Morphological effect of the type, concentration and etching time of acid solutions on enamel and dentin surfaces / Efeito morfológico de tipo, concentração e tempo de condicionamento de soluções ácidas em esmalte e superfícies dentinárias

ABSTRACT

Thirty-six noncarious human molars were extracted and stored in saline. The buccal surfaces were ground wet on 400--grit silicon carbide paper to create a flat surface. The enamel and dentin surfaces were treated with 35 per cent phosphoric acid gel, 10 per cent phosphoric acid gel and 10 per cent maleic acid gel for 15 and 60 seconds. Scanning electron microscope analysis showed that all the acid atchants modified the micromorphological appearance of enamel and dentin surfaces independent of the type of acid, the etching time and the concentration. On the enamel surface, the 35 per cent and 10 per cent phosphoric acid gels and the 10 per cent maleic acid gel applied for 15 or 60 seconds preferentially removed the prism core material. In the specimens trated for 15 seconds with 10 per cent maleic acid the prism core material was partially removed. On the dentin surface, the phosphoric acid gel (35 per cent and 10 per cent) and the 10 per cent maleic acid gel applied for 15 and 60 seconds removed the smear layer and opened the dentinal tubule orifices; however, the dentinal surface etched for 15 or 60 seconds with 10 per cent maleic acid gel showed residues of the smear layer