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Metal centers in biomolecular solid-state NMR.
Malanho Silva, José; Cerofolini, Linda; Giuntini, Stefano; Calderone, Vito; Geraldes, Carlos F G C; Macedo, Anjos L; Parigi, Giacomo; Fragai, Marco; Ravera, Enrico; Luchinat, Claudio.
Afiliação
  • Malanho Silva J; Magnetic Resonance Center (CERM), University of Florence and Consorzio Interuniversitario Risonanze Magnetiche di Metalloproteine, Via L. Sacconi 6, 50019 Sesto Fiorentino, FI, Italy; UCIBIO-Requimte, Faculty of Sciences and Technology, Universidade NOVA de Lisboa, Caparica, Portugal.
  • Cerofolini L; Magnetic Resonance Center (CERM), University of Florence and Consorzio Interuniversitario Risonanze Magnetiche di Metalloproteine, Via L. Sacconi 6, 50019 Sesto Fiorentino, FI, Italy.
  • Giuntini S; Magnetic Resonance Center (CERM), University of Florence and Consorzio Interuniversitario Risonanze Magnetiche di Metalloproteine, Via L. Sacconi 6, 50019 Sesto Fiorentino, FI, Italy; Department of Chemistry "Ugo Schiff", University of Florence, Via della Lastruccia 3, 50019 Sesto Fiorentino, FI, It
  • Calderone V; Magnetic Resonance Center (CERM), University of Florence and Consorzio Interuniversitario Risonanze Magnetiche di Metalloproteine, Via L. Sacconi 6, 50019 Sesto Fiorentino, FI, Italy; Department of Chemistry "Ugo Schiff", University of Florence, Via della Lastruccia 3, 50019 Sesto Fiorentino, FI, It
  • Geraldes CFGC; Department of Life Sciences and Coimbra Chemistry Center, University of Coimbra, Coimbra, Portugal.
  • Macedo AL; UCIBIO-Requimte, Faculty of Sciences and Technology, Universidade NOVA de Lisboa, Caparica, Portugal.
  • Parigi G; Magnetic Resonance Center (CERM), University of Florence and Consorzio Interuniversitario Risonanze Magnetiche di Metalloproteine, Via L. Sacconi 6, 50019 Sesto Fiorentino, FI, Italy; Department of Chemistry "Ugo Schiff", University of Florence, Via della Lastruccia 3, 50019 Sesto Fiorentino, FI, It
  • Fragai M; Magnetic Resonance Center (CERM), University of Florence and Consorzio Interuniversitario Risonanze Magnetiche di Metalloproteine, Via L. Sacconi 6, 50019 Sesto Fiorentino, FI, Italy; Department of Chemistry "Ugo Schiff", University of Florence, Via della Lastruccia 3, 50019 Sesto Fiorentino, FI, It
  • Ravera E; Magnetic Resonance Center (CERM), University of Florence and Consorzio Interuniversitario Risonanze Magnetiche di Metalloproteine, Via L. Sacconi 6, 50019 Sesto Fiorentino, FI, Italy; Department of Chemistry "Ugo Schiff", University of Florence, Via della Lastruccia 3, 50019 Sesto Fiorentino, FI, It
  • Luchinat C; Magnetic Resonance Center (CERM), University of Florence and Consorzio Interuniversitario Risonanze Magnetiche di Metalloproteine, Via L. Sacconi 6, 50019 Sesto Fiorentino, FI, Italy; Department of Chemistry "Ugo Schiff", University of Florence, Via della Lastruccia 3, 50019 Sesto Fiorentino, FI, It
J Struct Biol ; 206(1): 99-109, 2019 04 01.
Article em En | MEDLINE | ID: mdl-30502494
ABSTRACT
Solid state NMR (SSNMR) has earned a substantial success in the characterization of paramagnetic systems over the last decades. Nowadays, the resolution and sensitivity of solid state NMR in biological molecules has improved significantly and these advancements can be translated into the study of paramagnetic biomolecules. However, the electronic properties of different metal centers affect the quality of their SSNMR spectra differently, and not all systems turn out to be equally easy to approach by this technique. In this review we will try to give an overview of the properties of different paramagnetic centers and how they can be used to increase the chances of experimental success.
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Compostos Organometálicos / Espectroscopia de Ressonância Magnética / Ressonância Magnética Nuclear Biomolecular / Metaloproteínas / Metais Idioma: En Revista: J Struct Biol Assunto da revista: BIOLOGIA MOLECULAR Ano de publicação: 2019 Tipo de documento: Article País de afiliação: Portugal
Texto completo
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Compostos Organometálicos / Espectroscopia de Ressonância Magnética / Ressonância Magnética Nuclear Biomolecular / Metaloproteínas / Metais Idioma: En Revista: J Struct Biol Assunto da revista: BIOLOGIA MOLECULAR Ano de publicação: 2019 Tipo de documento: Article País de afiliação: Portugal