure is to twist two fibers and bend them at a certain radius. However, the dual point sensor is developed through the cascading of twisted micro bend (TMB-1 and TMB-2). The twisting of fibers couples the light from one fiber to another fiber through the side coupling method. An increase in the humidity level leads to a change in the reflective index, which helps to get variation in coupled light intensity. To measure the humidity, the dual point sensors are placed into the control humidity chamber at two random positions. The power reading variation is significantly linear when the humidity level increases from 30 to 80%. The sensor has a fast response of about 1 s and a recovery time of about 4 s. Furthermore, the chemical coating is applied to improve the sensor's sensitivity. Between 30 and 80% range of humidity, the both sensors of dual point TMB-1 and TMB-2 have appropriate sensitivity and detection limits, which is about 680.8 nW/% and 763.9 nW/% and 1.37% and 1.98%, respectively. To measure the humidity at variable positions, the present dual points humidity sensor is well-stable, easy, and straightforward, which uses a less expensive method.

Soft Polymer Optical Fiber Sensors for Intelligent Recognition of Elastomer Deformations and Wearable Applications.

In recent years, soft robotic sensors have rapidly advanced to endow robots with the ability to interact with the external environment. Here, we propose a polymer optical fiber (POF) sensor with sensitive and stable detection performance for strain, bending, twisting, and pressing. Thus, we can map the real-time output light intensity of POF sensors to the spatial morphology of the elastomer. By leveraging the intrinsic correlations of neighboring sensors and machine learning algorithms, we realize the spatially resolved detection of the pressing and multi-dimensional deformation of elastomers. Specifically, the developed intelligent sensing system can effectively recognize the two-dimensional indentation position with a prediction accuracy as large as ~99.17%. The average prediction accuracy of combined strain and twist is ~98.4% using the random forest algorithm. In addition, we demonstrate an integrated intelligent glove for the recognition of hand gestures with a high recognition accuracy of 99.38%. Our work holds promise for applications in soft robots for interactive tasks in complex environments, providing robots with multidimensional proprioceptive perception. And it also can be applied in smart wearable sensing, human prosthetics, and human-machine interaction interfaces.

Influence of Annealing on Polymer Optical Fiber Bragg Grating Inscription, Stability and Sensing: A Review.

This article reviews recent research progress on the annealing effects on polymer optical fibers (POFs), which are of great importance for inscription, stability and sensing applications of fiber Bragg gratings (FBGs) in POFs due to their unique properties related to polymer molecular chains. In this review, the principle of annealing to reduce frozen-in stress in POFs drawing and different annealing timings are firstly summarized. Then, the annealing methods for POFs are introduced under several different conditions (temperature, humidity, strain, stress and solution). Afterwards, the principle of FBGs and several inscription techniques are reported. Subsequently, the annealing effects on the properties of POFs and polymer optical fiber Bragg gratings (POFBGs) quality are discussed. Finally, the influence of annealing on POFBG sensitivity is summarized. Overall, this paper provides a comprehensive overview of annealing techniques and their impact on both POFs and POFBGs. We hope that it will highlight the important progress made in this field.

Structural Health Monitoring of Adhesively Bonded Pipe-to-Socket Joints by Integration of Polymer Optical Fibers and Their Load-Dependent Transmission Properties.

Adhesively bonded pipe-to-socket joints are used in numerous industrial applications. One example is in the transport of media, e.g., in the gas industry or in structural joints for such sectors as construction, wind energy, and the vehicle industry. To monitor such load-transmitting bonded joints, this study investigates a method based on the integration of polymer optical fibers into the adhesive layer. Previous methods for monitoring the condition of pipes, such as acoustic or ultrasonic methods or the use of glass fiber optic-based sensors (FBG or OTDR), are very complex in methodology and require cost-intensive (opto-) electronic devices to generate and evaluate the sensor signals; they are therefore unsuitable for large-scale use. The method investigated in this paper is based on the measurement of integral optical transmission with a simple photodiode under increasing mechanical stress. When tried at coupon level (single-lap joint), the light coupling was varied to obtain a significant load-dependent sensor signal. Based on an angle-selective coupling of 30° to the fiber axis, a drop of 4% of the optically transmitted light power by a load of 8 N/mm2 can be detected for the adhesively bonded pipe-to-socket joint with the structural adhesive Scotch Weld DP810 (2C acrylate).

Optical fiber sensors for posture monitoring, ulcer detection and control in a wheelchair: a state-of-the-art.

BACKGROUND: In the last ten years, the design and implementation of Optical Fiber Sensors (OFS) in biomedical applications have been discussed, with a focus on different subareas, such as body parameter monitoring and control of assistive devices. MATERIALS AND METHODS: A scoping review was performed including scientific literature (PubMed/Scopus, IEEE and Web of Science), patents (WIPO/Google Scholar), and commercial information. RESULTS: The main applications of OFS in the rehabilitation field for preventing future postural diseases and applying them in device controllers were discussed in this review. Physical characteristics of OFS, different uses, and applications of Polymer Optical Fiber pressure sensors are mentioned. The main postures used for posture monitoring analysis when the user is sitting are normal position, crooked back, high lumbar pressure, sitting on the edge of the chair, and crooked back, left position, and right position. Additionally, it is possible to use Machine Learning (ML) algorithms for posture classification, and device control such as Support Vector Machine, k-Nearest Neighbors, etc., obtaining accuracies above 97%. Moreover, the literature mentions wheelchair controllers and Graphical User Interfaces using pressure maps to provide feedback to the user. CONCLUSIONS: OFS have been used in several healthcare applications as well as postural and preventive applications. The literature showed an effort to implement and design accessible devices for people with disabilities and people with specific diseases. Alternatively, ML algorithms are widely used in this direction, leaving the door open for further studies that allow the application of real-time systems for posture monitoring and wheelchairs control.

IMPLICATIONS FOR REHABILITATIONPosture monitoring and ulcer detection systems are very useful to prevent or treat diseases related to bedsores or pressure ulcers using a different kind of electronic or optic instrumentation to improve the user's quality of life.The system characteristics using optical fiber sensors discussed in this review set an important precedent in the fabrication of low-cost systems for biomedical applications.

Incipient Biofouling Detection via Fiber Optical Sensing and Image Analysis in Reverse Osmosis Processes.

Reverse osmosis (RO) is a widely used membrane technology for producing process water or tap water that is receiving increased attention due to water scarcity caused by climate change. A significant challenge in any membrane filtration is the presence of deposits on the membrane surfaces, which negatively affect filtration performance. Biofouling, the formation of biological deposits, poses a significant challenge in RO processes. Early detection and removal of biofouling are essential for effective sanitation and prevention of biological growth in RO-spiral wound modules. This study introduces two methods for the early detection of biofouling, capable of identifying initial stages of biological growth and biofouling in the spacer-filled feed channel. One method utilizes polymer optical fibre sensors that can be easily integrated into standard spiral wound modules. Additionally, image analysis was used to monitor and analyze biofouling in laboratory experiments, providing a complementary approach. To validate the effectiveness of the developed sensing approaches, accelerated biofouling experiments were conducted using a membrane flat module, and the results were compared with common online and offline detection methods. The reported approaches enable the detection of biofouling before known online parameters become indicative, effectively providing an online detection with sensitivities otherwise only achieved through offline characterization methods.

Power Flow in Multimode Graded-Index Microstructured Polymer Optical Fibers.

We investigate mode coupling in a multimode graded-index microstructured polymer optical fiber (GI mPOF) with a solid core by solving the time-independent power flow equation (TI PFE). Using launch beams with various radial offsets, it is possible to calculate for such an optical fiber the transients of the modal power distribution, the length Lc at which an equilibrium mode distribution (EMD) is reached, and the length zs for establishing a steady-state distribution (SSD). In contrast to the conventional GI POF, the GI mPOF explored in this study achieves the EMD at a shorter length Lc. The earlier shift to the phase of slower bandwidth decrease would result from the shorter Lc. These results are helpful for the implementation of multimode GI mPOFs as a part of communications and optical fiber sensory systems.

Three-Dimensional-Printed Fabrication of POFs Using Different Filaments and Their Characterization for Sensing Applications.

This paper presents the development and sensor applications of 3D-printed polymer optical fibers (POFs) using commercially available filaments. The well-known intensity variation sensor was developed using this fiber for temperature and curvature sensing, where the results indicate a linear response in the curvature analysis, with a coefficient of determination (R2) of 0.97 and sensitivity of 4.407 × 10-4 mW/∘, whereas the temperature response was fitted to an R2 of 0.956 with a sensitivity of 5.718 × 10-3 mW/∘C. Then, the POF was used in the development of a modal interferometer by splicing the POF in-between two single-mode fibers (SMFs), which result in a single-mode-multimode-single-mode (SMS) configuration. The such interferometer was tested for temperature and axial strain responses, where the temperature response presented a linear trend R2 of around 0.98 with a sensitivity of -78.8 pm/∘C. The negative value of the sensitivity is related to the negative thermo-optic coefficient commonly obtained in POFs. Furthermore, the strain response of the SMS interferometer showed a high sensitivity (9.5 pm/µÏµ) with a quadratic behavior in which the R2 of around 0.99 was obtained. Therefore, the proposed approach is a low-cost, environmentally friendly and straightforward method for the production of highly sensitive optical fiber sensors.

A D-Shaped Polymer Optical Fiber Surface Plasmon Resonance Biosensor for Breast Cancer Detection Applications.

Fiber-optic biosensors have garnered significant attention and witnessed rapid development in recent years owing to their remarkable attributes such as high sensitivity, immunity to electromagnetic interference, and real-time monitoring. They have emerged as a potential tool in the realm of biomarker detection for low-concentration and small molecules. In this paper, a portable and cost-effective optical fiber biosensor based on surface plasmon resonance for the early detection of breast cancer is demonstrated. By utilizing the aptamer human epidermal growth factor receptor 2 (HER2) as a specific biomarker for breast cancer, the presence of the HER2 protein can be detected through an antigen-antibody binding technique. The detection method was accomplished by modifying a layer of HER2 aptamer on the flat surface of a gold-coated D-shaped polymer optical fiber (core/cladding diameter 120/490 µm), of which the residual thickness after side-polishing was about 245 µm, the thickness of the coated gold layer was 50 nm, and the initial wavelength in pure water was around 1200 nm. For low-concentration detection of the HER2 protein, the device exhibited a wavelength shift of ~1.37 nm with a concentration of 1 µg/mL (e.g., 5.5 nM), which corresponded to a limit of detection of ~5.28 nM. Notably, the response time of the biosensor was measured to be as fast as 5 s. The proposed biosensor exhibits the potential for early detection of HER2 protein in initial cancer serum and offers a pathway to early prevention of breast cancer.

Effects of Nanoscale Morphology on Optical Properties of Photoluminescent Polymer Optical Fibers.

Bicomponent photoluminescent polymer optical fibers (PL-POFs) have been melt-spun and in-situ drawn to different extents. The results suggest that scattering in the sheath can effectively increase the photoluminescent dye excitation probability in the fiber core. The core/sheath PL-POFs are made of a semi-crystalline fluoropolymer sheath of low refractive index (RI) and an amorphous cycloolefin polymeric core of high RI, which is doped with a luminescent dye. The axial light emission, as well as the guiding attenuation coefficients of the core/sheath PL-POFs, have been measured using a side-illumination set-up. The incident blue laser is down-converted to red light, which is re-emitted and partially guided by the core. The axial light emission is measured at the fiber tip as a function of the distance from the illumination position to the integrating sphere. It is demonstrated that the presence of a semi-crystalline sheath significantly enhances the axial light emission and that it also lowers the attenuation coefficient, compared to the emission and guiding properties of PL core-only fibers. Additionally, the attenuation coefficient has been found to be lower in more strongly drawn PL-POFs. Wide-angle X-ray diffraction and small-angle X-ray scattering experiments reveal structural differences in differently drawn PL-POFs that can be linked to the observed differences in the optical properties.

Properties of Fiber Bragg Grating in CYTOP Fiber Response to Temperature, Humidity, and Strain Using Factorial Design.

The characteristics of fiber Bragg grating (FBG) in cyclic transparent fluoropolymer (CYTOP) optical fiber have attracted more and more attention in recent years. However, different results of the FBG response to environmental parameters are reported. This work presents a three-variable two-level factorial experimental method to investigate the FBG response to temperature, humidity, and strain in CYTOP fiber. Two uniform FBGs are inscribed separately in CYTOP fiber with and without over-clad. With only eight measuring points, the interactions among three variable parameters are computed and the parameter sensitivities and cross-sensitivities are estimated. Similar temperature and strain sensitivities were found for both gratings, whereas significant cross-sensitivity between humidity and temperature was present only in FBG inscribed in CYTOP fiber with over-clad.

Treatment of Mode Coupling in Step-Index Multimode Microstructured Polymer Optical Fibers by the Langevin Equation.

By solving the Langevin equation, mode coupling in a multimode step-index microstructured polymer optical fibers (SI mPOF) with a solid core was investigated. The numerical integration of the Langevin equation was based on the computer-simulated Langevin force. The numerical solution of the Langevin equation corresponded to the previously reported theoretical data. We demonstrated that by solving the Langevin equation (stochastic differential equation), one can successfully treat a mode coupling in multimode SI mPOF as a stochastic process, since it is caused by its intrinsic random perturbations. Thus, the Langevin equation allowed for a stochastic mathematical description of mode coupling in SI mPOF. Regarding the efficiency and execution speed, the Langevin equation was more favorable than the power flow equation. Such knowledge is useful for the use of multimode SI mPOFs for potential sensing and communication applications.

Low-Cost 3D Printer Drawn Optical Microfibers for Smartphone Colorimetric Detection.

A fused deposition modeling (FDM) 3D printer extruder was utilized as a micro-furnace draw tower for the direct fabrication of low-cost optical fibers. An air-clad multimode microfiber was drawn from optically transparent polyethylene terephthalate glycol (PETG) filament. A custom-made spooling collection allows for an automatic variation of fiber diameter between ϕ ∼ 72 to 397 µm by tuning the drawing speed. Microstructure imaging as well as the 3D beam profiling of the transmitted beam in the orthogonal axes was used to show good quality, functioning microfiber fabrication with uniform diameter and identical beam profiles for orthogonal axes. The drawn microfiber was used to demonstrate budget smartphone colorimetric-based absorption measurement to detect the degree of adulteration of olive oils with soybean oil.

Recent Achievements on Grating Fabrications in Polymer Optical Fibers with Photosensitive Dopants: A Review.

This review discusses recent achievements on grating fabrications in polymer optical fibers doped with photosensitive materials. First, different photosensitive dopants in polymer optical fibers (POFs) are summarized, and their refractive index change mechanisms are discussed. Then, several different doping methods to fabricate the photosensitive POFs are presented. Following that, the principles of gratings, including standard fiber Bragg gratings (FBGs), tilted fiber Bragg gratings (TFBGs), chirped fiber Bragg gratings (CFBGs), phase-shifted fiber Bragg gratings (PSFBGs), and long period fiber gratings (LPFGs), are reported. Finally, fabrications of different gratings based on photosensitive POFs in the last 20 years are reported. We present our article clearly and logically, so that it will be helpful for researchers to explore a broad perspective on this proposed topic. Overall, the content provides a comprehensive overview of photosensitive POF fabrications and grating inscriptions in photosensitive POFs, including previous breakthroughs and recent advancements.

Interrogation Method with Temperature Compensation Using Ultra-Short Fiber Bragg Gratings in Silica and Polymer Optical Fibers as Edge Filters.

The use of simpler and less bulky equipment, with a reliable performance and at relative low cost is increasingly important when assembling sensing configurations for a wide variety of applications. Based on this concept, this paper proposes a simple, efficient and relative low-cost fiber Bragg grating (FBG) interrogation solution using ultra-short FBGs (USFBGs) as edge filters. USFBGs with different lengths and reflection bandwidths were produced in silica optical fiber and in poly(methyl methacrylate) (PMMA) microstructured polymer optical fiber (mPOF), and by adjusting specific inscription parameters and the diffraction pattern, these gratings can present self-apodization and unique spectral characteristics suitable for filtering operations. In addition to being a cost-effective edge filter solution, USFBGs and standard uniform FBGs in silica fiber have similar thermal sensitivities, which results in a straightforward operation without complex equipment or calculations. This FBG interrogation configuration is also quite promising for dynamic measurements, and due to its multiplexing capabilities multiple USFBGs can be inscribed in the same optical fiber, allowing to incorporate several filters with identical or different spectral characteristics at specific wavelength regions in the same fiber, thus showing great potential to create and develop new sensing configurations.

Online Gamma Radiation Monitoring Using Few-Mode Polymer CYTOP Fiber Bragg Gratings.

We investigated the gamma radiation response of fiber Bragg gratings (FBGs) inscribed in a few-mode polymer optical fiber. The fiber had a graded-index CYTOP core of 20 µm and XYLEX overclad of 250 µm in diameter. Four FBGs were exposed to gamma radiation during four irradiation sessions at a 5.3 kGy/h dose rate. The FBGs showed a linear Bragg wavelength shift with the received dose with a mean sensitivity of -3.95 pm/kGy at 43 °C. The increased temperature provides a rise in the sensitivity: it reached -10.6 pm/kGy at 58 °C. After irradiation, the FBGs showed partial recovery, which increased with the received dose. Furthermore, the FBG's reflection power decreased with the dose. This attenuation is mainly due to insertion losses caused by the radiation induced attenuation in the CYTOP fiber. Linear response to the received dose makes CYTOP FBGs attractive for gamma radiation dosimetry. However, temperature dependence of the sensitivity should be compensated in practical applications.

Influence of Two-Plane Position and Stress on Intensity-Variation-Based Sensors: Towards Shape Sensing in Polymer Optical Fibers.

Shape reconstruction is growing as an important real-time monitoring strategy for applications that require rigorous control. Polymer optical fiber sensors (POF) have mechanical properties that allow the measurement of large curvatures, making them appropriate for shape sensing. They are also lightweight, compact and chemically stable, meaning they are easy to install and safer in risky environments. This paper presents a sensor system to detect angles in multiple planes using a POF-intensity-variation-based sensor and a procedure to detect the angular position in different planes. Simulations are performed to demonstrate the correlation between the sensor's mechanical bending response and their optical response. Cyclic flexion experiments are performed at three test frequencies to obtain the sensitivities and the calibration curves of the sensor at different angular positions of the lateral section. A Fast Fourier Transform (FFT) analysis is tested as a method to estimate angular velocities using POF sensors. The experimental results show that the prototype had high repeatability since its sensitivity was similar using different test frequencies at the same lateral section position. The proposed approach proved itself feasible considering that all linear calibration curves presented a coefficient of determination (R2) higher than 0.9.

Biocompatible and Biodegradable Polymer Optical Fiber for Biomedical Application: A Review.

This article discusses recent advances in biocompatible and biodegradable polymer optical fiber (POF) for medical applications. First, the POF material and its optical properties are summarized. Then, several common optical fiber fabrication methods are thoroughly discussed. Following that, clinical applications of biocompatible and biodegradable POFs are discussed, including optogenetics, biosensing, drug delivery, and neural recording. Following that, biomedical applications expanded the specific functionalization of the material or fiber design. Different research or clinical applications necessitate the use of different equipment to achieve the desired results. Finally, the difficulty of implanting flexible fiber varies with its flexibility. We present our article in a clear and logical manner that will be useful to researchers seeking a broad perspective on the proposed topic. Overall, the content provides a comprehensive overview of biocompatible and biodegradable POFs, including previous breakthroughs, as well as recent advancements. Biodegradable optical fibers have numerous applications, opening up new avenues in biomedicine.

Humidity-Sensitive PMMA Fiber Bragg Grating Sensor Probe for Soil Temperature and Moisture Measurement Based on Its Intrinsic Water Affinity.

Soil moisture measurement is very important for soil system monitoring. Compared to the traditional thermo-gravimetric technique, which is time-consuming and can be only performed in labs, the optic-fiber technique has unique advantages, such as small size, remote application in fields, fast response time and immunity to electromagnetic fields. In this paper, the soil moisture is measured by using a polymer optical fiber Bragg grating (POFBG) probe with a packaged dimension of 40 mm × 15 mm × 8 mm. Due to the intrinsic water-absorbing property of poly (methyl methacrylate) (PMMA), optical fiber Bragg gratings based on PMMA have been widely investigated for humidity measurement. Taking advantage of this, a sensor based on the POFBG is investigated to verify the soil condition. The POFBG is protectively integrated inside a stainless-steel package. A window is opened with a thin polypropylene mat as a filter, which allows the air to go through but prevents the soil from going inside to pollute the POFBG. The sensor probe is embedded in soils with different gravimetric soil moisture contents (SMCs) ranging from 0% to 40% and, then, insulated by polyethylene films to minimize the impact from the external environment, showing an average temperature cross sensitivity of -0.080 nm/°C. For a constant temperature, an exponential relationship between the Bragg wavelength and the SMC is obtained. For the SMCs between 8% and 24%, linear relationships are presented showing a temperature-corresponded sensitivity between 0.011 nm/% and 0.018 nm/%. The maximal sensitivity is calculated to be 0.018 nm/% at 20 °C, which is 28 times as high as that in the previous work. For the SMC over 24%, the sensor becomes insensitive because of humidity saturation in the cavity of the sensor probe. Though temperature cross sensitivity is problematic for SMC measurement, the influence could be eliminated by integrating another humidity-insensitive temperature sensor, such as a silica FBG temperature sensor.

Fabrication Quality Assessment Based on the Coupling of a Dual-Core Microstructured Polymer Optical Fiber.

In this paper we report on the theoretical analysis and fabrication of a dual-core microstructured polymer optical fiber (mPOF) and demonstrate how the coupling characteristics of a dual-core mPOF may be a key factor to assess the quality of the fabrication process. The coupling characteristics of this fiber have been tested and, for comparison purposes, simulations regarding the effects of inaccuracies during the manufacturing process were carried out to evaluate the fabrication quality. Results indicate that theoretical, simulation and experimental data are in good agreement, which highlights the uniformity of the microstructure along the fiber and the quality of its fabrication process. In fact, the manufactured mPOF reached a coupling efficiency up to 95.26%, which makes this mPOF appealing for applications in which highly efficient power couplers are required.