Identification of conjugation positions of urinary glucuronidated vitamin D<sub>3</sub> metabolites by LC/ESI-MS/MS after conversion to MS/MS-fragmentable derivatives.

Yoshimura, Yusuke; Hibi, Ryuichiro; Nakata, Akiho; Togashi, Moeka; Ogawa, Shoujiro; Ishige, Takayuki; Satoh, Mamoru; Nomura, Fumio; Higashi, Tatsuya

Identification of conjugation positions of urinary glucuronidated vitamin D₃ metabolites by LC/ESI-MS/MS after conversion to MS/MS-fragmentable derivatives.

Yoshimura, Yusuke; Hibi, Ryuichiro; Nakata, Akiho; Togashi, Moeka; Ogawa, Shoujiro; Ishige, Takayuki; Satoh, Mamoru; Nomura, Fumio; Higashi, Tatsuya.

Afiliação

Yoshimura Y; Faculty of Pharmaceutical Sciences, Tokyo University of Science, Noda-shi, Chiba, Japan.
Hibi R; Faculty of Pharmaceutical Sciences, Tokyo University of Science, Noda-shi, Chiba, Japan.
Nakata A; Faculty of Pharmaceutical Sciences, Tokyo University of Science, Noda-shi, Chiba, Japan.
Togashi M; Faculty of Pharmaceutical Sciences, Tokyo University of Science, Noda-shi, Chiba, Japan.
Ogawa S; Faculty of Pharmaceutical Sciences, Tokyo University of Science, Noda-shi, Chiba, Japan.
Ishige T; Division of Laboratory Medicine, Chiba University Hospital, Chiba, Japan.
Satoh M; Division of Clinical Mass Spectrometry, Chiba University Hospital, Chiba, Japan.
Nomura F; Division of Clinical Mass Spectrometry, Chiba University Hospital, Chiba, Japan.
Higashi T; Faculty of Pharmaceutical Sciences, Tokyo University of Science, Noda-shi, Chiba, Japan.

Biomed Chromatogr ; 33(7): e4538, 2019 Jul.

Article em En | MEDLINE | ID: mdl-30912169

Assuntos

Colecalciferol/urina; Cromatografia Líquida/métodos; Glucuronídeos/urina; Espectrometria de Massas em Tandem/métodos; Colecalciferol/química; Colecalciferol/metabolismo; Glucuronídeos/química; Glucuronídeos/metabolismo; Humanos; Espectrometria de Massas por Ionização por Electrospray/métodos

Palavras-chave

LC/ESI-MS/MS; conjugation position; fragmentable derivatization; glucuronidated vitamin D metabolite; human urine

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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Cromatografia Líquida / Colecalciferol / Glucuronídeos / Espectrometria de Massas em Tandem Tipo de estudo: Diagnostic_studies Limite: Humans Idioma: En Revista: Biomed Chromatogr Ano de publicação: 2019 Tipo de documento: Article País de afiliação: Japão País de publicação: Reino Unido

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